Name: key factors affecting the performance of sb2s3-sensitized solar cells during an sb2s3 deposition via sbcl3-thiourea complex solution-processing
Uploaded: 2018-07-16T15:00:00
Description: Watch this Scientific Journal Video about Key Factors Affecting the Performance of Sb2S3-sensitized Solar Cells During an Sb2S3 Deposition via SbCl3-thiourea Complex Solution-processing at JoVE.com

Bu eser Daegu Gyeongbuk Enstitüsü bilim ve teknoloji (DGIST) R & D programları ICT, Kore ve Bilim Bakanlığı tarafından desteklenmiştir (hibe No 18-ET-01 ve 18-01-HRSS-04).

1. TiO2- BL çözüm sentezi
<ol><li>50 mL birimi olan 2 şeffaf tüpleri hazırlayın.</li>
	<li>20 mL etanol 1 flakon (V1) ekleyin ve V1 mühür.</li>
	<li>V1 bir N2' ye naklet-torpido < 1 ppm bir H2O düzeyde bir nem kontrol sistemi ile dolu.</li>
	<li>1.225 mL ekleyin V1 için titanyum (IV) isopropoxide (TTIP), kullanarak 0,45 µm PVDF filtre ve yavaşça karıştırın karışım en az 30 dakika için. Not: Bu adım bir eldiven kutusuna (veya çok düşük nem koşullarında) ge...

<ol>
	<li>Choi, Y. C., Lee, D. U., Noh, J. H., Kim, E. K., Seok, S. I. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Highly+Improved+Sb2S3+Sensitized-Inorganic-Organic+Heterojunction+Solar+Cells+and+Quantification+of+Traps+by+Deep-Level+Transient+Spectroscopy.">Highly Improved Sb2S3 Sensitized-Inorganic-Organic Heterojunction Solar Cells and Quantification of Traps by Deep-Level Transient Spectroscopy.</a> Advanced Functional Materials. 24 (23), 3587-3592 (2014).</li><li>Kim, D. -. H., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Highly+reproducible+planar+Sb2S3-sensitized+solar+cells+based+on+atomic+layer+deposition.">Highly reproducible planar Sb2S3-sensitized solar cells based on atomic layer deposition.</a> Nanoscale. 6 (23), 14549-14554 (2014).</li><li>Choi, Y. C., Seok, S. I. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Efficient+Sb2S3-Sensitized+Solar+Cells+Via+Single-Step+Deposition+of+Sb2S3+Using+S/Sb-Ratio-Controlled+SbCl3-Thiourea+Complex+Solution.">Efficient Sb2S3-Sensitized Solar Cells Via Single-Step Deposition of Sb2S3 Using S/Sb-Ratio-Controlled SbCl3-Thiourea Complex Solution.</a> Advanced Functional Materials. 25 (19), 2892-2898 (2015).</li><li>Godel, K. C., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Efficient+room+temperature+aqueous+Sb2S3+synthesis+for+inorganic-organic+sensitized+solar+cells+with+5.1%+efficiencies.">Efficient room temperature aqueous Sb2S3 synthesis for inorganic-organic sensitized solar cells with 5.1% efficiencies.</a> Chemical Communications. 51 (41), 8640-8643 (2015).</li><li>Choi, Y. C., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Sb2Se3-Sensitized+Inorganic-Organic+Heterojunction+Solar+Cells+Fabricated+Using+a+Single-Source+Precursor.">Sb2Se3-Sensitized Inorganic-Organic Heterojunction Solar Cells Fabricated Using a Single-Source Precursor.</a> Angewandte Chemie International Edition. 53 (5), 1329-1333 (2014).</li><li>Chen, C., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=6.5%+Certified+Efficiency+Sb2Se3+Solar+Cells+Using+PbS+Colloidal+Quantum+Dot+Film+as+Hole-Transporting+Layer.">6.5% Certified Efficiency Sb2Se3 Solar Cells Using PbS Colloidal Quantum Dot Film as Hole-Transporting Layer.</a> ACS Energy Letters. 2 (9), 2125-2132 (2017).</li><li>Choi, Y. C., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Efficient+Inorganic-Organic+Heterojunction+Solar+Cells+Employing+Sb2(Sx/Se1-x)3+Graded-Composition+Sensitizers.">Efficient Inorganic-Organic Heterojunction Solar Cells Employing Sb2(Sx/Se1-x)3 Graded-Composition Sensitizers.</a> Advanced Energy Materials. 4 (7), 1301680 (2014).</li><li>Choi, Y. C., Yeom, E. J., Ahn, T. K., Seok, S. I. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=CuSbS2-Sensitized+Inorganic-Organic+Heterojunction+Solar+Cells+Fabricated+Using+a+Metal-Thiourea+Complex+Solution.">CuSbS2-Sensitized Inorganic-Organic Heterojunction Solar Cells Fabricated Using a Metal-Thiourea Complex Solution.</a> Angewandte Chemie International Edition. 54 (13), 4005-4009 (2015).</li><li>Versavel, M. Y., Haber, J. A. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Structural+and+optical+properties+of+amorphous+and+crystalline+antimony+sulfide+thin-films.">Structural and optical properties of amorphous and crystalline antimony sulfide thin-films.</a> Thin Solid Films. 515 (18), 7171-7176 (2007).</li><li>Yang, B., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Hydrazine+solution+processed+Sb2S3,+Sb2Se3+and+Sb2(S1-xSex)3+film:+molecular+precursor+identification,+film+fabrication+and+band+gap+tuning.">Hydrazine solution processed Sb2S3, Sb2Se3 and Sb2(S1-xSex)3 film: molecular precursor identification, film fabrication and band gap tuning.</a> Scientific Reports. 5, 10978 (2015).</li><li>Peng, B., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Systematic+investigation+of+the+role+of+compact+TiO2+layer+in+solid+state+dye-sensitized+TiO2+solar+cells.">Systematic investigation of the role of compact TiO2 layer in solid state dye-sensitized TiO2 solar cells.</a> Coordination Chemistry Reviews. 248 (13-14), 1479-1489 (2004).</li><li>Chen, C., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Accelerated+Optimization+of+TiO2/Sb2Se3+Thin+Film+Solar+Cells+by+High-Throughput+Combinatorial+Approach.">Accelerated Optimization of TiO2/Sb2Se3 Thin Film Solar Cells by High-Throughput Combinatorial Approach.</a> Advanced Energy Materials. 7 (20), 1700866 (2017).</li><li>Sung, S. -. J., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Systematic+control+of+nanostructured+interfaces+of+planar+Sb2S3+solar+cells+by+simple+spin-coating+process+and+its+effect+on+photovoltaic+properties.">Systematic control of nanostructured interfaces of planar Sb2S3 solar cells by simple spin-coating process and its effect on photovoltaic properties.</a> Journals of Industrial and Engineering Chemistry. 56, 196-202 (2017).</li><li>Gong, J., Liang, J., Sumathy, K. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Review+on+dye-sensitized+solar+cells+(DSSCs):+Fundamental+concepts+and+novel+materials.">Review on dye-sensitized solar cells (DSSCs): Fundamental concepts and novel materials.</a> Renewable &amp; Sustainable Energery Reviews. 16 (8), 5848-5860 (2012).</li><li>Jeon, N. J., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Solvent+engineering+for+high-performance+inorganic-organic+hybrid+perovskite+solar+cells.">Solvent engineering for high-performance inorganic-organic hybrid perovskite solar cells.</a> Nature Materials. 13 (9), 897-903 (2014).</li><li>Choi, Y. C., Lee, S. W., Jo, H. J., Kim, D. -. H., Sung, S. -. J. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Controlled+growth+of+organic-inorganic+hybrid+CH3NH3PbI3+perovskite+thin+films+from+phase-controlled+crystalline+powders.">Controlled growth of organic-inorganic hybrid CH3NH3PbI3 perovskite thin films from phase-controlled crystalline powders.</a> RSC Advances. 6 (106), 104359-104365 (2016).</li><li>Choi, Y. C., Lee, S. W., Kim, D. -. H. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Antisolvent-assisted+powder+engineering+for+controlled+growth+of+hybrid+CH3NH3PbI3+perovskite+thin+films.">Antisolvent-assisted powder engineering for controlled growth of hybrid CH3NH3PbI3 perovskite thin films.</a> APL Materials. 5 (2), 026101 (2017).</li></ol>

TiO2- BL yaygın olduğu bir delik engelleme katman güneş hücreleri olarak kullanılır. Şekil 2' de gösterildiği gibi büyük bir fark TiO2- BL kalınlığına bağlı olarak aygıt performans gözlendi. Eleştirel FTO ve delik taşıma malzemeleri11arasında herhangi bir doğrudan temas önlemek için bir delik engelleme katman olarak görür çünkü bu nedenle, kalınlığı en iyi genel aygıt performansı elde etmek için optimize edi...

Antimon tabanlı chalcogenides (Sb-Chs), SB2S3, Sb2Se3, Sb2(S, Se)3ve CuSbS2, dahil olmak üzere yeni nesil güneş hücreleri1 kullanılabilir gelişmekte olan malzeme olarak kabul edilir ,2,3,4,5,6,7,8. Ancak, fotovoltaik cihazlar üzerinde Sb-Chs ışık emici dayalı henüz mümkün ticarileştirilmesi göstermek için gereken % 10 güç dönüşüm verimliliği (PCE) ulaşılmış.
Bu sınırlamalarının üstesinden gelir, çeşitli yöntem ve teknikler, yüzey işleme thioacetamide kaynaklı1, oda sıcaklığında ifade Yöntem4, bir atom katman ifade tekniği2ve kullanımı gibi uygulanmış olan albüminkolloid nokta kuantum nokta6. Bu çeşitli yöntemler arasında bir kimyasal banyoya ayrışma dayalı çözüm işleme1en yüksek performans sergiledi. Ancak, kimyasal reaksiyon ve tedavi sonrası kesin bir denetim en iyi performans1,3elde etmek için gereklidir.
Son zamanlarda, biz basit bir çözüm-işleme yüksek performanslı Sb2S3için geliştirilen-duyarlı güneş hücreleri bir SbCl3kullanarak-karmaşık çözüm Tioüre (TU)3. Bu yöntemi kullanarak, kaliteli Sb2S%3 6.4 karşılaştırılabilir aygıtı performansını elde etmek için bir güneş hücreye uygulanan kontrollü bir Sb/S oranı sayesinde imal etmek başardık PCE. Ayrıca Sb2S3 tek adım ifade tarafından fabrikasyon beri etkili işlem zamanı azaltmak başardık.
Bu çalışmada, biz mesoporous TiO2 (mp-TiO2) oluşan substrat detaylı deneysel işlemin bir Sb2S3 ifade için tarif / TiO2 katman engelleme (TiO2- BL) / F-katkılı SnO2 () FTO) cam Sb2S3imalatı için-duyarlı güneş hücreleri ile SbCl3- TU karmaşık çözüm-işleme3. Buna ek olarak, bir Sb2S3 ifade sırasında fotovoltaik performansını etkileyen üç önemli faktörler ele tespit ve. Yöntem kavramı diğer derhal tipi güneş hücreleri üzerinde metal katılaşarak alarak kolayca uygulanabilir.

<table border="0" cellpadding="0" cellspacing="0" width="847">
	<tbody>
		<tr height="21">
			<td height="21" style="height:21px;width:316px;">Ethyl alcohol, Pure, &#62;99.5%</td>
			<td style="width:227px;">Sigma-Aldrich</td>
			<td style="width:129px;">459836</td>
			<td style="width:176px;"></td>
		</tr>
		<tr height="20">
			<td height="20" style="height:20px;width:316px;">Titanium(IV) isopropoxide 97%</td>
			<td style="width:227px;">Aldrich</td>
			<td style="width:129px;">205273</td>
			<td></td>
		</tr>
		<tr height="20">
			<td height="20" style="height:20px;width:316px;">Nitic acid, ACS reagent, 70%</td>
			<td style="width:227px;">Sigma-Aldrich</td>
			<td style="width:129px;">438073</td>
			<td></td>
		</tr>
		<tr height="20">
			<td height="20" style="height:20px;width:316px;">Antimony(III) chloride</td>
			<td style="width:227px;">Sigma-Aldrich</td>
			<td style="width:129px;">311375</td>
			<td></td>
		</tr>
		<tr height="20">
			<td height="20" style="height:20px;width:316px;">Thiourea</td>
			<td style="width:227px;">Sigma-Aldrich</td>
			<td style="width:129px;">T7875</td>
			<td></td>
		</tr>
		<tr height="40">
			<td height="40" style="height:40px;width:316px;">N,N-Dimethylformamide, anhydrous, 99.8%</td>
			<td style="width:227px;">Sigma-Aldrich</td>
			<td style="width:129px;">227056</td>
			<td></td>
		</tr>
		<tr height="20">
			<td height="20" style="height:20px;width:316px;">TiO2 paste with 50 nm particles</td>
			<td style="width:227px;">ShareChem</td>
			<td style="width:129px;">SC-HT040</td>
			<td></td>
		</tr>
		<tr height="20">
			<td height="20" style="height:20px;width:316px;">Poly(3-hexylthiophene)</td>
			<td style="width:227px;">1-Material</td>
			<td style="width:129px;">PH0148</td>
			<td></td>
		</tr>
		<tr height="20">
			<td height="20" style="height:20px;width:316px;">Chlorobenzene</td>
			<td style="width:227px;">Sigma-Aldrich</td>
			<td style="width:129px;">284513</td>
			<td></td>
		</tr>
		<tr height="20">
			<td height="20" style="height:20px;width:316px;">FTO/glass (8 Ohmos/sq)</td>
			<td style="width:227px;">Pilkington</td>
			<td style="width:129px;"></td>
			<td></td>
		</tr>
		<tr height="20">
			<td height="20" style="height:20px;width:316px;">Spin coater</td>
			<td style="width:227px;">DONG AH TRADE CORP</td>
			<td style="width:129px;">ACE-200</td>
			<td></td>
		</tr>
		<tr height="20">
			<td height="20" style="height:20px;width:316px;">Hot plate</td>
			<td style="width:227px;">AS ONE Corporation</td>
			<td style="width:129px;">HHP-411</td>
			<td></td>
		</tr>
		<tr height="20">
			<td height="20" style="height:20px;width:316px;">Glove box</td>
			<td style="width:227px;">KIYON</td>
			<td style="width:129px;">KK-021AS</td>
			<td></td>
		</tr>
		<tr height="20">
			<td height="20" style="height:20px;width:316px;">UV OZONE Cleaner</td>
			<td style="width:227px;">AHTECH LTS</td>
			<td style="width:129px;">AC-6</td>
			<td></td>
		</tr>
		<tr height="20">
			<td height="20" style="height:20px;width:316px;">Furnace</td>
			<td style="width:227px;">WiseTherm</td>
			<td style="width:129px;">FP-14</td>
			<td></td>
		</tr>
		<tr height="20">
			<td height="20" style="height:20px;width:316px;">UV/Vis Absorption spectroscopy</td>
			<td style="width:227px;">PerkinElmer</td>
			<td style="width:129px;">Lambda 750</td>
			<td></td>
		</tr>
		<tr height="40">
			<td height="40" style="height:40px;width:316px;">Multifunctional evaporator with glove box</td>
			<td style="width:227px;">DAEDONG HIGH TECHNOLOGIES</td>
			<td style="width:129px;">DDHT-SDP007</td>
			<td></td>
		</tr>
	</tbody>
</table>

key factors affecting the performance of sb2s3-sensitized solar cells during an sb2s3 deposition via sbcl3-thiourea complex solution-processing

SB2S3 nesil güneş hücreleri için benzersiz optik ve elektriksel özellikleri nedeniyle uygulanabilir ortaya çıkan ışık emici biri olarak kabul edilir. Son zamanlarda, biz potansiyel yeni nesil güneş hücreleri Sb2S%3> 6 yüksek bir fotovoltaik verim elde tarafından gösterdi-duyarlı güneş hücreleri basit Tioüre (TU) kullanarak-dayalı karmaşık çözüm yöntemi. Burada, biz güneş hücreleri imalatı SbCl3- TU karmaşık bir çözüm kullanarak bir mesoporous TiO2 (mp-TiO2) katmandaki devrilmesinden sonra Sb2S3 için anahtar deneysel yordamlar açıklar. İlk olarak, SbCl3- TU çözüm N, N- dimethylformamide SbCl3farklı molar oranları, SbCl3 ve TU çözülerek sentezlenir: TU. O zaman, çözüm hazırlanan yüzeyler üzerinde mp-TiO2/TiO2/ oluşan yatırılır-spin kaplama tarafından SnO2 cam katman/F-katkılı engelleme. Son olarak, kristal Sb2S3oluşturmak için örnekleri N2' komplementer-torpido 300 ° C'de dolu Fotovoltaik aygıt performans deneysel parametrelerin etkilerini de ele alınmıştır.

Şekil 1 Sb2S3 ifade için deneysel bir işlem şematik gösterimi mp-TiO2/TiO2- BL/FTO cam yüzey üzerinde gösterir. Şekil 1 d temel özellikleri ve burada açıklanan yöntemle fabrikasyon tipik bir ürün düzenini gösterir. Ana x-ışını kırınım (XRD) desen de bu bir stibnite Sb2S3 yapısı1,3<...

Watch this Scientific Journal Video about Key Factors Affecting the Performance of Sb2S3-sensitized Solar Cells During an Sb2S3 Deposition via SbCl3-thiourea Complex Solution-processing at JoVE.com

Key Factors Affecting the Performance of Sb2S3-sensitized Solar Cells During an Sb2S3 Deposition via SbCl3-thiourea Complex Solution-processing

Anahtar Sb2S3performansını etkileyen faktörler-güneş hücreleri bir Sb2S3 ifade ile SbCl3sırasında sensitize-Tioüre karmaşık çözüm-işleme

Bu eser devrilmesinden sonra Sb2S3 SbCl3kullanarak bir mesoporous TiO2 katman için detaylı deneysel bir işlem sağlar-Sb2S3uygulamalarında karmaşık çözüm Tioüre-duyarlı güneş hücreleri. Bu makalede ayrıca önemli faktörler biriktirme işlemi yöneten belirler.

Sb2S3 is considered as one of the emerging light absorbers that can be applied to next-generation solar cells because of its unique optical and electrical ...

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Chemistry

Key Factors Affecting the Performance of Sb2S3-sensitized Solar Cells During an Sb2S3 Deposition via SbCl3-thiourea Complex Solution-processing

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Atmospheric pressure spatial atomic layer deposition (AP-SALD) was used to deposit n-type ZnO and Zn1-xMgxO thin films onto p-type thermally oxidized Cu2O ...

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Yüzeyel Kimyasal Yapıştırmanın TiO&#39;ya Etkisi<sub&gt; 2</sub&gt; -SiO<sub&gt; 2</sub&gt; Fotokatalitik NOx Azaltma Performansına Sahip Kompozitler

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