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Chemoselective Preparation of 1-Iodoalkynes, 1,2-Diiodoalkenes, and 1,1,2-Triiodoalkenes Based on the Oxidative Iodination of Terminal Alkynes

7.6K Views

09:54 min

September 12th, 2018

DOI :

10.3791/58063-v

September 12th, 2018


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Chemoselective Iodination

Rozdziały w tym wideo

0:04

Title

1:15

Synthesis of 1-(Iodoethynyl)-4-Methylbenzene (Compound 2)

3:16

Synthesis of (E)-1-(1,2-Diiodovinyl)-4-Methylbenzene (Compound 3)

4:44

Synthesis of 1-Methyl-4-(1,2,2-Triiodovinyl)benzene (Compound 4)

6:58

Determination of Selectivity for Mono-, Di-, or Tri-Iodination of Terminal Alkynes by HPLC

7:53

Results: Chemoselective Synthesis of 1-Iodoalkynes, 1,2-Diiodoalkenes, and 1,1,2-Triiodoalkenes

9:37

Conclusion

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