Name: the evolution of silica nanoparticle-polyester coatings on surfaces exposed to sunlight
Uploaded: 2016-10-11T14:00:00
Description: Watch this Scientific Journal Video about The Evolution of Silica Nanoparticle-polyester Coatings on Surfaces Exposed to Sunlight at JoVE.com

Funding from the Australian Research Council Industrial Transformation Research Hubs Scheme (Project Number IH130100017) is gratefully acknowledged. Authors gratefully acknowledge the RMIT Microscopy and Microanalysis Facility (RMMF) for providing access to the characterisation instruments. This research was also undertaken on the Infrared Microscopectroscopy beamline at the Australian Synchrotron, Victoria, Australia.

<html> 1.钢铁样品<ol><li>从商业供应商获得厚度为1毫米的钢试样。 注：样品涂覆有聚酯或聚酯涂覆有二氧化硅纳米粒子。 </li><li>样品暴露在罗克汉普顿，澳大利亚昆士兰州的阳光：收集了总共5年的时间后，一年期和五年期的时间间隔采样。切样片到用打孔器直径1厘米的圆形光盘。 </li><li>前表面表征，用双蒸水漂洗样品，然后干燥用氮气（99.99％）。保持在所有样品中的气密容?...

<ol>
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聚酯涂料已被广泛地用于保护钢基质从上未涂布表面将发生因水分和污染物的积累的腐蚀。的聚酯涂料的应用可以保护钢免受腐蚀;然而这些涂料的长期效力，如果它们暴露于高水平的潮湿条件下的紫外光，损害作为在热带气候发生。二氧化硅纳米粒子可被施加到聚酯的表面以改善这些环境内的这些涂层的坚固性，对这些含二氧化硅的涂层材料的环境因素然而效果，到现在为止，未知的，特别是关...

Environmental corrosion of metals in the environment is both prevalent and costly1-3. A recent study conducted by the Australasian Corrosion Association (ACA) reported that corrosion of metals resulted in a yearly cost of $982 million, which was directly associated with the degradation of assets and infrastructure through metallic corrosion within the water industry4. From an international perspective, the World Corrosion Organization estimated that metallic corrosion was responsible for a direct cost of $3.3 trillion, over 3% of the world's GDP5. The process of galvanizing as a corrosion preventative method has been widely used to increase the lifespan of steel material6. In humid and subtropical climates, however, water tends to condense into small pockets or grooves within the surface of the galvanized steel, leading to the acceleration of corrosion rates through pit corrosion7,8. Thermosetting polymer coatings based on polyesters have been developed to coat the galvanized steel substrata increasing their ability to withstand humid weathering conditions for items such as satellite dishes, garden furniture, air-conditioning units or agricultural construction equipment9-11. Unfortunately polymer coatings on steel surfaces have been found to be considerably adversely affected by the presence of high levels of ultraviolet (uv) radiation12-14. Coatings comprised of silica nanoparticles (SiO2) spread over a polymer layer have been widely used with a view to increasing their corrosion-, wear-, tear- and degradation-resistance15,16. The tendency of the protective polymeric coatings to form pores and cracks can be reduced by incorporating nanoparticles (NPs), which contribute to the passive obstruction of corrosion initiation17,18. Also, the mechanical stability of the protective polymeric layer can be improved by NPs inclusion. However, these coatings act as passive physical barriers and, in comparison to the galvanization approach, cannot inhibit corrosion propagation actively.
An in-depth understanding of the effect that high-levels of ultraviolet light exposure under humid conditions upon these metal coatings is yet to be obtained. In this paper, a wide range of surface analytical techniques, including X-ray photoelectron spectroscopy (XPS), attenuated total reflection infrared micro-spectroscopy (ATR IR), contact angle goniometry, optical profiling and atomic force microscopy (AFM) will be employed to examine the changes in the surface of steel coatings prepared from polyester- and silica nanoparticle-coated polyester (silica nanoparticles/polyester) after exposure to sunlight. Furthermore, the aim of this work is to give a concise, practical overview of the overall characterization techniques to examine weathered samples.

<table border="0" cellpadding="0" cellspacing="0" width="1044">
	<colgroup>
		<col />
		<col />
		<col />
		<col />
	</colgroup>
	<tbody>
		<tr height="41">
			<td height="41" style="height:41px;width:263px;">polyester-coated steel 
			silica nanoparticle-polyester coated steel substrata</td>
			<td style="width:231px;">BlueScope Steel</td>
			<td style="width:163px;"></td>
			<td style="width:387px;">Samples provided by company</td>
		</tr>
		<tr height="26">
			<td height="26" style="height:26px;width:263px;">Millipore PetriSlideTM&#160;</td>
			<td style="width:231px;">Fisher Scientific</td>
			<td style="width:163px;">PDMA04700</td>
			<td>Storing samples</td>
		</tr>
		<tr height="49">
			<td height="49" style="height:49px;width:263px;">Thermo ScientificTM K-alpha 
			X-ray Photoelectron Spectrometer</td>
			<td>Thermo Fisher Scientific, Inc.</td>
			<td>IQLAADGAAFFACVMAHV</td>
			<td>Acquire XPS spectra</td>
		</tr>
		<tr height="21">
			<td height="21" style="height:21px;width:263px;">Avantage Data System</td>
			<td>Thermo Fisher Scientific, Inc.</td>
			<td>IQLAADGACKFAKRMAVI</td>
			<td>Analyse XPS spectra</td>
		</tr>
		<tr height="21">
			<td height="21" style="height:21px;">A Bruker Hyperion 2000 microscope&#160;</td>
			<td style="width:231px;">Bruker Corporation</td>
			<td style="width:163px;"></td>
			<td>Synchrotron integrated instrument</td>
		</tr>
		<tr height="21">
			<td height="21" style="height:21px;">Bruker Opus v. 7.2</td>
			<td style="width:231px;">Bruker Corporation</td>
			<td style="width:163px;"></td>
			<td>ATR-IR analysis software</td>
		</tr>
		<tr height="21">
			<td height="21" style="height:21px;width:263px;">Contact angle goniometer, FTA1000c</td>
			<td>First Ten &#197;ngstroms Inc., VA, USA</td>
			<td style="width:163px;"></td>
			<td>Measuring the wettability of surfaces</td>
		</tr>
		<tr height="21">
			<td height="21" style="height:21px;width:263px;">FTA v. 2.0</td>
			<td>First Ten &#197;ngstroms Inc., VA, USA</td>
			<td style="width:163px;"></td>
			<td>Anaylyzing water contact angle</td>
		</tr>
		<tr height="21">
			<td height="21" style="height:21px;">Optical profiler, Wyko NT1100&#160;</td>
			<td>Bruker Corporation</td>
			<td style="width:163px;"></td>
			<td>Measure surface topography</td>
		</tr>
		<tr height="21">
			<td height="21" style="height:21px;">Innova atomic force microscope&#160;</td>
			<td>Bruker Corporation</td>
			<td style="width:163px;"></td>
			<td>Measure surface topography</td>
		</tr>
		<tr height="42">
			<td height="42" style="height:42px;width:263px;">Phosphorus doped silicon probes, MPP-31120-10</td>
			<td>Bruker Corporation</td>
			<td style="width:163px;"></td>
			<td>AFM probes</td>
		</tr>
		<tr height="21">
			<td height="21" style="height:21px;">Gwyddion software</td>
			<td style="width:231px;">http://gwyddion.net/</td>
			<td style="width:163px;"></td>
			<td>Software used to measure optical profiling and AFM data</td>
		</tr>
	</tbody>
</table>

the evolution of silica nanoparticle-polyester coatings on surfaces exposed to sunlight

金属表面的腐蚀是在环境中普遍存在，并在许多领域，包括军事，交通，航空，建筑，食品等行业，除其他外的极大关注。聚酯和含有聚酯和二氧化硅纳米粒子的涂层（SiO 2的纳米颗粒）已经被广泛地用于保护钢基质免受腐蚀。在这项研究中，我们利用X射线光电子能谱，衰减全反射红外微光谱，水接触角的测量，光分析和原子力显微镜，以提供深入了解暴露于阳光下如何导致在微米和纳米级的完整性的改变的涂层。使用光学轮廓检测在表面微地形无显著变化，然而，使用原子力显微镜进行检测统计学显著纳米变化到表面。 X射线光电子能谱分析和衰减全反射红外微光谱数据表明，已通过暴露于紫外线光发生酯基的降解以形成COO·，-H 2 C·，-O·， - CO·自由基。在降解过程，CO和CO 2的也被生产。

<html>已被经受暴露于阳光下一个或五年涂覆的钢样品收集，与水的接触角测量进行了决定曝光是否已导致在所述表面的表面疏水性的改变（ 图2 ）。 <img alt="图2" src="/files/ftp_upload/54309/54309fig2.jpg" /> 图2.润湿与聚酯或二氧化硅纳米微粒/聚酯涂料（硅胶/聚酯）在五年内暴露于阳光的表面的变化 （A）的测角的图?...

Watch this Scientific Journal Video about The Evolution of Silica Nanoparticle-polyester Coatings on Surfaces Exposed to Sunlight at JoVE.com

The Evolution of Silica Nanoparticle-polyester Coatings on Surfaces Exposed to Sunlight

两种类型的表面，涂覆有二氧化硅纳米颗粒的层的聚酯涂层钢板及聚酯，进行了研究。两面暴露在阳光下，将其发现导致在表面的化学性质和纳米形貌实质性的变化。

表面上的纳米硅聚酯涂料暴露在阳光下的演变

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高分辨率热显微成像采用铕螯合物的荧光涂料

Micro-electronic devices often undergo significant self-heating when biased to their typical operating conditions. This paper describes a convenient ...

Evanescent Field Based Photoacoustics: Optical Property Evaluation at Surfaces

基于渐逝场光声：光学性能评估在表面

Here, we present a protocol to estimate material and surface optical properties using the photoacoustic effect combined with total internal reflection. ...

Pool-Boiling Heat-Transfer Enhancement on Cylindrical Surfaces with Hybrid Wettable Patterns

在圆柱面池沸腾传热强化与混合可湿性模式

In this study, pool-boiling heat-transfer experiments were performed to investigate the effect of the number of interlines and the orientation of the ...

Fabrication of Superhydrophobic Metal Surfaces for Anti-Icing Applications

防结冰用超疏水性金属表面的制备

Several ways to produce superhydrophobic metal surfaces are presented in this work. Aluminum was chosen as the metal substrate due to its wide use in ...