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Center for High Pressure Science and Technology Advanced Research

2 ARTICLES PUBLISHED IN JoVE

Chemistry

An Externally-Heated Diamond Anvil Cell for Synthesis and Single-Crystal Elasticity Determination of Ice-VII at High Pressure-Temperature Conditions

Xiaojing Lai^1,2, Feng Zhu², Jin S. Zhang³, Dongzhou Zhang^2,4, Sergey Tkachev⁴, Vitali B. Prakapenka⁴, Bin Chen²

¹Gemmological Institute, China University of Geosciences (Wuhan), ²Hawai'i Institute of Geophysics and Planetology, University of Hawai'i at Mānoa, ³Department of Earth and Planetary Sciences, University of New Mexico, ⁴Center for Advanced Radiation Sources, University of Chicago

This work focuses on the standard protocol for preparing the externally-heated diamond anvil cell (EHDAC) for generating high-pressure and high-temperature (HPHT) conditions. The EHDAC is employed to investigate materials in Earth and planetary interiors under extreme conditions, which can be also used in solid state physics and chemistry studies.

JoVE Core

Determining the Mechanical Strength of Ultra-Fine-Grained Metals

Jianing Xu^*1,2, Yanju Wang^*2, Jinyuan Yan³, Bin Chen^1,2

¹School of Science, Harbin Institute of Technology, ²Center for High Pressure Science and Technology Advanced Research, ³Advanced Light Source, Lawrence Berkeley National Lab

The protocol presented here describes the high-pressure radial diamond-anvil-cell experiments and analyzing the related data, which are essential for obtaining the mechanical strength of the nanomaterials with a significant breakthrough to the traditional approach.