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294 Views
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01:28 min
June 23rd, 2023
DOI :
10.3791/200250-v
* These authors contributed equally
Transcript
首先测量23.3毫克H 2 BDC三唑并将其放入闪烁瓶中。为了将H 2BDC配体溶解在水溶液中,使用玻璃移液管将1.0毫升4%氢氧化钾溶液转移到小瓶中。接下来,对混合物进行超声处理,直到所有固体完全溶解。
将一摩尔盐酸溶液加入含脱羧酸的小瓶中并搅拌直至pH值达到7。将33毫克UiO-66 MOF加入闪烁瓶中。然后将小瓶与MOF和配体在室温和120RPM下在摇床中孵育24小时。
接下来,通过以 1166g 离心五分钟从混合物中分离固体 MOF。在室温下。向获得的固体M
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