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DOI :
10.3791/61955-v
July 14th, 2022
Chapters
0:04
Introduction
0:29
Scanning Electron Microscope (SEM) and Cryogenic Station Preparation
1:31
Sample Vitrification
2:51
Sample Surface Imaging and Feature Location
4:19
Cross-Section Preparation
6:52
Energy Dispersive X-Ray (EDX) Mapping
8:12
Results: Representative Nanoscale Liquid-Solid Interface Characterization
10:24
Conclusion
極低温集束イオンビーム(FIB)および走査型電子顕微鏡(SEM)技術は、無傷の固液界面の化学的性質および形態に関する重要な洞察を提供することができる。このような界面の高品質のエネルギー分散型X線(EDX)分光マップを調製するための方法は、エネルギー貯蔵デバイスに焦点を当てて詳述されている。
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