A Direct, Regioselective and Atom-Economical Synthesis of 3-Aroyl-N-hydroxy-5-nitroindoles by Cycloaddition of 4-Nitronitrosobenzene with Alkynones

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8.0K Views

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07:30 min

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January 21st, 2020

DOI :

10.3791/60201-v

January 21st, 2020

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Luca Scapinello¹, Angelo Maspero¹, Stefano Tollari¹, Giovanni Palmisano¹, Kenneth M Nicholas², Andrea Penoni¹

¹Dipartimento di Scienza e Alta Tecnologia, Università degli Studi dell'Insubria, ²Department of Chemistry and Biochemistry, University of Oklahoma, Stephenson Life Sciences Research Center

Podsumowanie

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Synthetic Organic Chemistry

4 nitronitrosobenzene

Jones Reagent

Thin Layer Chromatography

N hydroxy Derivatives

1 phenyl 2 propyne 1 one

Potassium Peroxy Monosulfate

Rozdziały w tym wideo

0:05

Title

1:02

1-Phenyl-2-Propyne-1-One Synthesis

2:29

4-Nitronitrosobenzene Preparation

3:37

3-Benzoyl-1-Hydroxy-5-Nitroindole Synthesis

4:48

Results: Representative 3-Aroyl-N-Hydroxy-5-Nitroindole Synthesis

6:32

Conclusion

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