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DOI :
10.3791/57897-v
July 26th, 2018
Chapters
0:04
Title
0:51
Procedure for O-Glycosylation Reactions
5:59
NMR Studies of Cyclic Boronic Ester
7:28
Results: O-Glycosylations of Nucleosides Utilizing Temporary Protection of 2 ,3 -Diol by Boronic Ester
8:08
Conclusion
在这里, 我们提出了合成双糖苷的协议, 选择性O-糖基化的 ribonucleosides通过临时保护其 2 ', 3 '-二醇的基团利用循环硼酸酯。该方法适用于几种不受保护的苷, 如腺苷、鸟嘌呤、胞苷、苷、5-methyluridine 和 5-fluorouridine, 给予相应的双糖苷。
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