Visualization of Failure and the Associated Grain-Scale Mechanical Behavior of Granular Soils under Shear using Synchrotron X-Ray Micro-Tomography

Summary

The protocol describes procedures to acquire high-spatial resolution computed tomography (CT) images of a granular soil during triaxial compression, and to apply image processing techniques to these CT images to explore the grain-scale mechanical behavior of the soil under loading.

Abstract

The rapid development of X-ray imaging techniques with image processing and analysis skills has enabled the acquisition of CT images of granular soils with high-spatial resolutions. Based on such CT images, grain-scale mechanical behavior such as particle kinematics (i.e., particle translations and particle rotations), strain localization and inter-particle contact evolution of granular soils can be quantitatively investigated. However, this is inaccessible using conventional experimental methods. This study demonstrates the exploration of the grain-scale mechanical behavior of a granular soil sample under triaxial compression using synchrotron X-ray micro-tomography (μCT). With this method, a specially fabricated miniature loading apparatus is used to apply confining and axial stresses to the sample during the triaxial test. The apparatus is fitted into a synchrotron X-ray tomography setup so that high-spatial resolution CT images of the sample can be collected at different loading stages of the test without any disturbance to the sample. With the capability of extracting information at the macro scale (e.g., sample boundary stresses and strains from the triaxial apparatus setup) and the grain scale (e.g., grain movements and contact interactions from the CT images), this procedure provides an effective methodology to investigate the multi-scale mechanics of granular soils.

Introduction

It is widely recognized that the macro-scale mechanical properties of granular soil, such as stiffness, shear strength and permeability, are critical to many geotechnical structures, for example, foundations, slopes and rock-fill dams. For many years, on-site tests and conventional laboratory tests (e.g., one-dimensional compression tests, triaxial compression tests and permeability tests) have been used to evaluate these properties in different soils. Codes and standards for testing soil mechanical properties have also been developed for engineering purposes. While these macro-scale mechanical properties have been intensively studied, the grain-scale mechanical behav....

Protocol

1. Designing the experiment well in advance

1. Determine test material, particle size, sample size and sample initial porosity.
   NOTE: Leighton Buzzard sand with a diameter of 0.15~0.30 mm and a sample size of 8 x 16 mm (Diameter x Height) is used as an example to demonstrate the protocol of this study. Other sands such as Fujian sand, Houston Sand, Ottawa sand and Caicos ooids, etc. and similar sample sizes can also be used.
2. Choose an appropriate detector (Figure 1A) according to the required spatial resolution and scanning area, which are determined according to the predetermined particle size a....

Results

Figure 5 depicts the particle kinematics results of a Leighton Buzzard sand (LBS) sample at a 2D slice during two typical shear increments, I and II. Most of the particles are successfully tracked and their translations and rotations are quantified following the above protocol. During the first shear increment, neither particle displacements nor particle rotations show clear localization. However, a localized band is developed in both the particle displacement map and particle rotation map d.......

Discussion

High-spatial resolution X-ray micro-CT and advanced image processing and analysis techniques have enabled the experimental investigation of the mechanical behavior of granular soils under shear at multi-scale levels (i.e., at macro-scale, meso-scale and grain-scale levels). However, CT image-based meso- and grain-scale investigations require the acquisition of high-spatial resolution CT images of soil samples during loading. The most challenging aspect of this process is perhaps the fabrication of a miniature triaxial lo.......

Materials

Name	Company	Catalog Number	Comments
Confining pressure offering device	GDS	STDDPC
De-aired water	N/A	N/A	Water de-aired in the lab
Leighton Buzzard sand	Artificial Grass Cambridge	Drained Industrial Sand 25 kg	Can be replaced with different soils
Miniature triaxial loading device	N/A	N/A	The miniature loading device is specially fabricated by the authors
Silicon grease	RS company	RS 494-124
Synchrotron radiation X-ray micro CT setup	Shanghai Synchrotron Radiation Facility Center (SSRF)	13W1	The triaxial testing is carried out at the BL13W beam-line of the SSRF
Vacuum pump	Hong Kong Labware Co., ltd.	Rocker 300