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10.7K Views
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12:27 min
September 8th, 2013
DOI :
10.3791/50886-v
Chapters
0:00
Title
3:46
Synthesis of Phenyl HIAT
5:35
Synthesis of n-Pentyl HIAT
8:33
O-H insertion cyanocarbene reaction using Phenyl HIAT
10:17
Cylcopropanation cyanocarbene reaction using Phenyl HIAT
11:50
Conclusion
Summary
ここにcyanocarbenesを生成するためのアジドとの合成、単離、および超原子価ヨードアルキトリフ(HIATs)の反応が記載されている。手順は、不活性雰囲気下で低温ろ過などの空気に敏感と寒剤技術を伴う。合成された化合物の取り扱いや安全性も議論される。
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