Research
Education
Sign In
EN
EN - English
CN - 中文
DE - Deutsch
ES - Español
KR - 한국어
IT - Italiano
FR - Français
PT - Português
Please note that all translations are automatically generated. Click here for the English version.
DOI :
10.3791/59409-v
•
9:37 min
October 18th, 2019
Chapters
0:04
Title
2:32
Leak Check for all the High Vacuum Vessels and Their Connection to the HVL
2:59
Dehydroxylated Silica Preparation
3:55
Solvent Preparation (Removal of Oxygen & Moisture)
4:35
General Procedure for Grafting Metal Complexes on Dehydroxylated Silica using Hf(NMe2)4
6:15
Preparation of the Catalyst and Imine Metathesis Catalysis
7:29
Results: Characterization of New Heterogeneous Catalyst for Imine Metathesis
8:58
Conclusion
イミンメタセシスのための新しいグループIV金属触媒は、脱ヒドロキシレートシリカ上にアミン金属複合体を移植することによって調製される。表面金属断片は、FT-IR、元素微小分析、および固体NMR分光法を使用して特徴付けられます。さらに動的な核偏光面強化NMR分光実験は、協調球の決定を補完する。
Tags
-- Views
Related Videos
Privacy
Terms of Use
Policies
Contact Us
Recommend to library
JoVE NEWSLETTERS
JoVE Journal
Methods Collections
JoVE Encyclopedia of Experiments
Archive
JoVE Core
JoVE Business
JoVE Science Education
JoVE Lab Manual
Faculty Resource Center
Authors
Overview
Publishing Process
Editorial Board
Scope and Policies
Peer Review
FAQ
Submit
Librarians
Testimonials
Subscriptions
Access
Resources
Library Advisory Board
ABOUT JoVE
Leadership
Copyright © 2024 MyJoVE Corporation. All rights reserved