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DOI :
10.3791/59409-v
•
9:37 min
October 18th, 2019
Chapters
0:04
Title
2:32
Leak Check for all the High Vacuum Vessels and Their Connection to the HVL
2:59
Dehydroxylated Silica Preparation
3:55
Solvent Preparation (Removal of Oxygen & Moisture)
4:35
General Procedure for Grafting Metal Complexes on Dehydroxylated Silica using Hf(NMe2)4
6:15
Preparation of the Catalyst and Imine Metathesis Catalysis
7:29
Results: Characterization of New Heterogeneous Catalyst for Imine Metathesis
8:58
Conclusion
通过将胺金属复合物嫁接到脱羟基化二氧化硅上,制备了用于胺代谢的新型IV类金属催化剂。表面金属碎片采用FT-IR、元素微分析和固态NMR光谱法进行特征。进一步的动态核极化表面增强了核磁共振光谱实验,补充了协调范围的确定。
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