Lead 2,3,6,7,10,11-Triphenylene Hexathiol (HTT-Pb) Framework Single Crystal Synthesis and Interaction with Paraquat Diiodide
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Results: HVaTT and HTT-Pb ([Pb3OH0.5(HTT)]-1.5) Characterization
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Conclusion
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The overall goal of this protocol is to synthesize thiol linker molecules and to prepare single crystals of porous, metal-sulfur frameworks from these thiol species. This method can help answer key questions in the field of materials chemistry as
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Here, we present a one-pot, transition-metal-free synthesis of thiols and thioesters from aromatic halides and sodium thiomethoxide, followed by the preparation of single crystals of a metal-dithiolene network using thiol species generated in situ from the more stable and tractable thioester.