Electrochemical Exfoliation to Produce High-Quality Black PhosphorusPayam Hashemi 1,2, Davood Sabaghi 1, Sheng Yang 1, Ali Shaygan Nia 1,2, Xinliang Feng 1,2
1Center for Advancing Electronics Dresden (cfaed) and Department of Chemistry and Food Chemistry, Technische Universität Dresden, 2Department of Synthetic Materials and Functional Devices, Max Planck Institute of Microstructure Physics
We present a step-by-step procedure for electrochemical exfoliation of black phosphorus (BP), one of the most promising emerging 2D materials with applications in (opto)electronics, from its bulk crystals, as well as the morphological characterization by scanning electron microscopy, atomic force microscopy, and transmission electron microscopy.
