Name: quantifying the relative thickness of conductive ferromagnetic materials using detector coil-based pulsed eddy current sensors
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Description: Watch this Scientific Journal Video about Quantifying the Relative Thickness of Conductive Ferromagnetic Materials Using Detector Coil-Based Pulsed Eddy Current Sensors at JoVE.com

The authors would like to acknowledge the contributions made by Michael Behrens and Damith Abeywardana in designing and implementing several sensing hardware components. Research supervision roles played by Alen Alempijevic, Teresa Vidal-Calleja, Gamini Dissanayake, and Sarath Kodagoda, as well as contributions made by all persons and organizations who funded and partnered with the Critical Pipes Project, are also acknowledged.

1. Extracting the decay rate &#946; from an available detector coil-based PEC signal
<ol>
	<li>Express an available experimentally captured PEC signal (i.e., a time domain detector coil voltage (denoted as V(t))) in the logarithmic form of ln[V(t)]. A typical PEC signal expressed in the form of ln[V(t)] is shown in Figure 1.</li>
	<li>Find a linear region in the form of <img align="center" alt="Equation 2" src="/files/ftp_uploa...

<ol>
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A protocol to quantify the relative thickness (i.e., thickness as a percentage with respect to a reference) of conductive ferromagnetic materials using detector coil-based PEC sensors was presented. The main advantage of this method is the ability to overcome the calibration requirement (i.e., overcome the need to measure or estimate the magnetic permeability and electrical conductivity of the material being inspected to enable thickness quantification). The protocol involves logarithmic representation of the time domain...

The pulsed eddy current (PEC) sensing technique is perhaps the most versatile member of the family of eddy current (EC) non-destructive evaluation (NDE) techniques and has many applications in detection and quantification of defects, and the geometry of metals and metallic structures1. Thickness quantification of conductive ferromagnetic wall-like structures, having wall thicknesses of no more than a few millimeters to a few tens of millimeters, is a high demand engineering service in the field of structural health monitoring of infrastructure. Critical infrastructure made of ferromagnetic alloys that require this service are commonly available in the energy, water, oil, and gas industries. While PEC sensors can be designed following several architectures, the detector coil-based architecture was determined to be the most effective and commonly used in condition assessment of ferromagnetic materials2,3,4,5. Therefore, it is the detector coil-based PEC sensor architecture that sets the foundation to the problem of thickness quantification of conductive ferromagnetic materials.
The detector coil-based PEC sensor architecture is typically comprised of two concentrically wound, air cored, conductive coils2,3,4,5,6 (typically copper coils). It is quite common to wind these coils to be circular in shape2,3,4,5,6, but occasionally, rectangular shaped coils6 have been used. From the two coils in the sensor, one behaves as an exciter coil while the other acts as the detector coil. In a PEC sensor, the exciter coil is excited by a voltage pulse - something that can be characterized as a Heaviside step function in principle. This pulsed excitation generates a transient magnetic field (called the primary field) around the sensor. When the sensor is placed adjacent to a conductive test piece (e.g., a conductive ferromagnetic wall-like structure), this transient magnetic field induces time varying eddy currents in the test piece. These eddy currents generate a secondary magnetic field (called the secondary field) that opposes the primary field. In response to the resultant effect of the primary and secondary fields, a transient voltage is induced in the detector coil - which becomes the time domain PEC signal of interest for this work.
The PEC sensor detector coil voltage decay rate (denoted as &#946;) has been reported6,7,8 to show the proportionality &#946; <img align="center" alt="Equation 7" src="/files/ftp_upload/59618/59618eq7a.jpg" /> &#956;&#963;d2, when a signal is acquired placing a PEC sensor above a conductive ferromagnetic layer of magnetic permeability &#956;, electrical conductivity &#963;, and thickness d. Although this decay rate signal feature has considerable immunity to parameters such as sensor size, sensor shape, and lift-off6,7,8, which makes the decay rate highly desirable for challenging NDE scenarios such as in situ pipe condition assessment9,10,11, this feature must be calibrated (i.e., &#956;, &#963; of the material being inspected be estimated) to enable thickness (i.e., d) quantification. To enable conventional methods of decay rate-based thickness quantification6,8, this calibration must be done by extracting calibration samples6,8 or by involving eddy current-based material property characterization methods12,13. Alternatively, the complexity of calibration can be avoided by representing thickness in the form of relative thickness. Suppose an NDE exercise is carried out and &#946; values are extracted from signals, then, the &#946; value qualitatively representative of the maximum thickness point in the test piece is considered as a reference (i.e., &#946;ref <img align="center" alt="Equation 7" src="/files/ftp_upload/59618/59618eq7a.jpg" /> &#956;&#963;dmax2); then, the thickness of any other location can be represented as a percentage of the maximum thickness in the form <img align="center" alt="Equation 1" src="/files/ftp_upload/59618/59618eq1g.jpg" />, presenting a relative thickness as the output, which is still useful qualitative information as an NDE output that also carries the simplicity of not having to calibrate for &#956;, &#963;. The protocol presented herein describes the steps to be followed to accomplish this.
Since the decay rate &#946; shows generality to the detector coil-based PEC sensor architecture while showing immunity to parameters of the sensor design as well as lift-off6,7,8,14, practitioners may use any detector coil-based PEC sensing system of their choice on a suitable conductive ferromagnetic material to perform relative thickness quantification following the protocol here. A PEC sensor design example for a conductive ferromagnetic material is available for interested readers15. The signals and results presented in this work were acquired using the PEC system developed by University of Technology Sydney6,8. The conductive ferromagnetic material used for representative results acquired by the PEC system is grey cast iron extracted from a pipe test-bed9,10,11 in Sydney Australia.
It should be noted that the methods, results, and discussions presented in this publication explicitly focus on the use of the detector coil-based PEC sensor architecture&#39;s time domain signal&#39;s decay rate for thickness quantification of conductive ferromagnetic materials. The publication does not include a broader discussion on general conventions of PEC sensing principles and sensor configurations. Other published work16,17,18 can be useful for readers to gain more insight about PEC sensor configurations other than the detector coil-based sensor architecture.

<table border="1" fo:keep-together.within-page="1" fo:keep-with-next.within-page="always">
	<tbody>
		<tr>
			<td>A Detector Coil-based PEC Sensing System.</td>
			<td>N/A</td>
			<td></td>
			<td>The representative results in this work were generated using the PEC system developed by University of Technology Sydney (UTS), Australia and published in works 6,8. This system may be accessible to readers via collaborating with UTS.</td>
		</tr>
		<tr>
			<td>A suitable conductive ferromagnetic material of varying thickness.</td>
			<td>N/A</td>
			<td></td>
			<td>The representative results in this work were generated by acquiring PEC measurements on grey cast iron test pieces extracted from a pipe test-bed located in Sydney Australia, whose location and vintage details are available in references 9-11. The pipe test-bed as well as the extracted calibration samples may be accessible to readers via collaborating with UTS.</td>
		</tr>
		<tr>
			<td>A computation platform for PEC signal processing</td>
			<td>MathWorks, Natick, MA, USA.</td>
			<td></td>
			<td>A computation platform in which the PEC signal processing algorithm can be coded and executed is required. In this publication, PEC signal processing was done using a software executable named &#34;PEC_Signal_Processor&#34;, produced using MATLAB R2017b, Publisher: MathWorks, Natick, MA, USA.</td>
		</tr>
		<tr>
			<td>An application that can produce a table containing raw PEC signals (e.g., Microsoft Office Excel).</td>
			<td>Microsoft Corporation, One Microsoft Way, Redmond, Washington, USA.</td>
			<td></td>
			<td>Microsoft Office Excel (Office 16) was used for the work of this publication.</td>
		</tr>
	</tbody>
</table>

quantifying the relative thickness of conductive ferromagnetic materials using detector coil-based pulsed eddy current sensors

Thickness quantification of conductive ferromagnetic materials by means of non-destructive evaluation (NDE) is a crucial component of structural health monitoring of infrastructure, especially for assessing the condition of large diameter conductive ferromagnetic pipes found in the energy, water, oil, and gas sectors. Pulsed eddy current (PEC) sensing, especially detector coil-based PEC sensor architecture, has established itself over the years as an effective means for serving this purpose. Approaches for designing PEC sensors as well as processing signals have been presented in previous works. In recent years, the use of the decay rate of the detector coil-based time domain PEC signal for the purpose of thickness quantification has been studied. Such works have established that the decay rate-based method holds generality to the detector coil-based sensor architecture, with a degree of immunity to factors such as sensor shape and size, number of coil turns, and excitation current. Moreover, this method has shown its effectiveness in NDE of large pipes made of grey cast iron. Following such literature, the focus of this work is explicitly PEC sensor detector coil voltage decay rate-based conductive ferromagnetic material thickness quantification. However, the challenge faced by this method is the difficulty of calibration, especially when it comes to applications such as in situ pipe condition assessment since measuring electrical and magnetic properties of certain pipe materials or obtaining calibration samples is difficult in practice. Motivated by that challenge, in contrast to estimating actual thickness as done by some previous works, this work presents a protocol for using the decay rate-based method to quantify relative thickness (i.e., thickness of a particular location with respect to a maximum thickness), without the requirement for calibration.

Representative results within this section have been generated using the PEC signals provided as supplementary material with reference8; as mentioned above, the signals have been captured on grey cast iron samples extracted from the pipe test bed in Sydney Australia, whose location and vintage details are provided in references9,10,11.
Figure 1 sho...

Watch this Scientific Journal Video about Quantifying the Relative Thickness of Conductive Ferromagnetic Materials Using Detector Coil-Based Pulsed Eddy Current Sensors at JoVE.com

Quantifying the Relative Thickness of Conductive Ferromagnetic Materials Using Detector Coil-Based Pulsed Eddy Current Sensors

Here, we present a protocol to quantify the relative thickness (i.e., thickness as a percentage with respect to a reference) of conductive ferromagnetic materials using detector coil-based pulsed eddy current sensors, while overcoming the calibration requirement.

Thickness quantification of conductive ferromagnetic materials by means of non-destructive evaluation (NDE) is a crucial component of structural health ...

Pulsed eddy current sensing is an electro-magnetic sensing technique used to assess certain physical properties and effects of electrically conductive and sometimes ferromagnetic materials. We will introduce the use of a software interface of utilizing the pulsed eddy current signals captured from detector coil based sensor architecture and how to extract information from those signals. This protocol enables a relative thickness quantification of ferromagnetic metallic woolite structures using pulsed eddy current sensing.This technique enables the measurement of the extent of corrosion, graphitization or wool loss of ferromagnetic wool like structures for assessment of there structure and build and integrate it. For pulsed eddy current signal processor installation, locate and execute the PEC signal processor. exe file, and when the interface appears, click next.When the next interface opens, specify the file location for installation and check the add a shortcut to the desktop check box to add the software icon to the desktop. Click next and specify the installation location for the required run time environment. When the installation is complete, click finish.The desktop icon will appear. Before beginning the analysis, use a detector coil based pulsed eddy current sensing unit with an operating electronic box and a detector coil based sensor to collect pulsed eddy current signals from the metal structure of interest. At the end of the scan, export the collected signals from the sensing unit to a compatible, editable word processor and confirm that the signals are arranged as a table.Copy the table to the desktop and double click the desktop icon to run the application. The interface will open. To load the signals, click the load signals tab and select the file containing the signals to import the signals to the software interface.When the number of signals contained within the table containing raw signals appears, click pot signals, and observe the signals plotted in logarithmic scale. Click the zoom tab and adjust the plot window for the linear region until it is clearly visible. The lower and upper margins should encompass a straight line region within the light shade of the signals.If unsure, we recommend generating relative thickness values using several margins and then compare the results. After entering reasonable lower and upper margins for the region, click plot margins and wait for the margins to be plotted in green. Click extract features, the straight line segments will be plotted in red.Click calculate relative thickness to observe the plotting of a histogram of calculated relative thickness values. Click save relative thickness to save the calculated relative thickness values. Enter a file name, and click ok.Then click ok again to confirm the file name. The relative thickness values will be saved as a table on the desktop. The relative thickness values shown on screen are in the form of fractions.One denotes maximum thickness for the 100%reference. Here, the typical shape of a time domain signal expressed in the logarithmic form captured from a detector coil based pulsed eddy current sensor is shown. An indicative linear region of the later stage of the logarithmic signal can be observed, for which t is much greater than 0, and from which the decay rate feature beta is extracted.Here, a set of signals captured on different thicknesses of gray cast iron is shown. This signal corresponds to the maximum thickness with the maximum beta value in the set. Such values can be selected as reference beta values to facilitate quantification of the relative thickness, using the equation as indicated.In this table, the actual relative thickness values and the relative thickness values calculated from beta values obtained from pulsed eddy current signals for a representative experiment, are shown. Here, the corelation between pulsed eddy current signal based relative thickness estimates and the actual relative thickness values can be observed. The effectiveness of the method is demonstrated by the high correlation depicted by the linear relationship.Take care to avoid the current region of the pulsed eddy current signal and to select the linear region at the light stage to allow extraction of the beta feature. Pulsed and other eddy current techniques are commonly used for a anomaly detection, physical property measurements, and for the assessment of non-metallic coatings covering metallic structures.

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JoVE Journal

Physics

Engineering

Unit 1

Sources of Magnetic Fields

SCIENTISTS IN ACTION

Concurrent Quantitative Conductivity and Mechanical Properties Measurements of Organic Photovoltaic Materials using AFM

Organic photovoltaic  (OPV) materials are inherently inhomogeneous at the nanometer scale. Nanoscale  inhomogeneity of OPV materials affects performance ...

Fabrication of Nano-engineered Transparent Conducting Oxides by Pulsed Laser Deposition

Nanosecond Pulsed  Laser Deposition (PLD) in the presence of a background gas allows the deposition  of metal oxides with tunable morphology, structure, ...

Using Neutron Spin Echo Resolved Grazing Incidence Scattering to Investigate Organic Solar Cell Materials

The spin echo resolved grazing incidence scattering (SERGIS) technique has been used to probe the length-scales associated with irregularly shaped ...

Using Microwave and Macroscopic Samples of Dielectric Solids to Study the Photonic Properties of Disordered Photonic Bandgap Materials

Recently, disordered photonic materials have been suggested as an alternative to periodic crystals for the formation of a complete photonic bandgap (PBG). ...

Formation of Thick Dense Yttrium Iron Garnet Films Using Aerosol Deposition

Aerosol deposition (AD) is a thick-film deposition process that can produce layers up to several hundred micrometers thick with densities greater than 95% ...

Detection and Recovery of Palladium, Gold and Cobalt Metals from the Urban Mine Using Novel Sensors/Adsorbents Designated with Nanoscale Wagon-wheel-shaped Pores

Developing low-cost, efficient processes for recovering and recycling palladium, gold and cobalt metals from urban mine remains a significant challenge in ...

Quantification of Hydrogen Concentrations in Surface and Interface Layers and Bulk Materials through Depth Profiling with Nuclear Reaction Analysis

Nuclear reaction analysis (NRA) via the resonant 1H(15N,&#945;&#947;)12C reaction is a highly effective method of depth profiling that quantitatively and ...

Characterization of Full Set Material Constants and Their Temperature Dependence for Piezoelectric Materials Using Resonant Ultrasound Spectroscopy

During the operation of high power electromechanical devices, a temperature rise is unavoidable due to mechanical and electrical losses, causing the ...