Name: characterization of anisotropic leaky mode modulators for holovideo
Uploaded: 2016-03-19T15:00:00
Description: Watch this Scientific Journal Video about Characterization of Anisotropic Leaky Mode Modulators for Holovideo at JoVE.com

The authors gratefully acknowledge financial support from Air Force Research Laboratory contract FA8650-14-C-6571 and from DAQRI LLC.

1. Initial Preparation
Note: Begin with a new X-cut lithium niobate wafer. It should be optical grade, 1 mm thick, clean, with nothing deposited on the surface, both sides polished, and the top side marked.
<ol>
	<li>Using an Electron Beam Evaporator or equivalent machine at a vacuum of 50 &#181;Torr, evaporate 200 nm of aluminum on the wafer at 5 &#197;/sec. To replicate the presented results, position the wafer constellation 65 cm above the aluminum crucible.</li>
	<li>Spin on 30 drops of a positive photo resi...

<ol>
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The design of each device has two critical steps, proton exchange and development of the LOR. Of the two, proton exchange time determines the depth of the waveguide, which in turn determines the number of guided to leaky mode transitions, the controllable frequency bandwidth, and every key design parameter for each color of light. Two guided modes in red is desired. If more exist then bandwidth is sacrificed. If less exist then no guided to leaky mode transition is guaranteed. Follow the note in step 2.2.1 to correct pro...

Most holographic display technologies, such as pixelated light valves as well as MEMs devices and bulk wave acousto-optic modulators, are too complex to allow for broad participation in their development. Pixelated modulators, especially those with filter layers and active back planes may require dozens of patterning steps to build5 and may be limited by fan-out6. The greater the number of patterning steps the higher the device complexity, and the tighter the fabrication protocol must be to achieve reasonable device yield7. Bulk-wave acousto-optic modulators do not lend themselves to wafer based processes8,9. Anisotropic leaky mode modulators, however, require only two patterning steps to fabricate and utilize relatively standard microfabrication techniques10,11. The accessibility of these processes make it possible for any institution with modest fabrication facilities to participate in the development of holographic video display technology12.
The simplicity of device fabrication can be beguiling, however, as the proper function of the devices is strongly dependent upon waveguides which must be carefully measured and adjusted to achieve the desired device characteristics. For example, if the waveguide is too deep, the device&#39;s operational bandwidth will be narrowed13. If the wave guide is too shallow, the device may not work for red illumination. If the waveguide is annealed too long, the shape of the waveguide&#39;s depth profile will be distorted, and the red, green and blue transitions may not sit adjacent in the frequency domain14. In this work the authors present the tools and techniques to perform this characterization.
The leaky mode modulator consists of a proton exchanged waveguide indiffused on the surface of a piezoelectric, x-cut lithium niobate substrate15,16. At one end of the waveguide is an aluminum interdigital transducer, see Figure 1. Light is introduced into the waveguide using a prism coupler17. The transducer then launches surface acoustic waves which interact contralinearly with light in the waveguide along the y-axis. This interaction couples guided light into a leaky mode which leaks out of the waveguide into the bulk and finally exits the substrate from the edge face18,19. This interaction also rotates the polarization from TE polarized guided light to TM polarized leaky mode light. The surface acoustic wave pattern is the hologram, and it is capable of scanning and shaping the output light to form a holographic image.
The waveguide is created by proton exchange. First, aluminum is deposited on the substrate. Then the aluminum is patterned photo-lithographically and etched to expose regions of the substrate to become waveguide channels. The remaining aluminum acts as a hard mask. The substrate is immersed in a melt of benzoic acid which alters the surface index in the exposed regions. The device is removed, cleaned and annealed in a muffle furnace. The final depth of the waveguide determines the number of leaky mode transitions. The waveguide depth also determines the frequency of each guided-to-mode transitions for each color4.
The aluminum transducers are formed by liftoff. After waveguides are formed, an E-beam resist is spun onto the substrate. An interdigital transducer is patterned with an electron beam to form a chirped transducer designed to respond to the 200 MHz band responsible for controlling color in waveguide devices. The finger period is determined by &#923;&#402; = v where, &#923;, is the finger period, v, is the velocity of sound in the substrate and, &#402;, is the radio frequency (RF). The transducer will have an impedance that must be matched to 75 ohms for efficient operation20.
The guided to leaky mode interaction occurs at different frequencies for different wavelengths of illumination light and as a result red, green, and blue light can be controlled in the frequency domain. The surface acoustic wave pattern is generated by an RF signal sent to the interdigital transducer. The RF of the input signal translate to spatial frequencies on the surface acoustic wave pattern. The waveguide can be fabricated so that low frequency signals control the angular sweep and amplitude of red light, while middle frequencies control green light and high frequencies control blue light. The authors have identified a set of waveguide parameters that allow all three of these interactions to be separate and adjacent in the frequency domain so that all three colors can be controlled with a single 200 MHz signal which is the maximum bandwidth of commodity graphics processing units (GPUs).
By matching the bandwidth of a GPU channel to that of a leaky mode modulator, the system becomes fully parallel and highly scalable. By adding bandwidth matched pairs of GPUs and leaky mode modulator channels, one may construct holographic displays of arbitrary size.
After the device is created, it is carefully characterized to verify that the frequencies for guided-to-leaky mode transition are appropriate for frequency control of color. First, the location of the guided modes are determined by a commercial prism coupler to confirm that the waveguide has the appropriate depth and the correct number of guided modes. Then, after the devices are mounted and packaged, they are placed in a custom prism coupler which maps the input frequencies of the scanned output light. The resulting data gives the frequency input response and the angular output response for red, green, and blue light for the device to be tested. If the device has been fabricated correctly, the device input response will be separated in frequency and the output response will be overlapping in angle. When this is confirmed, the device is ready for use in a holographic video display.
The first measurements take place before the device has been packaged. The waveguide depth is determined by a commercial prism coupler. This can be accomplished with just one illumination wavelength (typically 632 nm red) but authors have modified their commercial prism coupler to allow it to gather mode information for red, green and blue light. After packaging, the device undergoes a second measurement in a custom prism coupler which records deflected output light as a function of input RF. A detailed description of these measurements follows. Fabrication steps are also given.

<table border="0" cellpadding="0" cellspacing="0" width="921">
	<tbody>
		<tr height="40">
			<td height="40" style="height:40px;width:243px;">X-Cut Lithium Niobate</td>
			<td style="width:143px;">Gooch and Housego</td>
			<td style="width:147px;">99-00630-01</td>
			<td style="width:391px;">Lithium Niobate 3&#8243; Diameter X-CUT Wafer 1mm Polish/Polish</td>
		</tr>
		<tr height="40">
			<td height="40" style="height:40px;width:243px;">Positive Photo Resist 1</td>
			<td style="width:143px;">EMD Performance Materials</td>
			<td style="width:147px;">AZ 3330 F Photoresist</td>
			<td style="width:391px;">Used in the creation of the proton exchange mask.</td>
		</tr>
		<tr height="40">
			<td height="40" style="height:40px;width:243px;">Photoresist Developer</td>
			<td style="width:143px;">EMD Performance Materials</td>
			<td style="width:147px;">AZ MIF 300</td>
			<td style="width:391px;">Develops AZ3330 and LOR 3A</td>
		</tr>
		<tr height="40">
			<td height="40" style="height:40px;width:243px;">Aluminium</td>
			<td style="width:143px;">International Advanced Materials</td>
			<td style="width:147px;">AL13</td>
			<td style="width:391px;">99.999% Pure</td>
		</tr>
		<tr height="40">
			<td height="40" style="height:40px;width:243px;">Aluminium Etch</td>
			<td style="width:143px;">Transene</td>
			<td style="width:147px;">Type A Aluminum Etchant</td>
			<td style="width:391px;"></td>
		</tr>
		<tr height="20">
			<td height="20" style="height:20px;width:243px;">Benzoic Acid</td>
			<td style="width:143px;">Sigma Aldrich</td>
			<td style="width:147px;">109479-500G</td>
			<td style="width:391px;">99% Pure</td>
		</tr>
		<tr height="20">
			<td height="20" style="height:20px;width:243px;">Acetone</td>
			<td style="width:143px;">Fisher Chemical</td>
			<td style="width:147px;">UN1009</td>
			<td style="width:391px;"></td>
		</tr>
		<tr height="20">
			<td height="20" style="height:20px;width:243px;">IPA</td>
			<td style="width:143px;">Fisher Chemical</td>
			<td style="width:147px;">UN1219</td>
			<td style="width:391px;">99.5% pure Isopropyl Alcohol</td>
		</tr>
		<tr height="20">
			<td height="20" style="height:20px;width:243px;">Acidic Piranha etch</td>
			<td style="width:143px;">Cyantek Corperation</td>
			<td style="width:147px;">Nanostrip</td>
			<td style="width:391px;"></td>
		</tr>
		<tr height="20">
			<td height="20" style="height:20px;width:243px;">Under Layer Resist</td>
			<td style="width:143px;">Micro Chem</td>
			<td style="width:147px;">LOR 3A</td>
			<td style="width:391px;">Bottom layer used for liftoff.</td>
		</tr>
		<tr height="20">
			<td height="20" style="height:20px;width:243px;">Positive Photo Resist</td>
			<td style="width:143px;">Micro Chem</td>
			<td style="width:147px;">950 PMMA A9</td>
			<td style="width:391px;">Top layer used for liftoff</td>
		</tr>
		<tr height="20">
			<td height="20" style="height:20px;width:243px;">Anisole</td>
			<td style="width:143px;">Micro Chem</td>
			<td style="width:147px;">A Thinner</td>
			<td style="width:391px;"></td>
		</tr>
		<tr height="40">
			<td height="40" style="height:40px;width:243px;">Conductive polymer aqueous solution</td>
			<td style="width:143px;">Mitsubishi Rayon Company</td>
			<td style="width:147px;">AquaSAVE</td>
			<td style="width:391px;"></td>
		</tr>
		<tr height="20">
			<td height="20" style="height:20px;width:243px;">MIBK (4-Methyl-2-pentanone)</td>
			<td style="width:143px;">Sigma Aldrich</td>
			<td style="width:147px;">360511</td>
			<td style="width:391px;">Develops PMMA</td>
		</tr>
		<tr height="20">
			<td height="20" style="height:20px;width:243px;">NMP (1-methyl-2-pyrrolidone)</td>
			<td style="width:143px;">Sigma Aldrich</td>
			<td style="width:147px;">328634</td>
			<td style="width:391px;">Used for liftoff</td>
		</tr>
		<tr height="21">
			<td height="21" style="height:21px;width:243px;">Name of the Equipment</td>
			<td style="width:143px;">Company</td>
			<td style="width:147px;">Catalog Number</td>
			<td style="width:391px;">Comments/ Description</td>
		</tr>
		<tr height="20">
			<td height="20" style="height:20px;width:243px;">E-beam Evaporator&#160;</td>
			<td style="width:143px;">Denton Vacuum&#160;</td>
			<td style="width:147px;">Integrity 20</td>
			<td style="width:391px;">Any equivalent equipment would suffice.</td>
		</tr>
		<tr height="40">
			<td height="40" style="height:40px;width:243px;">Thin Film Spinner</td>
			<td style="width:143px;">Laurell Technologies Corporation</td>
			<td style="width:147px;">WS-400A-6NPP-LITE</td>
			<td style="width:391px;">Any equivalent equipment would suffice.</td>
		</tr>
		<tr height="20">
			<td height="20" style="height:20px;width:243px;">Mask Aligner&#160;</td>
			<td style="width:143px;">Karl Suss America Inc.</td>
			<td style="width:147px;">MA 150 CC</td>
			<td style="width:391px;">Any equivalent equipment would suffice.</td>
		</tr>
		<tr height="20">
			<td height="20" style="height:20px;width:243px;">Automatic Dicing Saw&#160;</td>
			<td style="width:143px;">Disco Corperation</td>
			<td style="width:147px;">Disco Dad 320</td>
			<td style="width:391px;">Any equivalent equipment would suffice.</td>
		</tr>
		<tr height="20">
			<td height="20" style="height:20px;width:243px;">Muffle Furnace</td>
			<td style="width:143px;">Thermo Scientific</td>
			<td style="width:147px;">FB1415M</td>
			<td style="width:391px;">Any equivalent equipment would suffice.</td>
		</tr>
		<tr height="20">
			<td height="20" style="height:20px;width:243px;">Electron Microscope</td>
			<td style="width:143px;">FEI</td>
			<td style="width:147px;">XL30 ESEM</td>
			<td style="width:391px;">Any equivalent equipment would suffice.</td>
		</tr>
		<tr height="40">
			<td height="40" style="height:40px;width:243px;">Dehydration Oven</td>
			<td style="width:143px;">Lab-Line Instruments&#160;</td>
			<td style="width:147px;">Ultra-Clean 100&#160; (3497M-3)</td>
			<td style="width:391px;">Any equivalent equipment would suffice.</td>
		</tr>
		<tr height="20">
			<td height="20" style="height:20px;width:243px;">Hot Plate</td>
			<td style="width:143px;">Thermo Scientific</td>
			<td style="width:147px;">SP131325</td>
			<td style="width:391px;">Any equivalent equipment would suffice.</td>
		</tr>
		<tr height="40">
			<td height="40" style="height:40px;width:243px;">Polisher</td>
			<td style="width:143px;">Ultra Tec Mfg., Inc.</td>
			<td style="width:147px;">Ultrapol End &#38; Edge Polisher</td>
			<td style="width:391px;">Any equivalent equipment would suffice.</td>
		</tr>
		<tr height="40">
			<td height="40" style="height:40px;width:243px;">Class IIIb 12V RBG Lasers: Wavelengths(nm): 638, 532, and 445</td>
			<td style="width:143px;"></td>
			<td style="width:147px;"></td>
			<td style="width:391px;">Bought second-hand. Probably pulled from a laser projector. Any equivalent equipment would suffice.</td>
		</tr>
		<tr height="60">
			<td height="60" style="height:60px;width:243px;">Signal Generator</td>
			<td style="width:143px;">Agilent</td>
			<td style="width:147px;">8648D</td>
			<td style="width:391px;">Now found at Keysight. Obsolete. Any equivalent equipment would suffice. Needed Frequency sweep 9 KHz-1000 MHz.</td>
		</tr>
		<tr height="40">
			<td height="40" style="height:40px;width:243px;">Signal Amplifier</td>
			<td style="width:143px;">Mini-Circuits</td>
			<td style="width:147px;">TB-17</td>
			<td style="width:391px;">Necessary only to overcome the limitations of the signal generator.</td>
		</tr>
		<tr height="40">
			<td height="40" style="height:40px;width:243px;">Power Meter Controller</td>
			<td style="width:143px;">ThorLabs</td>
			<td style="width:147px;">PM100D</td>
			<td style="width:391px;">With power meter model S130C. Any equivalent equipment would suffice. Needed sensitivity 500pW</td>
		</tr>
		<tr height="40">
			<td height="40" style="height:40px;width:243px;">Linear Actuator Controller</td>
			<td style="width:143px;">Newport</td>
			<td style="width:147px;">ESP7000</td>
			<td style="width:391px;">With linear actuator model MFN25PP. Any equivalent equipment would suffice. Needs 0.1mm accuracy.</td>
		</tr>
		<tr height="40">
			<td height="40" style="height:40px;width:243px;">AutomatedDeviceCharacterization.vi&#160;</td>
			<td style="width:143px;">LabView</td>
			<td style="width:147px;">Experimental Control Software by BYU</td>
			<td style="width:391px;">Found in the appendix</td>
		</tr>
		<tr height="40">
			<td height="40" style="height:40px;width:243px;">CompareWDMmodes.m</td>
			<td style="width:143px;">MATLab</td>
			<td style="width:147px;">Analytical Software by BYU</td>
			<td style="width:391px;">Found in the appendix</td>
		</tr>
	</tbody>
</table>

characterization of anisotropic leaky mode modulators for holovideo

Holovideo displays are based on light-bending spatial light modulators. One such spatial light modulator is the anisotropic leaky mode modulator. This modulator is particularly well suited for holographic video experimentation as it is relatively simple and inexpensive to fabricate1-3. Some additional advantages of leaky mode devices include: large aggregate bandwidth, polarization separation of signal light from noise, large angular deflection and frequency control of color1. In order to realize these advantages, it is necessary to be able to adequately characterize these devices as their operation is strongly dependent on waveguide and transducer parameters4. To characterize the modulators, the authors use a commercial prism coupler as well as a custom characterization apparatus to identify guided modes, calculate waveguide thickness and finally to map the device's frequency input and angular output of leaky mode modulators. This work gives a detailed description of the measurement and characterization of leaky mode modulators suitable for full-color holographic video.

The principle results of the protocol above are the guided mode measurement from the commercial prism coupler shown in Figure 2, the single frequency, raw input/output data gathered from the customized prism coupler shown in Figure 8 and the multicolor curves shown in Figure 9. In the following paragraphs we discuss the actionable information produced by each of these outputs.
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Characterization of Anisotropic Leaky Mode Modulators for Holovideo

This work describes fabrication and characterization of anisotropic leaky mode modulators for holographic video.

Holovideo displays are based on light-bending spatial light modulators.  One such spatial light modulator is the anisotropic leaky mode modulator.  This ...

The overall goal of this procedure is to reproducibly characterize spatial-light modulators by mapping their frequency response to angular output. This method helps to provide vital data required to answering key questions in the electroholography field, such as identifying guided leaky mode transitions and optimization requirements. The main advantage of this technique is that it clearly separates leaky mode transitions and allows us to quickly obtain repeatable information on their linearity, relative intensity, angular spread, and operational frequency.A visual demonstration of this process is critical as the alignment and the prism coupling both rely on visual cues that are hard to explain. To characterize the device, first prepare to mount it on a radio frequency breakout board. Have ready a device, an RF breakout board, and three glass slides to make a mounting platform.One slide is larger than the other two. It will form the base of the U-shaped platform. Begin to work with the largest slide.Place a generous bead of superglue over the left-most quarter of a slide's longest dimension. Next, orient a smaller slide so that its longest dimension is perpendicular to that of the first slide. Align the left edges of the two slides so that their lower-left corners overlap.Put them in contact and apply firm and equal pressure to the slides until the glue sets. Repeat the analogous steps for the right-hand side. This will result in a U-shaped structure.To mount the device, apply double-sided tape to the platform at the center of the U.Now, work with the leaky mode modulator to be characterized. Check that the device has polished ends and is ready for use. Next, place the device on top of the tape that is already on the platform.Mount it so the end of the device overhangs the end of the mounting platform to avoid interfering with the light path. At this point, mount the RF breakout board. Mount the breakout board so that it is not in the beam path of the light exiting the device.The next step is wire bonding. This is the device and breakout board after they have been wire bonded. Now, select an appropriate prism to cut the light into the device and use isopropyl alcohol to clean the surface that will be in contact with the device.In addition, clean the contact surface of the device. Then, place the prism on the device so that it is centered on the device channel to be tested. Continue by using a clamping mechanism to press the bottom of the prism firmly against the top of the device, coupling the elements.The clamping mechanism should press the bottom of the prism firmly against the top of the device and successful coupling will produce a wet spot at the interface. When viewed at the proper angle, the wet spot will reflect a rainbow of color. The next step is to make use of the characterization apparatus.The apparatus has three laser sources, red, green, and blue, at one end. Light from the lasers first passes through a variable attenuator, then a half-wave plate, followed by a variable aperture, and finally, a focusing lens. The focused light falls upon the prism on the sample which will be mounted on this rotation stage.This schematic provides an overview of the optical elements, the rotation stage, and the electronics. Once light has entered the device, input of a radio frequency signal generates surface acoustic waves. These cause light to exit at a frequency controllable angle and fall on a power meter.Configure the instruments to collect data over a range of frequencies and positions. Mount the device with the prism and holder on the rotation platform. Place the assembly so that light from the focusing lens first encounters the prism.To align the device, first turn on the laser, and adjust the attenuator until the intensity of the scattered light is comfortable to the eye. Next, place a polarizer in the beam path after the half-wave plate. Orient it so that it blocks horizontally polarized light.Rotate the half-wave plate to achieve maximum attenuation of the laser light. One this is achieved, remove the polarizer. Now, return to the rotation platform to manually rotate it.Adjust it so the laser light is at the proper entrance angle with respect to the top surface of the device. Align the prism using the linear translation stage on top of the rotation stage. Adjust the alignment until the focal point of the laser light passes through the 90-degree corner of the prism.At this point, make fine adjustments to the rotation stage to achieve coupling. Monitor the device. As the wave guide begins to couple, a characteristic streak of light appears in the wave guide from scattering.Another way to verify coupling is to have light exiting the device fall onto a back plane. On the back plane, confirm the presence of characteristic mode lines of the light. These are various transverse electric modes.Once coupling is detected, fine tune the rotation and translation stages to increase the evanescent coupling. Next, ready the cable that connects the breakout board to the amplifier and signal generator. Make the connection to the signal input of the breakout board.Continue by turning on both the radio frequency signal generator and the amplifier. Here it is useful to do a preliminary test of the device. Sweep the frequency from 400 megahertz to 600 megahertz and check for deflected light.Before continuing, clear the beam path and ensure the power meter is in place. Then, return to the attenuator in the optical path. There, undo any attentuation that was implemented for safety during alignment.Finally, use an optically isolating box to cover the entire characterization apparatus for the duration of the experiment. Make use of instrument control software to run the characterization apparatus. This experiment uses lab view, running a custom testing program.After entering the testing parameters, run the program. The script should take less than five minutes to run. During testing, it will produce a plot which can be manipulated.Both the plot and the data will be saved. This data collected before the device was packaged, is for a commercial thin film analyzer. The vertical axis is laser intensity.The horizontal axis is a measure of the rotation of the device. The two dips correspond to angles at which a guided mode allows light to enter the wave guide and exit at the end of the device, thus avoiding reflection into the power meter. This optical power data, collected after packaging, is from the characterization apparatus.The plot is the result of scanning the radio frequency input in megahertz and power meter location in millimeters. The projection of the data on the Y-axis gives the frequency response of the device. Projection on the X-axis gives the span of the diffracted light output.The slope of the data in the XY plane provides a sense of the scan's linearity. This plot combines raw data from several experiments in all three wavelengths for TE 1 guided modes. If the response for each color is adjacent in frequency and overlapping in angle, the device is appropriate for frequency control of color.Once mastered, a full characterization in red, green, and blue light for a single channel takes 30 minutes. Of course, high resolution images take more time. After its development, this technique paved the way for researchers in the field of electroholography to explore frequency division multiplexing in wave guiding spatial light modulators.After watching this video, you should have a good understanding of how to characterize spatial modulators in a repeatable way. This includes proper prism coupling, alignment and testing procedures.

characterization-of-anisotropic-leaky-mode-modulators-for-holovideo

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Engineering

Development of Whispering Gallery Mode Polymeric Micro-optical Electric Field Sensors

Optical modes of dielectric micro-cavities have received significant attention in recent years for their potential in a broad range of applications. The optical modes are frequently referred to as "whispering gallery modes" (WGM) or "morphology dependent resonances" (MDR) and exhibit high optical quality factors. Some proposed applications of micro-cavity optical resonators are in spectroscopy1, micro-cavity laser technology2, optical communications3-6 as well as sensor technology. The WGM-based sensor applications include those in biology7, trace gas detection8, and impurity detection in liquids9. Mechanical sensors based on microsphere resonators have also been proposed, including those for force10,11, pressure12, acceleration13 and wall shear stress14. In the present, we demonstrate a WGM-based electric field sensor, which builds on our previous studies15,16. A candidate application of this sensor is in the detection of neuronal action potential.
The electric field sensor is based on polymeric multi-layered dielectric microspheres. The external electric field induces surface and body forces on the spheres (electrostriction effect) leading to elastic deformation. This change in the morphology of the spheres, leads to shifts in the WGM. The electric field-induced WGM shifts are interrogated by exciting the optical modes of the spheres by laser light. Light from a distributed feedback (DFB) laser (nominal wavelength of ~ 1.3 &mu;m) is side-coupled into the microspheres using a tapered section of a single mode optical fiber. The base material of the spheres is polydimethylsiloxane (PDMS). Three microsphere geometries are used: (1) PDMS sphere with a 60:1 volumetric ratio of base-to-curing agent mixture, (2) multi layer sphere with 60:1 PDMS core, in order to increase the dielectric constant of the sphere, a middle layer of 60:1 PDMS that is mixed with varying amounts (2% to 10% by volume) of barium titanate and an outer layer of 60:1 PDMS and (3) solid silica sphere coated with a thin layer of uncured PDMS base. In each type of sensor, laser light from the tapered fiber is coupled into the outermost layer that provides high optical quality factor WGM (Q ~ 106). The microspheres are poled for several hours at electric fields of ~ 1 MV/m to increase their sensitivity to electric field.

A high-sensitivity photonic micro sensor was developed for electric field detection. The sensor exploits the optical modes of a dielectric sphere. Changes in the external electric field perturb the sphere morphology leading to shifts in its optical modes. The electric field strength is measured by monitoring these optical shifts.

Optical modes of dielectric micro-cavities have received significant attention in recent years for their potential in a broad range of applications. The ...

Microwave Photonics Systems Based on Whispering-gallery-mode Resonators

Microwave photonics systems rely fundamentally on the interaction between microwave and optical signals. These systems are extremely promising for various areas of technology and applied science, such as aerospace and communication engineering, sensing, metrology, nonlinear photonics, and quantum optics. In this article, we present the principal techniques used in our lab to build microwave photonics systems based on ultra-high Q whispering gallery mode resonators. First detailed in this article is the protocol for resonator polishing, which is based on a grind-and-polish technique close to the ones used to polish optical components such as lenses or telescope mirrors. Then, a white light interferometric profilometer measures surface roughness, which is a key parameter to characterize the quality of the polishing. In order to launch light in the resonator, a tapered silica fiber with diameter in the micrometer range is used. To reach such small diameters, we adopt the "flame-brushing" technique, using simultaneously computer-controlled motors to pull the fiber apart, and a blowtorch to heat the fiber area to be tapered. The resonator and the tapered fiber are later approached to one another to visualize the resonance signal of the whispering gallery modes using a wavelength-scanning laser. By increasing the optical power in the resonator, nonlinear phenomena are triggered until the formation of a Kerr optical frequency comb is observed with a spectrum made of equidistant spectral lines. These Kerr comb spectra have exceptional characteristics that are suitable for several applications in science and technology. We consider the application related to ultra-stable microwave frequency synthesis and demonstrate the generation of a Kerr comb with GHz intermodal frequency.

The customized techniques developed in our lab to build microwave photonics systems based on ultra-high Q whispering gallery mode resonators are presented. The protocols to obtain and characterize these resonators are detailed, and an explanation of some of their applications in microwave photonics is given.

Microwave photonics systems rely fundamentally on the interaction between microwave and optical signals. These systems are extremely promising for various ...

Construction and Characterization of External Cavity Diode Lasers for Atomic Physics

Since their development in the late 1980s, cheap, reliable external cavity diode lasers (ECDLs) have replaced complex and expensive traditional dye and Titanium Sapphire lasers as the workhorse laser of atomic physics labs1,2. Their versatility and prolific use throughout atomic physics in applications such as absorption spectroscopy and laser cooling1,2 makes it imperative for incoming students to gain a firm practical understanding of these lasers. This publication builds upon the seminal work by Wieman3, updating components, and providing a video tutorial. The setup, frequency locking and performance characterization of an ECDL will be described. Discussion of component selection and proper mounting of both diodes and gratings, the factors affecting mode selection within the cavity, proper alignment for optimal external feedback, optics setup for coarse and fine frequency sensitive measurements, a brief overview of laser locking techniques, and laser linewidth measurements are included.

This is an instructional paper to guide the construction and diagnostics of external cavity diode lasers (ECDLs), including component selection and optical alignment, as well as the basics of frequency reference spectroscopy and laser linewidth measurements for applications in the field of atomic physics.

Since their development in the late 1980s, cheap, reliable external cavity diode lasers (ECDLs) have replaced complex and expensive traditional dye and ...

Mechanical Expansion of Steel Tubing as a Solution to Leaky Wellbores

Wellbore cement, a procedural component of wellbore completion operations, primarily provides zonal isolation and mechanical support of the metal pipe (casing), and protects metal components from corrosive fluids. These are essential for uncompromised wellbore integrity. Cements can undergo multiple forms of failure, such as debonding at the cement/rock and cement/metal interfaces, fracturing, and defects within the cement matrix. Failures and defects within the cement will ultimately lead to fluid migration, resulting in inter-zonal fluid migration and premature well abandonment. Currently, there are over 1.8 million operating wells worldwide and over one third of these wells have leak related problems defined as Sustained Casing Pressure (SCP)1. 
The focus of this research was to develop an experimental setup at bench-scale to explore the effect of mechanical manipulation of wellbore casing-cement composite samples as a potential technology for the remediation of gas leaks. 
The experimental methodology utilized in this study enabled formation of an impermeable seal at the pipe/cement interface in a simulated wellbore system. Successful nitrogen gas flow-through measurements demonstrated that an existing microannulus was sealed at laboratory experimental conditions and fluid flow prevented by mechanical manipulation of the metal/cement composite sample. Furthermore, this methodology can be applied not only for the remediation of leaky wellbores, but also in plugging and abandonment procedures as well as wellbore completions technology, and potentially preventing negative impacts of wellbores on subsurface and surface environments.

This article reports on a laboratory scale investigation of an existing field procedure and its adaptation for sealing of leaky wellbores. It consists of mechanical expansion of metal pipe, which results in an improved metal/cement bond, ultimate sealing of hydraulic pathways and prevention of gas leaks caused by the presence of a microannular channel.

Wellbore cement, a procedural component of wellbore completion operations, primarily provides zonal isolation and mechanical support of the metal pipe ...

Electron Channeling Contrast Imaging for Rapid III-V Heteroepitaxial Characterization

Misfit dislocations in heteroepitaxial layers of GaP grown on Si(001) substrates are characterized through use of electron channeling contrast imaging (ECCI) in a scanning electron microscope (SEM). ECCI allows for imaging of defects and crystallographic features under specific diffraction conditions, similar to that possible via plan-view transmission electron microscopy (PV-TEM). A particular advantage of the ECCI technique is that it requires little to no sample preparation, and indeed can use large area, as-produced samples, making it a considerably higher throughput characterization method than TEM. Similar to TEM, different diffraction conditions can be obtained with ECCI by tilting and rotating the sample in the SEM. This capability enables the selective imaging of specific defects, such as misfit dislocations at the GaP/Si interface, with high contrast levels, which are determined by the standard invisibility criteria. An example application of this technique is described wherein ECCI imaging is used to determine the critical thickness for dislocation nucleation for GaP-on-Si by imaging a range of samples with various GaP epilayer thicknesses. Examples of ECCI micrographs of additional defect types, including threading dislocations and a stacking fault, are provided as demonstration of its broad, TEM-like applicability. Ultimately, the combination of TEM-like capabilities &#8211; high spatial resolution and richness of microstructural data &#8211; with the convenience and speed of SEM, position ECCI as a powerful tool for the rapid characterization of crystalline materials.

The use of electron channeling contrast imaging in a scanning electron microscope to characterize defects in III-V/Si heteroexpitaxial thin films is described. This method yields similar results to plan-view transmission electron microscopy, but in significantly less time due to lack of required sample preparation.

Misfit dislocations in heteroepitaxial layers of GaP grown on Si(001) substrates are characterized through use of electron channeling contrast imaging ...

Automation of Mode Locking in a Nonlinear Polarization Rotation Fiber Laser through Output Polarization Measurements

When a laser is mode-locked, it emits a train of ultra-short pulses at a repetition rate determined by the laser cavity length. This article outlines a new and inexpensive procedure to force mode locking in a pre-adjusted nonlinear polarization rotation fiber laser. This procedure is based on the detection of a sudden change in the output polarization state when mode locking occurs. This change is used to command the alignment of the intra-cavity polarization controller in order to find mode-locking conditions. More specifically, the value of the first Stokes parameter varies when the angle of the polarization controller is swept and, moreover, it undergoes an abrupt variation when the laser enters the mode-locked state. Monitoring this abrupt variation provides a practical easy-to-detect signal that can be used to command the alignment of the polarization controller and drive the laser towards mode locking. This monitoring is achieved by feeding a small portion of the signal to a polarization analyzer measuring the first Stokes parameter. A sudden change in the read out of this parameter from the analyzer will occur when the laser enters the mode-locked state. At this moment, the required angle of the polarization controller is kept fixed. The alignment is completed. This procedure provides an alternate way to existing automating procedures that use equipment such as an optical spectrum analyzer, an RF spectrum analyzer, a photodiode connected to an electronic pulse-counter or a nonlinear detecting scheme based on two-photon absorption or second harmonic generation. It is suitable for lasers mode locked by nonlinear polarization rotation. It is relatively easy to implement, it requires inexpensive means, especially at a wavelength of 1550 nm, and it lowers the production and operation costs incurred in comparison to the above-mentioned techniques.

A protocol to detect and automate mode locking in a pre-adjusted nonlinear polarization rotation fiber laser is presented. The detection of a sudden change in the output polarization state when mode locking occurs is used to command the alignment of an intra-cavity polarization controller in order to find mode-locking conditions.

When a laser is mode-locked, it emits a train of ultra-short pulses at a repetition rate determined by the laser cavity length. This article outlines a ...

Stimulated Stokes and Antistokes Raman Scattering in Microspherical Whispering Gallery Mode Resonators

Dielectric microspheres can confine light and sound for a length of time through high quality factor whispering gallery modes (WGM). Glass microspheres can be thought as a store of energy with a huge variety of applications: compact laser sources, highly sensitive biochemical sensors and nonlinear phenomena. A protocol for the fabrication of both the microspheres and coupling system is given. The couplers described here are tapered fibers. Efficient generation of nonlinear phenomena related to third order optical non-linear susceptibility &#935;(3) interactions in triply resonant silica microspheres is presented in this paper. The interactions here reported are: Stimulated Raman Scattering (SRS), and four wave mixing processes comprising Stimulated Anti-stokes Raman Scattering (SARS). A proof of the cavity-enhanced phenomenon is given by the lack of correlation among the pump, signal and idler: a resonant mode has to exist in order to obtain the pair of signal and idler. In the case of hyperparametric oscillations (four wave mixing and stimulated anti-stokes Raman scattering), the modes must fulfill the energy and momentum conservation and, last but not least, have a good spatial overlap.

Efficient generation of nonlinear phenomena related to third order optical non-linear susceptibility &#935;(3) interactions in triply resonant silica microspheres is presented in this paper. The interactions here reported are: Stimulated Raman Scattering (SRS), and four wave mixing processes comprising Stimulated Anti-stokes Raman Scattering (SARS).

Dielectric microspheres can confine light and sound for a length of time through high quality factor whispering gallery modes (WGM). Glass microspheres ...

Characterization of Ultra-fine Grained and Nanocrystalline Materials Using Transmission Kikuchi Diffraction

One of the challenges in microstructure analysis nowadays resides in the reliable and accurate characterization of ultra-fine grained (UFG) and nanocrystalline materials. The traditional techniques associated with scanning electron microscopy (SEM), such as electron backscatter diffraction (EBSD), do not possess the required spatial resolution due to the large interaction volume between the electrons from the beam and the atoms of the material. Transmission electron microscopy (TEM) has the required spatial resolution. However, due to a lack of automation in the analysis system, the rate of data acquisition is slow which limits the area of the specimen that can be characterized. This paper presents a new characterization technique, Transmission Kikuchi Diffraction (TKD), which enables the analysis of the microstructure of UFG and nanocrystalline materials using an SEM equipped with a standard EBSD system. The spatial resolution of this technique can reach 2 nm. This technique can be applied to a large range of materials that would be difficult to analyze using traditional EBSD. After presenting the experimental set up and describing the different steps necessary to realize a TKD analysis, examples of its use on metal alloys and minerals are shown to illustrate the resolution of the technique and its flexibility in term of material to be characterized.

This paper provides a detailed method to characterize the microstructure of ultra-fine grained and nanocrystalline materials using a scanning electron microscope equipped with a standard electron backscatter diffraction system. Metal alloys and minerals presenting refined microstructures are analyzed using this technique, showing the diversity of its possible applications.

One of the challenges in microstructure analysis nowadays resides in the reliable and accurate characterization of ultra-fine grained (UFG) and ...

A Novel Method for In Situ Electromechanical Characterization of Nanoscale Specimens

Electrically assisted deformation (EAD) is increasingly being used to improve the formability of metals during processes such as sheet metal rolling and forging. Adoption of this technique is proceeding despite disagreement concerning the underlying mechanism responsible for EAD. The experimental procedure described herein enables a more explicit study compared to previous EAD research by removing thermal effects, which are responsible for disagreement in interpreting previous EAD results. Furthermore, as the procedure described here enables EAD observation in situ and in real time in a transmission electron microscope (TEM), it is superior to existing post-mortem methods that observe EAD effects post-test. Test samples consist of a single crystal copper (SCC) foil having a free-standing tensile test section of nanoscale thickness, fabricated using a combination of laser and ion beam milling. The SCC is mounted to an etched silicon base that provides mechanical support and electrical isolation while serving as a heat sink. Using this geometry, even at high current density (~3,500 A/mm2), the test section experiences a negligible temperature increase (&#60;0.02 &#176;C), thus eliminating Joule heating effects. Monitoring material deformation and identifying the corresponding changes to microstructures, e.g. dislocations, are accomplished by acquiring and analyzing a series of TEM images. Our sample preparation and in situ experiment procedures are robust and versatile as they can be readily utilized to test materials with different microstructures, e.g., single and polycrystalline copper.

A Novel Method for In Situ Electromechanical Characterization of Nanoscale Specimens

Isolating electrical and thermal effects on electrically assisted deformation (EAD) is very difficult using macroscopic samples. Metallic sample micro- and nanostructures together with a custom test procedure have been developed to evaluate the impact of applied current on the formation without joule heating and evolution of dislocations on these samples.

Electrically assisted deformation (EAD) is increasingly being used to improve the formability of metals during processes such as sheet metal rolling and ...

Ultrasonic Fatigue Testing in the Tension-Compression Mode

Ultrasonic fatigue testing is one of a few methods which allow investigating fatigue properties in the ultra-high cycle region. The method is based on exposing the specimen to longitudinal vibrations on its resonance frequency close to 20 kHz. With use of this method, it is possible to significantly decrease the time required for the test, when compared to conventional testing devices usually working at frequencies under 200 Hz. It is also used to simulate loading of material during operation in high speed conditions, such as those experienced by components of jet engines or car turbo pumps. It is necessary to operate only in the high and ultra-high cycle region, due to the possibility of extremely high deformation rates, which can have a significant influence on the test results. Specimen shape and dimensions have to be carefully selected and calculated to fulfill the resonance condition of the ultrasonic system; thus, it is not possible to test the full components or specimens of arbitrary shape. Before each test, it is necessary to harmonize the specimen with the frequency of the ultrasonic system to compensate for deviations of the real shape from the ideal one. It is not possible to run a test until a total fracture of the specimen, since the test is automatically terminated after initiation and propagation of the crack to a certain length, when the stiffness of the system changes enough to shift the system out of the resonance frequency. This manuscript describes the process of evaluation of materials' fatigue properties at high-frequency ultrasonic fatigue loading with use of mechanical resonance at a frequency close to 20 kHz. The protocol includes a detailed description of all steps required for a correct test, including specimen design, stress calculation, harmonizing with the resonance frequency, performing the test, and final static fracture.

A protocol for ultrasonic fatigue testing in the high and ultra-high cycle region in axial tension-compression loading mode.

Ultrasonic fatigue testing is one of a few methods which allow investigating fatigue properties in the ultra-high cycle region. The method is based on ...