JoVE Logo

Zaloguj się

Melting Point

Przegląd

Source: Vy M. Dong and Jan Riedel, Department of Chemistry, University of California, Irvine, CA

One of the most important properties of a crystalline solid is its melting point. It can be used to determine the purity of a known compound and gives important information about the stability of the formed crystals.

Procedura

1. Sample Preparation

  1. Take a special glass capillary that fits the melting point apparatus in use.
  2. Dip the open end of the capillary into a sample of benzoic acid
  3. Gently tap the glass capillary on a hard surface, like a table, so that the benzoic acid moves down to the very bottom of the glass capillary

2. Measuring the Melting Point

  1. Insert the glass capillary into the melting point apparatus.
  2. Heat the apparatus with a rate of 10 

Log in or to access full content. Learn more about your institution’s access to JoVE content here

Wyniki

A sample of pure benzoic acid will melt at 122 °C.

Log in or to access full content. Learn more about your institution’s access to JoVE content here

Wniosek i Podsumowanie

The melting point is an important property of a crystalline solid. It can be measured easily and gives information about the identity and purity, as well as the bonding strength within the crystal lattice.

Due to its simple determination, the melting point is still an important property that is commonly employed to identify compounds and qualify their purity. The melting point can not only be used to identify solids, but also liquids like isopropanol. Through derivatization of isopropanol wit

Log in or to access full content. Learn more about your institution’s access to JoVE content here

Tagi
Melting PointSolidTemperatureOrganic CompoundsPurityIdentityMeasurementApplicationsSolid PhaseAmorphous SolidsCrystalline SolidsLattice StructureIntermolecular ForcesThermodynamic ConditionCoexistMelting RangeThermodynamic PropertyChemical Data

Przejdź do...

0:04

Overview

0:39

Principles of Melting Point

3:01

Melting Point Measurement Protocol

3:54

Applications

4:53

Summary

Filmy z tej kolekcji:

article

Now Playing

Melting Point

Organic Chemistry II

148.3K Wyświetleń

article

Cleaning Glassware

Organic Chemistry II

121.9K Wyświetleń

article

Nucleophilic Substitution

Organic Chemistry II

98.5K Wyświetleń

article

Reducing Agents

Organic Chemistry II

42.5K Wyświetleń

article

Grignard Reaction

Organic Chemistry II

147.9K Wyświetleń

article

n-Butyllithium Titration

Organic Chemistry II

47.3K Wyświetleń

article

Dean-Stark Trap

Organic Chemistry II

97.5K Wyświetleń

article

Ozonolysis of Alkenes

Organic Chemistry II

66.3K Wyświetleń

article

Organocatalysis

Organic Chemistry II

16.5K Wyświetleń

article

Palladium-Catalyzed Cross Coupling

Organic Chemistry II

33.3K Wyświetleń

article

Solid Phase Synthesis

Organic Chemistry II

40.4K Wyświetleń

article

Hydrogenation

Organic Chemistry II

48.5K Wyświetleń

article

Polymerization

Organic Chemistry II

90.2K Wyświetleń

article

Infrared Spectroscopy

Organic Chemistry II

211.4K Wyświetleń

article

Polarimeter

Organic Chemistry II

98.2K Wyświetleń

JoVE Logo

Prywatność

Warunki Korzystania

Zasady

Badania

Edukacja

O JoVE

Copyright © 2025 MyJoVE Corporation. Wszelkie prawa zastrzeżone