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University of Technology of Troyes

1 ARTICLES PUBLISHED IN JoVE

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Engineering

Characterization of Ultra-fine Grained and Nanocrystalline Materials Using Transmission Kikuchi Diffraction
Gwénaëlle Proust 1, Patrick Trimby 2, Sandra Piazolo 3, Delphine Retraint 4
1School of Civil Engineering, The University of Sydney, 2Australian Centre for Microscopy and Microanalysis, The University of Sydney, 3Department of Earth and Planetary Sciences, Macquarie University, 4Charles Delaunay Institute, LASMIS, UMR STMR CNRS 6281, University of Technology of Troyes

This paper provides a detailed method to characterize the microstructure of ultra-fine grained and nanocrystalline materials using a scanning electron microscope equipped with a standard electron backscatter diffraction system. Metal alloys and minerals presenting refined microstructures are analyzed using this technique, showing the diversity of its possible applications.

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