Name: Enhancing Fiber Composite Laminate Quality with the Wet Hand Lay-Up/Vacuum Bag Process (Video) | JoVE
Uploaded: 2023-06-30T14:40:00
Description: Watch this Scientific Journal Video about Enhancing Fiber Composite Laminate Quality with the Wet Hand Lay-Up/Vacuum Bag Process at JoVE.com

The authors would like to thank the grants from the National Key Research and Development Program of China (No. 2022YFB3706503) and the Stable Support Plan Program of Shenzhen Natural Science Fund (No. 20220815133826001).

1. Material preparation
<ol>
	<li>Cut eight pieces of 300 mm x 300 mm woven glass fiber fabric with scissors. Tape the cut first to prevent the fiber filaments from falling off. 
	NOTE: Wear a mask and gloves to prevent finger pricking and filament inhalation when cutting the fabric. Not only the woven glass fiber fabric, but unidirectional fabric and other types of fiber, such as carbon fiber and aramid fiber, are also available.</li>
	<li>Weigh out 260 g of epoxy resin and 78 g of hardener accor...

Fabrication and Mechanical Property Assessment of Fiber Composite Laminates

This paper focuses on the two different fabrication processes for the hand lay-up method with low cost. Therefore, two fabrication processes were selected to be carefully described in this paper, which are simpler, easier to master, lower in investment cost, and suitable for production with material modification in laboratories and small-scale factories. During the cure of laminates, high consolidation pressure plays an important role in manufacturing laminates with high quality. The adoption of the traditional WL proces...

Fiber reinforced polymer composite (FRP) is a type of high-strength material manufactured by mixing fiber reinforcement and polymer matrixes1,2,3. It is widely used in the aerospace4,5,6, construction7,8, automotive9, and marine10,11 industries due to its low density, high specific stiffness and strength, fatigue properties, and excellent corrosion resistance. Common synthetic fibers include carbon fibers, glass fibers, and aramid fibers12. Glass fiber was chosen for investigation in this paper. Compared to traditional steel, glass fiber reinforcement composite laminates (GFRPs) are lighter, with less than one-third of the density, but can achieve a higher specific strength than steel.
The preparation process of FRP includes vacuum-assisted resin transfer molding (VARTM)13, filament winding (FW)14, and prepreg molding, in addition to many other advanced fabrication processes15,16,17,18. Compared to other preparation processes, the wet hand lay-up/vacuum bag (WLVB) process has several advantages, including simple equipment requirements and uncomplicated process technology, and the products are not limited by size and shape. This process has a high degree of freedom and can be integrated with metal, wood, plastic, or foam.
The principle of the WLVB process is to apply greater forming pressure through vacuum bags to enhance the mechanical properties of the prepared laminates; the production technology of this process is easy to master, making it an economical and simple composite material preparation process. This process is completely manual, and it is greatly influenced by the skills of preparation personnel. Therefore, the products are prone to defects such as voids and uneven thickness, leading to unstable qualities and mechanical properties of the laminate. Hence, it is necessary to describe the WLVB process in detail, finely control steps, and quantify material proportion, in order to obtain a high stability of mechanical properties of laminates.
Most researchers have studied the quasi-static19,20,21,22,23 and dynamic behavior24,25,26,27,28, as well as the property modification29,30 of composite materials. The volume fraction ratio of fiber to matrix plays a crucial role in mechanical properties of FRP laminate. In an appropriate range, a higher volume fraction of fiber can improve the strength and stiffness of FRP laminate. Andrew et al.31 investigated the effect of fiber volume fraction on the mechanical properties of specimens prepared by the fused deposition modeling (FDM) additive manufacturing process. The results showed that when the fiber volume fraction was 22.5%, the tensile strength efficiency reached its maximum, and a slight improvement in strength was observed as the fiber volume fraction reached 33%. Khalid et al.32 studied the mechanical properties of continuous carbon fiber (CF)-reinforced 3D-printed composites with diverse fiber volume fractions, and the results showed that both tensile strength and stiffness were improved with the rise in fiber content. Uzay et al.33 investigated the effects of three fabrication methods-hand lay-up, compression molding, and vacuum bagging-on the mechanical properties of carbon fiber-reinforced polymer (CFRP). The fiber volume fraction and void of the laminates were measured, tensile and bending tests were conducted. The experiments showed that the higher the fiber volume fraction, the better the mechanical properties.
Voids are one of the most common defects in FRP laminate. Voids reduce the mechanical properties of composite materials, such as strength, stiffness, and fatigue resistance34. The stress concentration generated around the voids promotes the propagation of micro-cracks and reduces the interface strength between reinforcement and matrix. Internal voids also accelerate the moisture absorption of FRP laminate, resulting in interface debonding and performance degradation. Therefore, the existence of internal voids affects the reliability of composite and restricts their wide application. Zhu et al.35 investigated the influence of void content on the static interlaminar shear strength properties of CFRP composite laminates, and found that a 1% increase in void content ranging from 0.4% to 4.6% led to a 2.4% deterioration in interlaminar shear strength. Scott et al.36 presented the effect of voids on damage mechanism in CFRP composite laminates under hydrostatic loading using computed tomography (CT), and found that the number of voids is 2.6-5 times the number of randomly distributed cracks.
High-quality and reliable FRP laminates can be manufactured by using an autoclave. Abraham et al.37 manufactured low-porosity, high-fiber content laminates by placing a WLVB assembly in an autoclave with a pressure of 1.2 MPa for curing. Nevertheless, the autoclave is a large and expensive piece of equipment, resulting in considerable manufacturing costs. Although the vacuum-assisted resin transfer process (VARTM) has been in use for a long time, it has a limit in terms of the time cost, a more complicated preparation process, and more disposable consumables such as diversion tubes and diversion media. Compared with the WL process, the WLVB process compensates for insufficient molding pressure through a low-cost vacuum bag, absorbing excess resin from the system to increase the fiber volume fraction and reduce the internal pore content, thereby greatly improving the mechanical properties of the laminate.
This study explores the differences between the WL process and the WLVB process, and details the meticulous process of the WLVB process. The fiber volume content of laminates was calculated by the formula method, and the results showed that the fiber volume content of WL laminates was 42.04%, while that of WLVB laminates was 57.82%, increasing by 15.78%. The mechanical properties of laminates were characterized by tensile and impact tests. The experimental results revealed that with the WLVB process, the strength and modulus of the laminates were enhanced by 17.4% and 16.35%, respectively, and the specific absorbed energy was increased by 19.48%.

<table border="1" fo:keep-together.within-page="1" fo:keep-with-next.within-page="always">
	<tbody>
		<tr>
			<td>breather fabric</td>
			<td>Easy composites</td>
			<td>BR180</td>
			<td></td>
		</tr>
		<tr>
			<td>drop-weight impact testing machine</td>
			<td>Instron</td>
			<td>9340</td>
			<td></td>
		</tr>
		<tr>
			<td>Epoxy matrix</td>
			<td>Axson Technologies</td>
			<td>5015/5015</td>
			<td></td>
		</tr>
		<tr>
			<td>glass fiber</td>
			<td>Weihai Guangwei Composites</td>
			<td>W-9311</td>
			<td></td>
		</tr>
		<tr>
			<td>non-porous release film</td>
			<td>Easy composites</td>
			<td>R240</td>
			<td></td>
		</tr>
		<tr>
			<td>Peel ply&#160;</td>
			<td>Sino Composite</td>
			<td>CVP200</td>
			<td></td>
		</tr>
		<tr>
			<td>perforated released film</td>
			<td>Easy composites</td>
			<td>R120-P3</td>
			<td></td>
		</tr>
		<tr>
			<td>test machine</td>
			<td>ZwickRoell</td>
			<td>250kN</td>
			<td></td>
		</tr>
		<tr>
			<td>vacuum film</td>
			<td>Easy composites</td>
			<td>GVB200</td>
			<td></td>
		</tr>
	</tbody>
</table>

measuring the mechanical properties of glass fiber reinforcement polymer composite laminates obtained by different fabrication processes

The traditional wet hand lay-up process (WL) has been widely applied in the manufacturing of fiber composite laminates. However, due insufficiency in the forming pressure, the mass fraction of fiber is reduced and lots of air bubbles are trapped inside, resulting in low-quality laminates (low stiffness and strength). The wet hand lay-up/vacuum bag (WLVB) process for the fabrication of composite laminates is based on the traditional wet hand lay-up process, using a vacuum bag to remove air bubbles and provide pressure, and then carrying out the heating and curing process. 
Compared with the traditional hand lay-up process, laminates manufactured by the WLVB process show superior mechanical properties, including better strength and stiffness, higher fiber volume fraction, and lower void volume fraction, which are all benefits for composite laminates. This process is completely manual, and it is greatly influenced by the skills of the preparation personnel. Therefore, the products are prone to defects such as voids and uneven thickness, leading to unstable qualities and mechanical properties of the laminate. Hence, it is necessary to finely describe the WLVB process, finely control steps, and quantify material ratios, in order to ensure the mechanical properties of laminates. 
This paper describes the meticulous process of the WLVB process for preparing woven plain patterned glass fiber reinforcement composite laminates (GFRPs). The fiber volume content of laminates was calculated using the formula method, and the calculated results showed that the fiber volume content of WL laminates was 42.04%, while that of WLVB laminates was 57.82%, increasing by 15.78%. The mechanical properties of the laminates were characterized using tensile and impact tests. The experimental results revealed that with the WLVB process, the strength and modulus of the laminates were enhanced by 17.4% and 16.35%, respectively, and the specific absorbed energy was increased by 19.48%.

Measuring the Mechanical Properties of Glass Fiber Reinforcement Polymer Composite Laminates Obtained by Different Fabrication Processes

Table 1 shows the fiber volume fraction, average thickness, and fabrication process of the samples. The G8-WLVB and G8-WL represent the laminates consisting of 8-ply glass fabric manufactured by wet hand lay-up with and without the vacuum bag process, respectively. Obviously, with the vacuum bag assistance, laminates have an increase of 15.78% in fiber volume fraction, as well as an reduction of 16.27% in average thickness.
Strain-stress curves obtained by the tensile test of ...

Watch this Scientific Journal Video about Enhancing Fiber Composite Laminate Quality with the Wet Hand Lay-Up/Vacuum Bag Process at JoVE.com

Enhancing Fiber Composite Laminate Quality with the Wet Hand Lay-Up/Vacuum Bag Process (Video) | JoVE

This paper describes a fabrication process for fiber-reinforced polymer matrix composite laminates obtained using the wet hand lay-up/vacuum bag method.

The traditional wet hand lay-up process (WL) has been widely applied in the manufacturing of fiber composite laminates. However, due insufficiency in the ...