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DOI :
10.3791/55779-v
•
14:55 min
September 17th, 2017
Chapters
0:00
Title
0:57
Solid-state NMR sample production
4:02
Preliminary structural characterization based on 1D solid-state NMR
7:36
Conformational analysis and 3D structural determination
13:01
Results
14:15
Conclusion
超分子蛋白质的结构在原子分辨率下具有很高的相关性, 因为它们在各种生物现象中具有重要作用。在此, 我们提出了一个协议, 以执行高分辨率结构研究的不溶性和晶大分子蛋白组件的魔术角纺 solid-state 核磁共振光谱学 (MAS SSNMR)。
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