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DOI :
10.3791/50511-v
April 1st, 2013
Chapters
0:05
Title
2:33
Microwave-assisted Dehydrogenative DA Reaction
4:16
Palladium-catalyzed Cross-coupling Reaction
7:06
Preparation of Dye Solution for Photophysical Studies
7:50
Fluorescence Emission Spectroscopy
8:47
Results: Synthesis and Photophysical Analysis of Functionalized Nephthalenes/Solvatochromic Fluorescent Dyes
11:10
Conclusion
微波辅助分子内的脱氢的Diels-Alder反应(DA)提供简洁的访问功能化环戊[ B]萘积木。一个步骤转换成脱氢DA双环[2.2.2]辛烯酮类化合物的新型溶致变色荧光染料通过布赫瓦尔德-哈特维希钯催化交叉偶联反应证明了这种方法的效用。
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