Name: ultrasonic welding of thermoplastic composite coupons for mechanical characterization of welded joints through single lap shear testing
Uploaded: 2016-02-11T14:00:00.000+00:00
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Description: Watch this Scientific Journal Video about Ultrasonic Welding of Thermoplastic Composite Coupons for Mechanical Characterization of Welded Joints through Single Lap Shear Testing at JoVE.com

The authors would like to acknowledge the support of Ten Cate Advanced Materials in the form of free material supply to the work described in this paper.

1.试样切割并准备超声波焊接<ol><li>切矩形样品从利用切割技术，可防止样品（例如，金刚石锯或水射流切割）的边缘的剥离较大热塑性复合层压测量25.4毫米×101.6毫米。 注:样品的尺寸是根据ASTM D 1002标准。 <ol><li>由于焊接接头的强度依赖于表面上的纤维取向，以被焊接10，照顾切断所有样品中相同的方向。 </li></ol></li><li>切割，干燥的样品在烘箱中按照制造商的建议的情况下，后在热塑性树脂趋于吸收水分（例如，在135℃对六个层碳纤维6小时增强聚醚，CF / PEI，样本）。 </li><li>切做出来整齐热塑薄膜（相同的树脂在复合材料中的基质）平能量导向到大小（大约26毫米×26毫米）的厚度为至少0.25毫米。如果需要的话，干燥该能量控制器下列制造商的建议（例如，在135℃为PEI能量控制器1小时）。 </li><li>焊接前，检查样本逐一进行分层的角落，如果需要丢弃。用脱脂剂和棉布清洁。清洁按照相同的程序的平坦能量控制器。 </li></ol> 2.单搭接剪切券超声波焊接注意:微处理器控制超声波焊机能够以恒定的振幅焊接在该步骤中使用。焊机输出处理的数据，例如耗散功率，并在计算机中的超声焊极相对于时间对数据采集软件的位移。设计和制造的精确定位和超声波焊接期间夹紧单搭接剪切样品A定制夹具在此步骤中使用（参见图1）。 图1.超声波焊机和本研究中使用的定制焊接设置1:超声焊极，2:滑动平台，3:夹具上部试样（连接到2），和4:钳用于下试验片（由参考转载4爱思唯尔的许可。） <a href="https://www.jove.com/files/ftp_upload/53592/53592fig1large.jpg" target="_blank">点击此处查看该图的放大版本。</a> <ol><li>填写每个焊接实验前的日志表。 <ol><li>请注意以下参数:RT和湿度，焊接安装参考，超声焊极的类型，采样数和材料，宽度和顶部和底部样品厚度和​​能量控制器的厚度。 </li></ol></li><li>打开超声波焊机和计算机。启动数据采集软件，并打开一个新的会话。 </li><li>如果不是已经到位，改变sonot骑用直径40毫米的圆柱形超声波发生器，以便其底表面完全覆盖焊接区。 注意:超声波发生器的不同的形状都可以使用，但其底表面不应该比焊接面积小。 </li><li>位置和固定标本和能量导向到焊接夹具（ 参见图1）。 <ol><li>附加一个平坦能量控制器与胶带底部试样，使其覆盖比待焊接的区域略大的面积（12.7毫米×25.4毫米）。 </li><li>将底部样品放入夹具并拧紧顶部的螺丝夹紧。 </li><li>胶带将能量导向到安装的基底的另一端，以便它在此过程中保持就位。 </li><li>上好的样品放入夹子，对齐并拧紧顶部的螺丝。 </li><li>为顶样品放入滑动平台夹紧位置，拧紧两个螺丝。 </li><li>在进一步讨论之前，一旦收紧m该四个螺丝矿石。 </li></ol></li><li>确定基于所述超声焊极，以实现最高熔接强度的位移的振动相位的最佳持续时间，如在步骤2.5.1至2.5.8中描述。 注意:振动相位的最佳持续时间被用于焊接力和振动振幅的每个期望的组合来确定。 <ol><li>设置超声波焊机差分位移控制模式。 </li><li>输入的焊接力和振动振幅进入超声焊接机（例如，300 N和86.2微米）。 注意:对于该超声波焊机，86.2微米对应于峰 - 峰振幅。在机器的设置，表示为该值的一半，43.1微米。 </li><li>输入的超声焊极的位移，或旅行，在振动相位等于能量控制器（例如，0.25mm）的初始厚度的值的末尾。 </li><li>输入凝固力和时间进入超声焊接机（例如，1000N和4000毫秒）。 </li><li>准备就绪后，戴上隔音耳机和启动超声波焊接工艺。 </li><li>该过程完成后，请注意以下输出参数:焊接距离，最大功率，振动的时间和精力。从焊接安装取下优惠券，并写入其识别号码上都用油漆标记结束。 </li><li>焊接数据（功率和超声焊极的位移）导出到电子表格，并在该过程的振动相位绘制功率和位移随时间的曲线。 注意:位移曲线应在振动阶段的开始绘制相对于其位置的超声焊极的向下位移。 </li><li>识别所述功率高原（阶段4）的中间的位移上的图2（在这种情况下，0.10 MM），如图所示。 注意:这个特殊的位移值是控制振动相位和意愿的持续时间的最佳行程在相同的焊接力和振幅，以后每焊使用。 </li></ol></li></ol><img alt="图2" src="/files/ftp_upload/53592/53592fig2.jpg" /> 图2.电源（黑色）和用于指示最佳行程值的超声波焊接工艺位移（灰色）的曲线。在超声波焊接的振动相位可以在5个阶段进行分割。最佳旅游价值位于第4阶段分析案例中:碳纤维增强聚醚-PEI基板，厚0.25mm扁PEI能源董事，300N的焊接力，86.2微米振幅为0.25毫米的行程。 （从参考文献4与爱思唯尔的许可转载。） <a href="https://www.jove.com/files/ftp_upload/53592/53592fig2large.jpg" target="_blank">点击此处查看该图的放大版本。</a> <ol start="6"><li>在对给定的焊接力和振幅combinatio最佳旅游价值焊接券ñ。 <ol><li>重复步骤2.1至2.5.6每个焊缝。在步骤2.5.3，使用步骤2.5.8为相应的焊接力和振幅组合确定最佳行程。 注意:所有LSS的测试都进行了万能试验机上下列ASTM D 1002为1.3mm / min的十字头速度。 </li></ol></li></ol> 3.单搭接剪切强度（LSS）焊接券测试<ol><li>量取每个焊接优惠券的重叠宽度的音符。 </li><li>打开万能试验机上，然后打开计算机上的LSS测试程序。 </li><li>在测试接口，输入样品号和​​重叠的尺寸。置的力为0，并且把手抓握分离到其初始位置（例如60毫米）。 </li><li>关于图3所示的试验机的夹具的样品定位。 </li></ol><img alt="图3" srC ="/文件/ ftp_upload / 53592 / 53592fig3.jpg"/&gt; 图3.在兹维克/罗尔250千牛万能试验机（不按比例）夹紧的示意图。顶部和下夹具之间的偏移位移允许对准中心焊接线的载荷方向 ​​，以尽量减少搭接剪切期间弯曲强度试验。 <a href="https://www.jove.com/files/ftp_upload/53592/53592fig3large.jpg" target="_blank">请点击此处查看该图的放大版本。</a> <ol start="5"><li>单击"开始"按钮，开始从计算机检测程序。 </li><li>样品断裂后，从交手删除它，两部分用胶带固定在一起。 </li><li>重复步骤其他所有样品中3.3至3.6。 </li><li>当测试完成后，将数据导出到电子表格，并计算平均LSS值，根据标准的描述，对于每一个焊接力和振幅相结合的过程。 </li></ol>

<ol>
	<li>Yousefpour, A., Hojjati, M., Immarigeon, J. P. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Fusion+bonding/welding+of+thermoplastic+composites.">Fusion bonding/welding of thermoplastic composites.</a> J Thermoplast Compos. 17, 303-341 (2004).</li><li>Villegas, I. F. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=In+situ+monitoring+of+ultrasonic+welding+of+thermoplastic+composites+through+power+and+displacement+data.">In situ monitoring of ultrasonic welding of thermoplastic composites through power and displacement data.</a> J Thermoplast Compos. 28 (1), 66-85 (2015).</li><li>Benatar, A., Gutowski, T. G. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Ultrasonic+welding+of+PEEK+Graphite+APC-2+composites.">Ultrasonic welding of PEEK Graphite APC-2 composites.</a> Polym Eng Sci. 29 (23), 1705-1721 (1989).</li><li>Villegas, I. F. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Strength+development+versus+process+data+in+ultrasonic+welding+of+thermoplastic+composites+with+flat+energy+directors+and+its+application+to+the+definition+of+optimum+processing+parameters.">Strength development versus process data in ultrasonic welding of thermoplastic composites with flat energy directors and its application to the definition of optimum processing parameters.</a> Compos Part A-Appl S. 65, 27-37 (2014).</li><li>Lu, H. M., Benatar, A., He, F. G. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Sequential+ultrasonic+welding+of+PEEK/graphite+composite+plates.">Sequential ultrasonic welding of PEEK/graphite composite plates.</a> Proceedings of the ANTEC'91 Conference. , 2523-2526 (1991).</li><li>Potente, H. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Ultrasonic+welding+-+principles+&amp;+theory.">Ultrasonic welding - principles &amp; theory.</a> Mater Design. 5, 228-234 (1984).</li><li>Stavrov, D., Bersee, H. E. N. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Resistance+welding+of+thermoplastic+composites+-+an+overview.">Resistance welding of thermoplastic composites - an overview.</a> Compos Part A-Appl S. 36, 39-54 (2005).</li><li>Villegas, I. F., Valle-Grande, B., Bersee, H. E. N., Benedictus, R. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=A+comparative+evaluation+between+flat+and+traditional+energy+directors+for+ultrasonic+welding+of+CF/PPS+thermoplastic+composites.">A comparative evaluation between flat and traditional energy directors for ultrasonic welding of CF/PPS thermoplastic composites.</a> Compos Interface. , (2015).</li><li>Levy, A., Le Corre, S., Villegas, I. F. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Modelling+the+heating+phenomena+in+ultrasonic+welding+of+thermoplastic+composites+with+flat+energy+directors.">Modelling the heating phenomena in ultrasonic welding of thermoplastic composites with flat energy directors.</a> J Mater Process Tech. , 1361-1371 (2014).</li><li>Shi, H., Villegas, I. F., Bersee, H. E. N. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Strength+and+failure+modes+in+resistance+welded+thermoplastic+composite+joints:+effect+of+fibre-matrix+adhesion+and+fibre+orientation.">Strength and failure modes in resistance welded thermoplastic composite joints: effect of fibre-matrix adhesion and fibre orientation.</a> Compos Part A-Appl S. 55, 1-10 (2013).</li><li>Villegas, I. F., Bersee, H. E. N. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Ultrasonic+welding+of+advanced+thermoplastic+composites.+An+investigation+on+energy-directing+surfaces.">Ultrasonic welding of advanced thermoplastic composites. An investigation on energy-directing surfaces.</a> Adv Polym Tech. 29 (2), 113-121 (2010).</li><li>Harras, B. K., Cole, C., Vu-Khanh, T. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Optimization+of+the+ultrasonic+welding+of+PEEK-carbon+composites.">Optimization of the ultrasonic welding of PEEK-carbon composites.</a> J Reinf Plast Comp. 15 (2), 174-182 (1996).</li></ol>

The authors declare that they have no competing financial interest.

在上一节中提供的结果表明，在本文中用于热塑性复合单搭接券用于机械测试的目的的超声波焊接所提出的简单的方法的适当性。以下段落讨论的结果如何验证了该方法的三大支柱， 即采用平松能源董事，使用过程中的反馈来定义振动和使用位移控制的最佳时间，还有的适用性和局限性的技术。 至于第一支柱，扁平能量导向器被示为允许在​​TPC券的成功焊接。在的?...

热塑性复合材料（TPC）具有待焊接的能力，这有助于其成本效益的生产。焊接需要的压力，以软化或熔化的接合表面的热塑性树脂并允许紧密接触并穿过焊接界面的热塑性聚合物链的后续相互扩散下局部加热。一旦分子相互扩散实现时，在压力下冷却巩固了焊接接头。几个焊接技术适用于其中的主要区别在于热1，但是，主要的"粘着"的机制， 即，分子的缠结源热塑性复合材料，保持不变。超声波焊接提供了非常短的焊接时间（在几秒钟的数量级），易于自动化并且这几乎是独立加固在热塑性复合衬底的类型。此外，它提供了用于原位监控2,3的可能性</sup&gt;，它可用于在线路的质量保证或用于处理窗口4快速定义。热塑性复合材料的超声波焊接是大多点焊过程中，通过连续的超声波焊接更长接缝然而成功焊接已经报道在文献5。相对于电阻或感应焊接，超声波焊接尚未在工业上应用用于热塑性复合材料部件之间的结构接头为止。然而，显著的努力，目前正在致力于进一步为飞机应用热塑性复合材料结构超声波焊接的发展。 在超声波焊接，要接合的部分进行的静力和高频低幅的机械振动的组合横向于焊接界面，它通过表面和粘弹加热导致热量的产生。在焊接界面优先加热促进通过在表面上利用树脂突起待焊接其经受更高环状应变，并且因此更高的粘弹性加热，比基片6。力和振动施加在部分通过连接到一个媒体以及包括压电转换器和助力器的超声波列车超声焊极进行焊接。取决于其中超声焊极接触部分被接合点和焊接界面之间的距离，可以区别近场和远场超声波焊接之间进行。近场焊接（超声波发生器和焊接界面之间小于6毫米）是适用于更广范围的，而远场焊接的适用性到特定的热塑性材料的材料是高度依赖于材料的，进行声波6的能力。 超声波焊接过程可以分成三个主要阶段。首先，一个力建阶段，在此期间，sonotro德逐渐增加要被焊接的零件上的力，直到达到一定的触发力。在此阶段没有施加振动。其次，振动相位，一旦达到触发力，开始。在这个阶段，超声焊极振动在用于产生所需的焊接过程中的热量一定量的时间在规定的幅度。微处理器控制的超声波焊接机提供了多种选择，以控制振动阶段的持续时间，其中的时间（ 即直接控制），位移或能量（间接控制）。在这个阶段施加的力即焊接力，可以保持恒定并等于触发力或可振动的应用过程中逐渐改变。第三，凝固阶段，在此期间的焊接部分被允许冷却下一定的凝固力为一定的时间。在这个最后阶段无振动被应用。 焊接FORCE，振动幅度，振动频率和振动相位的持续时间（无论是直接或间接通过能量或位移控制）是控制热生成焊接参数。力，幅度和持续时间是用户定义的参数，而频率被固定为每个超声波焊接。凝固力和凝固时间，也焊接参数，不要在加热过程中与参数的休息，焊接接头的最终质量干预反而影响了巩固和一起。 本文提出了个人TPC券的近场超声波焊接在单圈配置随后的机械，单搭接剪切（LSS），测试按ASTM（美国测试和材料）D 1002标准的一种新型直接的方法。焊接试样的机械测试允许确定关节的表观搭接剪切强度，这是性能最COMM之一仅用于量化的热塑性复合材料的焊接接头7的强度。在本文中所述的焊接方法是基于三个主要支柱。首先，松平能量导向器以在焊接过程中的接合界面8,9用于优先发热。其次，通过超声波焊机提供的方法的数据被用于快速确定振动相位的最佳持续时间为特定的力/幅度组合2,4。第三，振动阶段的持续时间是间接通过超声焊极的位移，以确保焊接接头4的稳定的质量控制。这种焊接方法提供与问候国家的最先进的焊接工艺热塑性复合材料主要有以下新奇和优势:（1）通过使用松平能量导向，而不是传统的成型能源董事3的启用简化的样品制备，和（二）快速和c的基础上在原位过程监控，而不是普通的试验和错误的方法处理参数OST效率定义。虽然在本文中描述的方法，向得到一个非常具体和简单的焊接几何面向它可以作为一个基础，以定义实际部件的焊接过程。在这种情况下，一个主要的区别来自能源主任约束流结果在单圈券重叠的四个边缘反对自由流动。

<table><tbody><tr><td>&lt;strong&gt;Material/Reagent&lt;/strong&gt;</td><td></td><td></td><td></td></tr><tr><td>Cetex carbon fiber / polyetherimide (CF/PEI) 5 harness satin prepreg</td><td>TenCate Advanced Composites (www.tencate.com)</td><td>Contact vendor</td><td>Material used in this study for the specimens.</td></tr><tr><td>PFQD solvent degreaser</td><td>PT Technologies Europe (now Socomore - www.socomore.com)</td><td>Contact vendor</td><td>Solvent degreaser for cleaning the specimens and energy directors.</td></tr><tr><td>Cotton cloths</td><td></td><td></td><td>For general cleaning purposes. No specific vendor was used.</td></tr><tr><td>0.25 mm PEI film</td><td>TenCate Advanced Composites (www.tencate.com)</td><td>Contact vendor</td><td>Thin film used as energy director.</td></tr><tr><td>Adhesive tape</td><td>Airtech Advanced Materials Group (www.airtechintl.com)</td><td>1&quot; x 72 yds MFG # 327402 Contact vendor for catalog number</td><td>Used to attach energy director to bottom sample for ultrasonic welding.</td></tr><tr><td>&lt;strong&gt;Name&lt;/strong&gt;</td><td>&lt;strong&gt;Company&lt;/strong&gt;</td><td>&lt;strong&gt;Catalog Number&lt;/strong&gt;</td><td>&lt;strong&gt;Comments&lt;/strong&gt;</td></tr><tr><td>&lt;strong&gt;Equipment&lt;/strong&gt;</td><td></td><td></td><td></td></tr><tr><td>V&amp;ouml;tsch oven</td><td>V&amp;ouml;tsch Industrietechnik (www.voetsch-ovens.com)</td><td>VTU 60/60 - Contact vendor for specific catalog number</td><td>Oven used to dry PEI film (energy directors) and PEI specimens before welding.</td></tr><tr><td>Rinco Dynamic 3000 ultrasonic welder</td><td>Aeson BV (www.aeson.nl/en/)</td><td>Contact vendor</td><td>20 kHz ultrasonic welding machine used for the welding experiments. Several sonotrode sizes available. Contact vendor for details. ACUCapture software included.</td></tr><tr><td>Zwick/Roell universal testing machine</td><td>Zwick (www.zwick.com)</td><td>Z250 - Contact vendor for specific catalog number</td><td>Universal testing machine with maximum load of 250 kN used for single lap shear strength measurements.</td></tr></tbody></table>

ultrasonic welding of thermoplastic composite coupons for mechanical characterization of welded joints through single lap shear testing

This paper presents a novel straightforward method for ultrasonic welding of thermoplastic-composite coupons in optimum processing conditions. The ultrasonic welding process described in this paper is based on three main pillars. Firstly, flat energy directors are used for preferential heat generation at the joining interface during the welding process. A flat energy director is a neat thermoplastic resin film that is placed between the parts to be joined prior to the welding process and heats up preferentially owing to its lower compressive stiffness relative to the composite substrates. Consequently, flat energy directors provide a simple solution that does not require molding of resin protrusions on the surfaces of the composite substrates, as opposed to ultrasonic welding of unreinforced plastics. Secondly, the process data provided by the ultrasonic welder is used to rapidly define the optimum welding parameters for any thermoplastic composite material combination. Thirdly, displacement control is used in the welding process to ensure consistent quality of the welded joints. According to this method, thermoplastic-composite flat coupons are individually welded in a single lap configuration. Mechanical testing of the welded coupons allows determining the apparent lap shear strength of the joints, which is one of the properties most commonly used to quantify the strength of thermoplastic composite welded joints.

碳纤维增强聚醚酰亚胺（CF / PEI）的样品被焊接以下本文所描述的方法。将样品从造出来的五线束缎纹织物的CF / PEI，用（0/90）3S堆叠序列和1.92 mm标称厚度的复合层压材料获得。样品从这个叠层切割，使得纤维的主视方向平行于它们的最长边。使用了0.25毫米的厚度平面的PEI能量导向器。两者复合样品和能量导向器在烘箱中于135℃分别干燥6和1小时后，由制造商所指...

Watch this Scientific Journal Video about Ultrasonic Welding of Thermoplastic Composite Coupons for Mechanical Characterization of Welded Joints through Single Lap Shear Testing at JoVE.com

Ultrasonic Welding of Thermoplastic Composite Coupons for Mechanical Characterization of Welded Joints through Single Lap Shear Testing

A straightforward procedure for ultrasonic welding of thermoplastic composite coupons for basic mechanical testing is described. Key characteristics of this ultrasonic welding process are the use of flat energy directors for simplified process preparation and the use of process data for the fast definition of optimum processing conditions.

通过单搭接剪切试验的热塑性复合材料优惠券焊接接头的力学特性的超声波焊接

This paper presents a novel straightforward method for ultrasonic welding of thermoplastic-composite coupons in optimum processing conditions. The ...

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11.5K 次观看.  Delft University of Technology. A straightforward procedure for ultrasonic welding of thermoplastic composite coupons for basic mechanical testing is described. Key characteristics of this ultrasonic welding process are the use of flat energy directors for simplified process preparation and the use of process data for the fast definition of optimum processing conditions.

视频: Ultrasonic Welding of Thermoplastic Composite Coupons for Mechanical Characterization of Welded Joints through Single Lap Shear Testing

Experiments on Ultrasonic Lubrication Using a Piezoelectrically-assisted Tribometer and Optical Profilometer

Friction and wear are detrimental to engineered systems. Ultrasonic lubrication is achieved when the interface between two sliding surfaces is vibrated at a frequency above the acoustic range (20 kHz). As a solid-state technology, ultrasonic lubrication can be used where conventional lubricants are unfeasible or undesirable. Further, ultrasonic lubrication allows for electrical modulation of the effective friction coefficient between two sliding surfaces. This property enables adaptive systems that modify their frictional state and associated dynamic response as the operating conditions change. Surface wear can also be reduced through ultrasonic lubrication. We developed a protocol to investigate the dependence of friction force reduction and wear reduction on the linear sliding velocity between ultrasonically lubricated surfaces. A pin-on-disc tribometer was built which differs from commercial units in that a piezoelectric stack is used to vibrate the pin at 22 kHz normal to the rotating disc surface. Friction and wear metrics including effective friction force, volume loss, and surface roughness are measured without and with ultrasonic vibrations at a constant pressure of 1 to 4 MPa and three different sliding velocities: 20.3, 40.6, and 87 mm/sec. An optical profilometer is utilized to characterize the wear surfaces. The effective friction force is reduced by 62% at 20.3 mm/sec. Consistently with existing theories for ultrasonic lubrication, the percent reduction in friction force diminishes with increasing speed, down to 29% friction force reduction at 87 mm/sec. Wear reduction remains essentially constant (49%) at the three speeds considered.

We present a protocol for using a piezoelectrically-assisted tribometer and optical profilometer to investigate the dependence of ultrasonic wear and friction reduction on linear velocity, contact pressure, and surface properties.

使用超声波润滑实验一压电辅助摩擦试验机和光学轮廓

Friction and wear are detrimental to engineered systems. Ultrasonic lubrication is achieved when the interface between two sliding surfaces is vibrated at ...

科研

工程学

Testing of Nanoparticle Release from a Composite Containing Nanomaterial Using a Chamber System

With the rapid development of nanotechnology as one of the most important technologies in the 21st century, interest in the safety of consumer products containing nanomaterials is also increasing. Evaluating the nanomaterial release from products containing nanomaterials is a crucial step in assessing the safety of these products, and has resulted in several international efforts to develop consistent and reliable technologies for standardizing the evaluation of nanomaterial release. In this study, the release of nanomaterials from products containing nanomaterials is evaluated using a chamber system that includes a condensation particle counter, optical particle counter, and sampling ports to collect filter samples for electron microscopy analysis. The proposed chamber system is tested using an abrasor and disc-type nanocomposite material specimens to determine whether the nanomaterial release is repeatable and consistent within an acceptable range. The test results indicate that the total number of particles in each test is within 20% from the average after several trials. The release trends are similar and they show very good repeatability. Therefore, the proposed chamber system can be effectively used for nanomaterial release testing of products containing nanomaterials.

Nanoparticle release is tested using a chamber system that includes a condensation particle counter, an optical particle counter and sampling ports to collect filter samples for microscopy analysis. The proposed chamber system can be effectively used for nanomaterial release testing with a repeatable and consistent data range.

从使用室系统一个复合含纳米材料的纳米颗粒释放测试

With the rapid development of nanotechnology as one of the most important technologies in the 21st century, interest in the safety of consumer products ...

Challenges in Rheological Characterization of Highly Concentrated Suspensions &#8212; A Case Study for Screen-printing Silver Pastes

A comprehensive rheological characterization of highly concentrated suspensions or pastes is mandatory for a targeted product development meeting the manifold requirements during processing and application of such complex fluids. In this investigation, measuring protocols for a conclusive assessment of different process relevant rheological parameters have been evaluated. This includes the determination of yield stress, viscosity, wall slip velocity, structural recovery after large deformation and elongation at break as well as tensile force during filament stretching.
The importance of concomitant video recordings during parallel-plate rotational rheometry for a significant determination of rheological quantities is demonstrated. The deformation profile and flow field at the sample edge can be determined using appropriate markers. Thus, measurement parameter settings and plate roughness values can be identified for which yield stress and viscosity measurements are possible. Slip velocity can be measured directly and measuring conditions at which plug flow, shear banding or sample spillover occur can be identified clearly. 
Video recordings further confirm that the change in shear moduli observed during three stage oscillatory shear tests with small deformation amplitude in stage I and III but large oscillation amplitude in stage II can be directly attributed to structural break down and recovery. For the pastes investigated here, the degree of irreversible, shear-induced structural change increases with increasing deformation amplitude in stage II until a saturation is reached at deformations corresponding to the crossover of G' and G'', but the irreversible damage is independent of the duration of large amplitude shear. 
A capillary breakup elongational rheometer and a tensile tester have been used to characterize deformation and breakup behavior of highly filled pastes in uniaxial elongation. Significant differences were observed in all experiments described above for two commercial screen-printing silver pastes used for front side metallization of Si-solar cells.

A protocol for a robust and application relevant rheological characterization of highly concentrated suspensions is presented. Silver pastes used for screen-printing application in solar cell production are employed as model systems.

挑战流变特性高度集中悬架 - 为例进行丝网印刷银浆

A comprehensive rheological characterization of highly concentrated suspensions or pastes is mandatory for a targeted product development meeting the ...

A Novel Biaxial Testing Apparatus for the Determination of Forming Limit under Hot Stamping Conditions

The hot stamping and cold die quenching process is increasingly used to form complex shaped structural components of sheet metals. Conventional experimental approaches, such as out-of-plane and in-plane tests, are not applicable to the determination of forming limits when heating and rapid cooling processes are introduced prior to forming for tests conducted under hot stamping conditions. A novel in-plane biaxial testing system was designed and used for the determination of forming limits of sheet metals at various strain paths, temperatures, and strain rates after heating and cooling processes in a resistance heating uniaxial testing machine. The core part of the biaxial testing system is a biaxial apparatus, which transfers a uniaxial force provided by the uniaxial testing machine to a biaxial force. One type of cruciform specimen was designed and verified for the formability test of aluminum alloy 6082 using the proposed biaxial testing system. The digital image correlation (DIC) system with a high-speed camera was used for taking strain measurements of a specimen during a deformation. The aim of proposing this biaxial testing system is to enable the forming limits of an alloy to be determined at various temperatures and strain rates under hot stamping conditions.

This protocol proposes a novel biaxial testing system used on a resistance heating uniaxial tensile test machine in order to determine the forming limit diagram (FLD) of sheet metals under hot stamping conditions.

一种新型双轴试验设备的成形极限的下烫印条件的决定

The hot stamping and cold die quenching process is increasingly used to form complex shaped structural components of sheet metals. Conventional ...

Ultrasonic Fatigue Testing in the Tension-Compression Mode

Ultrasonic fatigue testing is one of a few methods which allow investigating fatigue properties in the ultra-high cycle region. The method is based on exposing the specimen to longitudinal vibrations on its resonance frequency close to 20 kHz. With use of this method, it is possible to significantly decrease the time required for the test, when compared to conventional testing devices usually working at frequencies under 200 Hz. It is also used to simulate loading of material during operation in high speed conditions, such as those experienced by components of jet engines or car turbo pumps. It is necessary to operate only in the high and ultra-high cycle region, due to the possibility of extremely high deformation rates, which can have a significant influence on the test results. Specimen shape and dimensions have to be carefully selected and calculated to fulfill the resonance condition of the ultrasonic system; thus, it is not possible to test the full components or specimens of arbitrary shape. Before each test, it is necessary to harmonize the specimen with the frequency of the ultrasonic system to compensate for deviations of the real shape from the ideal one. It is not possible to run a test until a total fracture of the specimen, since the test is automatically terminated after initiation and propagation of the crack to a certain length, when the stiffness of the system changes enough to shift the system out of the resonance frequency. This manuscript describes the process of evaluation of materials' fatigue properties at high-frequency ultrasonic fatigue loading with use of mechanical resonance at a frequency close to 20 kHz. The protocol includes a detailed description of all steps required for a correct test, including specimen design, stress calculation, harmonizing with the resonance frequency, performing the test, and final static fracture.

A protocol for ultrasonic fatigue testing in the high and ultra-high cycle region in axial tension-compression loading mode.

拉伸压缩模式下的超声疲劳试验

Ultrasonic fatigue testing is one of a few methods which allow investigating fatigue properties in the ultra-high cycle region. The method is based on ...

Generating Lap Joints Via Friction Stir Spot Welding on DP780 Steel

Friction stir spot welding (FSSW), a derivative of friction stir welding (FSW), is a solid-state welding technique that was developed in 1991. An industry application was found in the automotive industry in 2003 for the aluminum alloy that was used in the rear doors of automobiles. Friction stir spot welding is mostly used in Al alloys to create lap joints. The benefits of friction stir spot welding include a nearly 80% melting temperature that lowers the thermal deformation welds without splashing compared to resistance spot welding. Friction stir spot welding includes 3 steps: plunging, stirring, and retraction. In the present study, other materials including high strength steel are also used in the friction stir welding method to create joints. DP780, whose traditional welding process involves the use of resistance spot welding, is one of several high strength steel materials used in the automotive industry. In this paper, DP780 was used for friction stir spot welding, and its microstructure and microhardness were measured. The microstructure data showed that there was a fusion zone with fine grain and a heat effect zone with island martensite. The microhardness results indicated that the center zone exhibited a greater degree of hardness compared with the base metal. All data indicated that the friction stir spot welding used in dual phase steel 780 can create a good lap joint. In the future, friction stir spot welding can be used in high-strength steel welding applied in industrial manufacturing processes.

Here, we present a friction stir spot welding (FSSW) protocol on dual phase 780 steel. A tool pin with high-speed rotation generates heat from friction to soften the material, and then, the pin plunges into 2 sheet joints to create the lap joint.

通过 DP780 钢上的摩擦搅拌点焊生成圈接头

Friction stir spot welding (FSSW), a derivative of friction stir welding (FSW), is a solid-state welding technique that was developed in 1991. An industry ...

Cutting Procedures, Tensile Testing, and Ageing of Flexible Unidirectional Composite Laminates

Many body armor designs incorporate unidirectional (UD) laminates. UD laminates are constructed of thin (&#60;0.05 mm) layers of high-performance yarns, where the yarns in each layer are oriented parallel to each other and held in place using binder resins and thin polymer films. The armor is constructed by stacking the unidirectional layers in different orientations. To date, only very preliminary work has been performed to characterize the ageing of the binder resins used in unidirectional laminates and the effects on their performance. For example, during the development of the conditioning protocol used in the National Institute of Justice Standard-0101.06, UD laminates showed visual signs of delamination and reductions in V50, which is the velocity at which half of the projectiles are expected to perforate the armor, after ageing. A better understanding of the material property changes in UD laminates is necessary to comprehend the long-term performance of armors constructed from these materials. There are no current standards recommended for mechanically interrogating unidirectional (UD) laminate materials. This study explores methods and best practices for accurately testing the mechanical properties of these materials and proposes a new test methodology for these materials. Best practices for ageing these materials are also described.

The goal of the study was to develop protocols to prepare consistent specimens for accurate mechanical testing of high-strength aramid or ultra-high-molar-mass polyethylene-based flexible unidirectional composite laminate materials and to describe protocols for performing artificial ageing on these materials.

柔性单向复合层压板的切割程序、拉伸测试和老化

Many body armor designs incorporate unidirectional (UD) laminates. UD laminates are constructed of thin (&#60;0.05 mm) layers of high-performance yarns, ...

Determination of the Mechanical Properties of Flexible Connectors for Use in Insulated Concrete Wall Panels

This document contains recommendations for performing a non-standard, double-shear test suitable for both continuous and discrete insulated concrete sandwich wall panels (ICSWPs). Such a standardized test does not exist, but several iterations of this and similar tests have been performed in the literature to varying degrees of success. Further, the tests in the literature are rarely-if ever-described in detail or discussed at length with respect to the testing, data analysis, or safety procedures. A test specimen configuration is recommended herein, and variations are discussed. Important mechanical properties are identified from the load versus displacement data, and their extraction is detailed. The use of test data for design, such as for determining the stiffness of the connectors, is briefly demonstrated to show how ICSWP deflection and cracking behavior may be calculated. The strength behavior of panels may be determined using the full load versus displacement curve or only the maximum connector strength. Shortcomings and unknowns are acknowledged, and significant future work is delineated.

We propose a testing protocol that can be combined with widely available analytical methods to assess the mechanical properties of shear connectors for use in the design of insulated concrete wall panels to predict full-scale insulated panel behavior.

用于隔热混凝土墙板的柔性连接器的机械性能测定

This document contains recommendations for performing a non-standard, double-shear test suitable for both continuous and discrete insulated concrete ...

Mechanoluminescent Visualization of Crack Propagation for Joint Evaluation

In this study, methods for the mechanoluminescent (ML) visualization of crack propagation and mechanical behavior to evaluate adhesive joints are demonstrated and explained. The first step involved sample preparation; an air spray was used to apply ML paint to the surface of the adhesive joint specimens. The performance of the ML sensor was described to examine the measurement conditions. The results of ML sensing during a double cantilever beam (DCB) test and a lap-shear (LS) test are demonstrated as these are the most frequently and widely used methods for evaluating adhesives. Originally, it was difficult to directly quantify the crack tip and strain/stress distribution and concentration because the crack tip was too small, and the effects of the strain could not be observed. The mechanoluminescence, crack propagation, and mechanical behavior during mechanical testing can be visualized via the ML pattern during the adhesive evaluation. This allows for the recognition of the precise position of the crack tips and other mechanical behaviors related to structural failure.

In this study, a protocol is presented that describes the use of mechanoluminescent (ML) visualization for monitoring crack propagation and mechanical behavior during adhesive joint evaluation testing.

裂纹扩展的机械发光可视化用于联合评估

In this study, methods for the mechanoluminescent (ML) visualization of crack propagation and mechanical behavior to evaluate adhesive joints are ...

纤维复合材料层压板的制造和机械性能评估

Measuring the Mechanical Properties of Glass Fiber Reinforcement Polymer Composite Laminates Obtained by Different Fabrication Processes

The traditional wet hand lay-up process (WL) has been widely applied in the manufacturing of fiber composite laminates. However, due insufficiency in the forming pressure, the mass fraction of fiber is reduced and lots of air bubbles are trapped inside, resulting in low-quality laminates (low stiffness and strength). The wet hand lay-up/vacuum bag (WLVB) process for the fabrication of composite laminates is based on the traditional wet hand lay-up process, using a vacuum bag to remove air bubbles and provide pressure, and then carrying out the heating and curing process. 
Compared with the traditional hand lay-up process, laminates manufactured by the WLVB process show superior mechanical properties, including better strength and stiffness, higher fiber volume fraction, and lower void volume fraction, which are all benefits for composite laminates. This process is completely manual, and it is greatly influenced by the skills of the preparation personnel. Therefore, the products are prone to defects such as voids and uneven thickness, leading to unstable qualities and mechanical properties of the laminate. Hence, it is necessary to finely describe the WLVB process, finely control steps, and quantify material ratios, in order to ensure the mechanical properties of laminates. 
This paper describes the meticulous process of the WLVB process for preparing woven plain patterned glass fiber reinforcement composite laminates (GFRPs). The fiber volume content of laminates was calculated using the formula method, and the calculated results showed that the fiber volume content of WL laminates was 42.04%, while that of WLVB laminates was 57.82%, increasing by 15.78%. The mechanical properties of the laminates were characterized using tensile and impact tests. The experimental results revealed that with the WLVB process, the strength and modulus of the laminates were enhanced by 17.4% and 16.35%, respectively, and the specific absorbed energy was increased by 19.48%.

作者聚焦：使用湿法手糊/真空袋工艺提高纤维复合材料层压板质量 

This paper describes a fabrication process for fiber-reinforced polymer matrix composite laminates obtained using the wet hand lay-up/vacuum bag method.

测量通过不同制造工艺获得的玻璃纤维增强聚合物复合层压板的机械性能

The traditional wet hand lay-up process (WL) has been widely applied in the manufacturing of fiber composite laminates. However, due insufficiency in the ...