Thanks to the Defense Spectrum Office (DSO) for funding the work presented in this article.

NOTE: The ITS channel sounder system is shown in Figure 1 and Figure 2, and a benchtop evaluation setup is shown in Figure 3. Reference these figures while setting up the CW-channel sounder to ensure all components are properly configured. The following sections explain how to verify and validate a system prior to making measurements.
1. Measurement system setup
NOTE: This section describes how a system is set up for field measurements. First, system losses in both the transmitting and the receiving side of the system must be accounted for and measured separately before the full system is assembled. Then, the full system is assembled, and individual instruments are configured, calibrated, and synchronized to prepare for lab verification and validation.
<ol>
	<li>Measure the S-parameters, using a VNA2, for individual system components before assembling the system: cables, attenuators, power splitters, directional couplers, and low-pass filters. 
	NOTE: This will characterize losses and identify broken cables, or a device out of specification.</li>
	<li>Assemble the Type N cable at the output of the power amplifier, the directional coupler, the bandpass filter, and the Type N cable that will be connected to the antenna, and use the VNA to measure the component chain. 
	NOTE: This measurement will include internal reflections that are not seen by measuring individual components with a VNA.</li>
	<li>Record the S21 value, which will be a negative number, and will be used as the transmitting system losses. Use these values to correct the received signal level discussed in the representative results section.</li>
	<li>Transmitting system setup
	<ol>
		<li>Plug in all devices to a power source: either an uninterruptible power supply (UPS) or a surge-protected set of outlets. Make sure that all instruments are in a powered off state while hooking components together.</li>
		<li>Assemble the transmitting equipment (Figure 1).
		<ol>
			<li>Connect the 10 MHz output of the rubidium oscillator to the Ref IN port of the VSG using a Bayonet-Neill-Concelman (BNC) cable. Connect RF OUT port of the VSG to the input of the directional coupler IN port using a Type N cable. No power amplifier is inserted until Protocol Step 3.2.</li>
			<li>Connect the OUT port of the directional coupler to the input port appropriate bandpass filter (if needed) using a Type N female to female connector. 
			NOTE: A bandpass filter is used to minimize harmonic frequencies in other bands.</li>
		</ol>
		</li>
	</ol>
	</li>
	<li>Assemble the Type N cable that will be connected to the receiving antenna, the filter, the cable between the filter and the power splitter, and the Type N cable that will be connected to the VSA; use the VNA to measure this system of components.</li>
	<li>Make the same measurement, but through the same components connected to the SA. Record the S21 values, which will be used as the receiving system losses on the VSA side of the power splitter and the SA side of the power splitter. Use these values to correct the received signal level discussed in the representative results section.</li>
	<li>Receiving system setup
	<ol>
		<li>Plug in all devices to a power source: either a UPS or a surge-protected set of outlets. Make sure all instruments are in a powered off state while hooking components together.</li>
		<li>Assemble the receiving equipment (Figure 2).
		<ol>
			<li>Connect a Type N cable to the input of the bandpass filter. Connect the output of the bandpass filter to the input of the power divider (port 1).</li>
			<li>Connect port 2 of the power divider to the RF IN port on the VSA. Connect port 3 of the power divider to the RF IN port on the SA.</li>
			<li>Using a BNC to banana plug cord, connect the Frequency Adj of the rubidium oscillator to the DC OUT of the direct-current (DC) power supply.</li>
			<li>Connect a 10 MHz output of the rubidium oscillator to the Ext Ref In port on the VSA using a BNC cable. Connect a 10 MHz output of the rubidium oscillator to the Ext Trig/Ref In port on the spectrum analyzer.</li>
		</ol>
		</li>
	</ol>
	</li>
	<li>Power on the VSG and ensure that it is set to RF OFF. Power on the power meter. Turn all instruments on, and allow the instruments to warm up for an hour before making any measurements.</li>
	<li>Configure the VSA in VSA 89601B mode. While in VSA mode, set the center frequency to the CW frequency of interest. Finally, select the number of points taken with the desired length of the overall measurement in mind. 
	&#8203;NOTE: Although the system operates using a CW, the span must be set to capture any Doppler shifts and fading. The resolution bandwidth determines the filter used by the VSA to measure power as it sweeps across the frequency span, so selecting a low-resolution bandwidth allows a more precise measurement. As a tradeoff, a lower resolution bandwidth takes a greater time per point.</li>
	<li>Configure the VSA with the following settings: select VSA 89601B mode; center Frequency: Freq MHz (e.g., 1770 MHz); span: 3 kHz; TimeLen: 1 s; ResBW: 3.81938 Hz; NumPts: max (491026 pts, 409601 pts)-depends on VSA; Rng: -42 dBm; top graph upper scale value: -30 dBm.</li>
	<li>Ensure that the SA is controlled by instrument control software that uses programmable standard commands for programmable instruments (SCPI) commands, so that continuous sweeps can be collected and saved.
	<ol>
		<li>Set the SA such that the start and stop frequencies match the VSA center frequency. As the RBW similarly determines the filter size used by the SA, set the RBW to the same value as the span of the VSA measurement.</li>
		<li>Set the video bandwidth to the same value as the resolution bandwidth and the detection mode to sample to record unaveraged data. Leave attenuation off, making sure the SA will not be overloaded, and keep the preamp on.</li>
		<li>Configure the SA with the following for each sweep: StartFreq: Same center frequency as in the VSA setup (e.g., 1770 MHz); StopFreq: Same center frequency as in the VSA setup (e.g., 1770 MHz); RBW (MHz): 0.003; VBW (MHz): 0.003; detector: sample; sweep time: 500 ms; pts/trace: 461; preamp ON; attenuation: 0; auto attenuation: Off.</li>
		<li>On the SA, press Enter to access the menus. Enable External Reference by pressing the Shift button and selecting the System button on the spectrum analyzer. Then, select More | Port Settings | Ext Input | Ref using the softkeys near the screen.</li>
	</ol>
	</li>
	<li>Configure the VSG by selecting a CW output.
	<ol>
		<li>Set the frequency to 1770 MHz. Follow the procedure in section 4.22 to determine the linear range of the power amplifier.</li>
		<li>Set the VSG output amplitude to -4 dBm, the upper limit to the linear range of the power amplifier.</li>
	</ol>
	</li>
	<li>Calibrate the power meter.
	<ol>
		<li>Plug the power meter head into the reference port (channel A or B) and the other end of the power meter into a measurement port.</li>
		<li>Set the power meter frequency to 1770 MHz for the reference port used above. Zero and calibrate the power meter. Ensure the power meter reading remains within 0.2 dB of 0 dBm.</li>
		<li>Unplug the power meter head from the reference port, and connect the power meter head to the output of the attenuator shown in Figure 1.</li>
	</ol>
	</li>
	<li>Calibrate the VSA: Utilities | Calibration | Calibration. Turn RF ON the VSG. 
	&#8203;NOTE: Make sure there is a signal on the spectrum analyzer. If the signal level drops down to -120 dBm, the external reference is not on. If the signal is too strong, it will overload the receiving system and damage either the VSA or SA. Be aware of maximum input signal levels (usually shown on the front of the instrument), and stay at least 10 dB below this level.</li>
	<li>Synchronize the rubidium oscillators by setting the voltage, but do not exceed the maximum input voltage allowed on the rubidium synchronization port.
	<ol>
		<li>Change TimeLen on the top graph on the VSA screen to 100 ms. Set the y-axis on the bottom plot to I-Q.</li>
		<li>Press Current/Voltage on the front panel of the power supply. Change the voltage a little at a time and watch the dot on the VSA screen: if it rotates back and forth, do nothing, the frequencies are aligned. If it rotates in one direction consistently, change the power meter reading (voltage) until the dot on the I-Q plot starts to slow down, and it moves slowly back and forth (pendulum motion) (Figure 4).</li>
		<li>Set TimeLen on the top graph on the VSA screen back to 1 s, and set the y-axis back to Log Magnitude.</li>
	</ol>
	</li>
	<li>Take 10 records of acquisition on the SA to verify that all parameters have been set correctly, and that the signal level on the SA screen matches the signal level on the VSA lower screen.</li>
</ol>
2. Lab verification and validation
<ol>
	<li>Without attaching antennas, insert a variable attenuator between the transmitting side of the system and the receiving side of the system (Figure 5). Remove the power amplifier from the measurement setup for this verification.</li>
	<li>Set the stepped attenuator attenuation to 0 dB and the number of records on the VSA Input &#62; Recording to 120. 
	NOTE: One record is equal to the TimeLen set on the VSA.</li>
	<li>Set the number of sweeps on the SA to 120 records. Change the output amplitude of the VSG to 0 dBm, and press the RF ON button on the VSG.</li>
	<li>Set a peak marker to find the value of the signal strength, and verify a signal is seen on the VSA. Start the VSA by hitting the Record button at the top of the screen. Start an SA measurement using the instrument control software.</li>
	<li>Change the stepped attenuator to 10 dB, and repeat steps 4-10. Go through all settings of the stepped attenuator and record the values for each attenuation setting. 
	NOTE: As the attenuator approaches 90 to 110 dB, the signal will get noisier as it approaches the system noise floor of the instrument. Measurement values near the noise floor of the system will be highly variable.</li>
	<li>To verify the VSA received signal levels, calculate a 0.5 s windowed average to the 120 s VSA record, and average each sweep of the SA. Add the VSG output power level, the transmitting side and receiving side system losses, and the stepped attenuator setting. 
	NOTE: The value of the aforementioned sum in step 2.6 should equal the averaged received signal levels recorded by the VSA and the SA within 0.5 dB, for stepped attenuations less than 80 dB. If they do not, go back and remeasure system losses.</li>
</ol>
3. Field measurements
NOTE: Always test and verify the system before every measurement campaign.
<ol>
	<li>Complete steps 1.1-1.3 before each new measurement campaign, and set up the transmitting side of the system, as discussed in section 1.4. 
	&#8203;NOTE: This is typically housed in a cellular-on-wheels (COW), which remains fixed during measurements.</li>
	<li>Connect the power amplifier between the VSG and the directional coupler, as described in step 1.4.2.1.
	<ol>
		<li>Use a directional coupler that can handle the power levels generated by the power amplifier. Add a 50 dB attenuator to the directional coupler at the coupled port to stay within the specified input power levels of the power meter, and attach the power meter to this port. Connect the output Type N cable from the directional coupler to the transmitting antenna.</li>
		<li>Set up the receiving side of the system, as discussed in steps 1.5-1.6, inside a mobile vehicle. Connect the receiving antenna to the Type N cable connected to the filter.</li>
		<li>In addition to the SA setup steps 1.11.3-1.11.4, the GPS antenna needs to be set up in the SA.
		<ol>
			<li>Enable the GPS record: Meas Settings | Enable GPS Record | Standard GPS.</li>
			<li>Enable GPS on the spectrum analyzer by holding the Shift button and selecting the System button on the spectrum analyzer. Then, select More | GPS | GPS-ON &#38; GPS Info-ON using the softkeys near the screen.</li>
			<li>Place the GPS antenna on the roof of the receiver measurement vehicle. Ensure that the measurement software also reads in NMEA strings from the GPS for each sweep.</li>
		</ol>
		</li>
	</ol>
	</li>
	<li>Continue the setup as discussed in steps 1.11-1.17, and set the number of records on the VSA Input | Recording based on estimated measurement time. Set the number of SA records to the number of VSA records plus about 300 records, noting that the SA sweeps slower than the VSA.</li>
	<li>Begin the measurement by first starting the VSA by pressing the Record button at the top of the screen. Initiate the spectrum analyzer measurement.</li>
	<li>After the measurement, save the VSA recording file | Save | Save Recording. Save Options | Save Headers with Data. When saving the file, append a _VSA to the end of the file. Change the name of the data file for the spectrum analyzer to match the filename of the VSA, but append _SA for the spectrum analyzer.</li>
</ol>

<ol>
	<li>Commerce Spectrum Management Advisory Commmittee. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=.">.</a> 1755-1850 MHz Airborne Operations: Air Combat Training System Sub-Working Group Final Report. , (2014).</li><li>Best practices for radio propagation measurements. NTIA Technical Memo TM-19-535. U.S. Dept. of Commerce Available from: <a target="_blank" href="https://www.its.bldrdoc.gov/publications/3211.aspx">https://www.its.bldrdoc.gov/publications/3211.aspx</a> (2018)</li><li>Hammerschmidt, C. A., Johnk, R. T., Tran, S. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Calibration+of+a+Vector+Network+Analyzer+for+Measurements+in+Radio+Frequency+Propagation+Channels.">Calibration of a Vector Network Analyzer for Measurements in Radio Frequency Propagation Channels.</a> Journal of Visualized Experiments. (160), e60874 (2020).</li><li>Channel sounder measurement verification: conducted tests. NTIA Joint Report JR-20-549. U.S. Department of Commerce Available from: <a target="_blank" href="https://www.its.bldrdoc.gov/publications/3241.aspx">https://www.its.bldrdoc.gov/publications/3241.aspx</a> (2020)</li><li>Molisch, A. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=.">.</a> Wireless communications. 2nd edition. , (2010).</li><li>Anderson, C. R. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Design+and+implementation+of+an+ultrabroadband+millimeter-wavelength+vector+sliding+correlator+channel+sounder+and+in-building+multipath+measurements+at+2.5+&amp;+60+GHz.">Design and implementation of an ultrabroadband millimeter-wavelength vector sliding correlator channel sounder and in-building multipath measurements at 2.5 &amp; 60 GHz.</a> Virginia Polytechnic Institute and State University. , (2002).</li><li>Johnk, R., Hammerschmidt, C. A., Stange, I. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=A+high-performance+CW+mobile+channel+sounder.">A high-performance CW mobile channel sounder.</a> Proceedings of the 2017 IEEE International Symposium on Electromagnetic Compatibility &amp; Signal/Power Integrity (EMCSI. , (2017).</li><li>Johnk, R., Hammerschmidt, C. A., McFarland, M. A., Lemmon, J. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=A+fast-fading+mobile+channel+measurement+system.">A fast-fading mobile channel measurement system.</a> Proceedings of the 2012 IEEE International Symposium on Electromagnetic Compatibility (EMC). , 584-587 (2012).</li><li>Vector signal analysis basics. Keysight Technologies Available from: <a target="_blank" href="https://www.keysight.com/us/en/assets/7018-02891/application-notes/5990-7451.pdf?success=true">https://www.keysight.com/us/en/assets/7018-02891/application-notes/5990-7451.pdf?success=true</a> (2020)</li><li>Johnk, R. T., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=A+mobile+propagation+measurement+system.">A mobile propagation measurement system.</a> Proceedings of the 2009 IEEE International Symposium on Electromagnetic Compatibility (EMC. , (2009).</li><li>. 3.5 GHz Exclusion zone analysis and methodology. NTIA Technical Report 15-517 Available from: <a target="_blank" href="https://www.its.bldrdoc.gov/publications/2805.aspx">https://www.its.bldrdoc.gov/publications/2805.aspx</a> (2015)</li><li>The national map. United States Geological Survey Available from: <a target="_blank" href="https://viewer.nationalmap.gov/basic">https://viewer.nationalmap.gov/basic</a> (2017)</li><li>Radiocommunication Sector of International Telecommunication Union. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Propagation+by+diffraction.">Propagation by diffraction.</a> Propagation by diffraction. ITU-R Recommendation. , 526 (2019).</li><li>Yoza, N. P. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Narrowband+5+GHz+mobile+channel+characterization.">Narrowband 5 GHz mobile channel characterization.</a> Interdisciplinary Telecommunications Program, University of Colorado at Boulder. , (2015).</li></ol>

It is very important to test a system as described in this protocol before attempting to make measurements in an outdoor environment. In this way, any bad components or instabilities can be traced and identified in the measurement system and can be resolved. The critical steps in this protocol are to 1) test the individual components first, and verify that they are operating within their specification, 2) assemble transmitting and receiving sides separately and test the chain of components, 3) assemble the transmitting and receiving side by inserting a stepped attenuator and measuring the signal levels as the attenuation is changed to make sure the received signal levels in the VSA and SA are as calculated. Further troubleshooting can be performed by using a VSG, such as the one shown in the Table of Materials, that has an option to generate fading simulations, which can be used to test the system using simulated waveforms in various fading environments encountered in real-world propagation environments. Once the measurement system is operating correctly, measurements can be made in an outdoor environment with the confidence that measurements will be accurate.
Another important step is to monitor the transmitting power throughout the measurement to verify that the system is operating correctly. The power amplifier is characterized and tested separately to understand its linearity and out-of-band emissions spectra. The power amplifier may be validated on the benchtop with the rest of the setup, but care must be taken to reduce the signal power below the maximum rated power input to the VSA using appropriately rated attenuators. Neither the GPS antenna nor its settings should be used for lab verification and validation. As the VSA&#39;s screen is not capable of providing real-time monitoring of the environment, the addition of an SA as a real-time monitor helps determine the current state of the system. There are several types of channel-sounding measurement systems to capture channel characteristics for radio systems: CW, direct pulse, frequency domain using a VNA, correlation-based, swept-time delay cross-correlator.
One limitation of this system is that a CW signal probing the local environment does not contain time-domain information such as time-delay profiles. A time-delay profile gives information about the timing of source reflections of the signal in the local environment. However, an advantage of using a CW signal is that it is easier to obtain permission to transmit on one frequency in various bands using the narrowband CW signal rather than trying to transmit a wide-band signal. CW systems can have a larger dynamic range than other systems, and the signal can usually propagate further in the environment. A CW signal also has audio sampling rates that result in smaller file sizes than other types of channel-sounding systems. With this system, data collections are continuous and can last for several hours. The CW-channel sounder measurement system discussed in this article can be used at different frequencies, depending on the range of the various assembled components. The system can be used in an outdoor propagation environment or an indoor propagation environment15.

The Institute for Telecommunication Sciences (ITS) is the research laboratory of the National Telecommunications and Information Administration (NTIA), an agency of the U.S. Department of Commerce. ITS has a long history of conducting accurate, well-regarded radio frequency (RF) propagation measurements. The increase in spectrum-sharing has been accompanied by the need for accurate, reproducible measurements that provide a better understanding of the radio environment that multiple services will have to share. For the past few years, the military services have been developing spectrum-sharing arrangements with commercial wireless carriers in the Advanced Wireless Services (AWS)-3 band (1755-1780 MHz)1. This will allow commercial wireless carriers to use the AWS-3 band prior to phasing military services out of the band. The use of the band will be coordinated by both isolating systems geographically and by modeling frequency interference scenarios. To share this band of spectrum, propagation measurements are necessary to develop and improve propagation models for the evaluation of RF interference between the military and commercial wireless systems within the band.
The Defense Spectrum Organization (DSO) is responsible for the management of the AWS-3 transition and has tasked ITS and others with performing a series of channel-sounding measurements. These measurements will be used to build new models for the calculation of the impact of foliage and man-made structures in the environment (collectively known as clutter). Improved propagation modeling that accounts for clutter could lead to fewer restrictions on commercial transmitters in the vicinity of military systems. The CW-channel-sounder system discussed in this article has been used for the past five years to collect radio propagation measurement data and calculate the clutter attenuation. This measurement system produces accurate, repeatable, and unbiased results, and DSO encouraged ITS to share its institutional knowledge-including best measurement practices for the measurement and processing of RF propagation data-with the wider technical community.
Best measurement practices require understanding a system from the component level to the assembled-system level. These best measurement practices have been documented in the recently published NTIA Technical Memorandum TM-19-5352 that describes a set of best practices for the preparation and verification of radio propagation measurement systems. ITS recently completed a JoVE article on calibrating a VNA used to measure component losses and identify bad components for this measurement system3. This article is a continuation in documenting these best measurement practices for the wider community. Although best practices are discussed in this article for a CW-channel sounder, these same techniques can be used to verify other channel sounder systems: VNA systems; CW systems; full-bandwidth, correlation-based systems; direct pulse systems; and sliding correlator-based systems4,5,6.
This article describes in detail how to setup a CW-channel sounder measurement system using a vector signal analyzer (VSA), a spectrum analyzer (SA), two rubidium oscillators, a power meter, a vector signal generator (VSG), and various filters and power dividers for measurements in an outdoor measurement environment7,8. The transmitting side of the system consists of the VSG, which generates a CW signal that is boosted by a power amplifier. This is then split by a directional couple to divert some of the signal to the power meter, which allows the user to monitor the system output. The rest of the signal is sent to the receiving side of the system via the propagation channel. The receiving side consists of a low-pass filter to reduce interference and harmonics produced by the power amplifier. The filtered signal is split in a power divider and fed into the SA for monitoring during the measurement along with a time stamp and Global Positioning System (GPS) location. The other half of the signal is sent to the VSA to be downconverted into in-phase quadrature (I-Q) data in the range of 1-5 kHz. The sampling rate is determined by the instrument span9 and is guided by the expected Doppler spectrum shifts, which are a function of the speed of the vehicle. The resulting time series is then transferred to a computer for postprocessing and data analysis.
Rubidium clocks are used at both the transmitter and receiver to provide highly accurate measurements and highly stable frequencies. The rubidium clock at the receiving end has a fine frequency adjustment for the precise alignment of the transmitting and receiving frequencies. Typically, the frequencies are adjusted to be within 0.1 Hz of each other for testing. Rubidium clocks are essential for high-accuracy CW propagation measurements. They ensure precise time base accuracy over the course of the measurements and prevent frequency drift of the transmitter and receiver. This article also details how to validate and verify that a system is making accurate measurements in a laboratory setting, both with and without an antenna, prior to making measurements in an outdoor environment. The system has been used for an extensive series of outdoor and indoor tests at frequencies ranging from 430 MHz to 5.5 GHz and for many different transmitting powers7,8,10.

<table border="1" fo:keep-together.within-page="1" fo:keep-with-next.within-page="always">
	<tbody>
		<tr>
			<td>Cabling</td>
			<td>Micro-Coax</td>
			<td></td>
			<td>Various lengths</td>
		</tr>
		<tr>
			<td>Directional Coupler</td>
			<td>Anatech Electronics, Inc.</td>
			<td></td>
			<td>AM1650DC833</td>
		</tr>
		<tr>
			<td>Filter 1</td>
			<td>K&#38;L Microwave, Inc.</td>
			<td></td>
			<td>8FV50-1802-T95-O/O</td>
		</tr>
		<tr>
			<td>GPS Antenna</td>
			<td>Trimble</td>
			<td></td>
			<td>SMA connection to SA</td>
		</tr>
		<tr>
			<td>Instrument Control &#38; Processing Software</td>
			<td>MATLAB</td>
			<td></td>
			<td>Used to store and process measurement data</td>
		</tr>
		<tr>
			<td>Power Amplifier</td>
			<td>Ophir RF</td>
			<td></td>
			<td>5263-003</td>
		</tr>
		<tr>
			<td>Power Divider</td>
			<td>Mini-Circuits</td>
			<td></td>
			<td>ZAPD-20+</td>
		</tr>
		<tr>
			<td>Power Meter and Power Sensor</td>
			<td>Keysight</td>
			<td></td>
			<td>E4417A/E4412A</td>
		</tr>
		<tr>
			<td>Receiving Antenna</td>
			<td>Cobham</td>
			<td></td>
			<td>OA2-0.3-10.0V/1505</td>
		</tr>
		<tr>
			<td>Rubidium Frequency Standard</td>
			<td>Stanford Research Systems</td>
			<td></td>
			<td>FS725</td>
		</tr>
		<tr>
			<td>SA</td>
			<td>Agilent</td>
			<td></td>
			<td>N9344C</td>
		</tr>
		<tr>
			<td>Transmitting Antenna</td>
			<td>COMTELCO</td>
			<td></td>
			<td>BS1710XL6</td>
		</tr>
		<tr>
			<td>Vector Signal Generator</td>
			<td>Rohde &#38; Schwarz</td>
			<td></td>
			<td>SMIQ</td>
		</tr>
		<tr>
			<td>VSA</td>
			<td>Keysight Technologies</td>
			<td></td>
			<td>N9030A</td>
		</tr>
	</tbody>
</table>

continuous-wave propagation channel-sounding measurement system - testing, verification, and measurements

Channel sounders are used to measure channel characteristics for radio systems. There are several types of channel sounders used today: continuous-wave (CW), direct pulse, frequency domain using a vector network analyzer (VNA), correlation-based, and swept-time delay cross-correlator. Each of these has unique advantages and disadvantages. CW systems have a larger dynamic range than other systems with a signal that can propagate further into the environment. As the audio sampling rates allow smaller file sizes than other systems, data collection can be continuous and last for several hours. This article discusses a CW-channel sounder system, which has been used to make numerous propagation loss measurements in various cities in the United States of America. Such propagation measurements should be accurate, reproducible, and free of artifacts or biases. This article shows how to set up the measurement, how to validate and verify that the system is making reliable measurements, and finally, it shows results from some of the measurement campaigns such as repeatability measurements, clutter loss measurements (where clutter loss is defined as the excess loss from free-space transmission loss), and reciprocity measurements.

The following results were obtained during a field verification of the presented system. The transmitter was located on the Kohler Mesa behind the Department of Commerce Boulder Laboratories in Boulder, Colorado. The receiver was driven through Boulder, Colorado, in a specially designed measurement vehicle (see Figure 6), and continuous measurements were taken. The SA stores the swept data as log magnitude format in an event data structure, while the GPS data are stored in a separate event data structure within in the same file. An example of data for one sweep is shown in Figure 7. The stored data are converted to linear power in Watts; a mean is computed for all points in that sweep and then converted back to log magnitude. The GPS information is assigned to this mean value for the sweep shown by the red X at a value of &#8722;71.5 dBm. This process is done for every sweep in the file.
Next, the baseband I-Q data from the VSA are processed as shown in equation 1. The power in dBm is calculated for every I-Q sample. The VSA collects peak data, which must be converted to dBm, during this step.
<img alt="Equation 1" src="/files/ftp_upload/62124/62124eq01.jpg" />(1)
During the measurement, the baseband I-Q data are stored in a temporary file. No GPS information is acquired by the VSA. The length of the file is chosen such that the number of records requested is equal to the number of seconds of drive time. Once the measurement has finished, the data are written to a file whose structure is preprogrammed by the VSA software developers. Data saved into this file include the time difference between measurement samples, the frequency, and the complex data samples. The processing step involves the smoothing of the magnitude of the baseband I-Q data over a 500 ms window for the entire data set to approximate a 40-wavelength driving distance. Figure 8 shows how the smoothed mean power compares to the raw data for a larger portion of a drive test. The raw data are shown by the blue trace, and the smoothed mean power is shown by the red trace.
The VSA and SA data sets are aligned using a circular convolution. The VSA data point at each second is aligned with the SA samples generated at each second to transfer the GPS coordinates from the SA to the VSA data points. A linear regression model aligns the data by minimizing the residuals between the measured power levels of the two data sets. The aligned data are presented by plotting the SA power in dBm on the x-axis and the VSA power in dBm on the y-axis (Figure 9). As the SA system noise floor is higher than the VSA system noise floor, the graph will show a downward curvature at points below approximately -115 dBm for data sets close to the noise floor. Figure 9 and Figure 10 show&#160;the alignment of the VSA power and the SA power vs. the elapsed time in seconds. The GPS time stamp from the SA mean power is then attached to the first data point of the VSA average-smoothed power data series. The vertical offset between the two data sets is eliminated by correcting for cable loss from the power divider to the SA; however, as only the time-stamped VSA data are used, this extra step is unnecessary. These data are then saved and used in the Longley-Rice/Irregular Terrain Model (ITM)11,12 to predict terrain losses. The VSA data are corrected by adding system losses and removing system gains to obtain the measured basic transmission loss (BTL) or basic transmission gain (BTG) along the drive route as shown in Figure 11 and Figure 12 and given by equation 2.
<img alt="Equation 2" src="/files/ftp_upload/62124/62124eq02.jpg" />(2)
where, BTL is the basic transmission loss, Pt and Pr are the transmitting and receiving powers in dBm, Gt and Gr are the gains of the transmitting and receiving antennas in dBi, respectively, and Lt and Lr are the system losses for the transmitting system and receiving system in dB, respectively.
In Figure 11, the purple star is the transmitting location. The yellow and purple dots represent the highest and lowest received signal levels, respectively. A plot of the measured BTG (black x&#39;s), the ITM-modelled BTG (blue +&#39;s), free-space transmission gain (FSTG) (red circles), and the system noise floor (pink dots) is shown in Figure 12. When the ITM BTG equals the FSTG, there are no terrain interactions, and all losses (difference between FSTG and MBTG)&#160; can be assumed to come from buildings, foliage, or other interactions with the surrounding environment. This is shown in Figure 13, where the black line is the terrain pulled from the USGS terrain database13, the red, dashed line is the line-of-sight (LOS) line between the transmitting antenna and the receiving antenna, and the blue, dotted and dashed lines are the upper and lower first Fresnel zones14 where most of the energy is localized.
<img alt="Figure 1" class="xfigimg" src="/files/ftp_upload/62124/62124fig01.jpg" /> 
Figure 1:&#160;Diagram of transmitting components and connections. Transmitting side of continuous-wave (CW)-channel sounder. Abbreviations: RF = radio frequency; Ref = reference. <a href="https://www.jove.com/files/ftp_upload/62124/62124fig01large.jpg" target="_blank">Please click here to view a larger version of this figure.</a>
<img alt="Figure 2" class="xfigimg" src="/files/ftp_upload/62124/62124fig02.jpg" /> 
Figure 2:&#160;Diagram of receiving components and connections. Receiving side of continuous-wave (CW) channel sounder. Abbreviations: GPS = Global Positioning System; RF = radio frequency; Ext Ref = external reference; GPS Ant = GPS antenna; Ext Trig/Ref = external Trigger/Reference; TCP/IP = transmission control protocol/internet protocol; Freq Adj = Frequency-adjusted; DC = direct current. <a href="https://www.jove.com/files/ftp_upload/62124/62124fig02large.jpg" target="_blank">Please click here to view a larger version of this figure.</a>
<img alt="Figure 3" class="xfigimg" src="/files/ftp_upload/62124/62124fig03.jpg" /> 
Figure 3: CW channel sounder system in laboratory. A benchtop deployment of the Institute for Telecommunication Sciences (ITS) channel sounder for system validation and accuracy testing showing the main components. Abbreviations: VSA = vector signal analyzer; VSG = vector signal generator. <a href="https://www.jove.com/files/ftp_upload/62124/62124fig03large.jpg" target="_blank">Please click here to view a larger version of this figure.</a>
<img alt="Figure 4" class="xfigimg" src="/files/ftp_upload/62124/62124fig04.jpg" /> 
Figure 4:&#160;I-Q display. Frequency adjustment using in-phase and quadrature (I-Q) plot. Abbreviations: CW = continuous-wave; TimeLen = time length; I-axis = in-phase axis; Q-axis = quadrature axis. <a href="https://www.jove.com/files/ftp_upload/62124/62124fig04large.jpg" target="_blank">Please click here to view a larger version of this figure.</a>
<img alt="Figure 5" class="xfigimg" src="/files/ftp_upload/62124/62124fig05.jpg" /> 
Figure 5:&#160;Verification and validation system setup. System setup for verification and validation measurements. Abbreviations: I-Q = in-phase quadrature; RF = radio frequency; Ref = reference; GPS = Global Positioning System; Ext Trig/Ref = external trigger/Reference; TCP/IP = transmission control protocol/internet protocol; Freq Adj = frequency adjusted; DC = direct current. <a href="https://www.jove.com/files/ftp_upload/62124/62124fig05large.jpg" target="_blank">Please click here to view a larger version of this figure.</a>
<img alt="Figure 6" class="xfigimg" src="/files/ftp_upload/62124/62124fig06.jpg" /> 
Figure 6:&#160;Cellular-on-wheels (COW) and measurement van. Photo showing green van used for receiving system and cellular-on-wheels (COW) used to house transmitting system. <a href="https://www.jove.com/files/ftp_upload/62124/62124fig06large.jpg" target="_blank">Please click here to view a larger version of this figure.</a>
<img alt="Figure 7" class="xfigimg" src="/files/ftp_upload/62124/62124fig07.jpg" /> 
Figure 7:&#160;Spectrum analyzer sweep and sweep average. Single sweep for spectrum analyzer data capture consisting of 461 points over a 0.5 s sweep time. Abbreviation: SA = spectrum analyzer. <a href="https://www.jove.com/files/ftp_upload/62124/62124fig07large.jpg" target="_blank">Please click here to view a larger version of this figure.</a>
<img alt="Figure 8" class="xfigimg" src="/files/ftp_upload/62124/62124fig08.jpg" /> 
Figure 8:&#160;Vector signal analyzer received power and moving average. In-phase and quadrature (I-Q) magnitude data (blue trace) for a small slice of a larger run compared to the mean power (red trace) calculated over a 0.5 s window. <a href="https://www.jove.com/files/ftp_upload/62124/62124fig08large.jpg" target="_blank">Please click here to view a larger version of this figure.</a>
<img alt="Figure 9" class="xfigimg" src="/files/ftp_upload/62124/62124fig09.jpg" /> 
Figure 9:&#160;VSA and SA signal alignment. Alignment of vector signal analyzer power and spectrum analyzer power. Abbreviations: VSA = vector signal analyzer; SA = spectrum analyzer. <a href="https://www.jove.com/files/ftp_upload/62124/62124fig09large.jpg" target="_blank">Please click here to view a larger version of this figure.</a>
<img alt="Figure 10" class="xfigimg" src="/files/ftp_upload/62124/62124fig10.jpg" /> 
Figure 10:&#160;VSA and SA received power after signal alignment. Aligned vector signal analyzer power and spectrum analyzer power vs elapsed time in seconds. Abbreviations: VSA = vector signal analyzer; SA = spectrum analyzer. <a href="https://www.jove.com/files/ftp_upload/62124/62124fig10large.jpg" target="_blank">Please click here to view a larger version of this figure.</a>
<img alt="Figure 11" class="xfigimg" src="/files/ftp_upload/62124/62124fig11.jpg" /> 
Figure 11:&#160;Geolocation of measured basic transmission gain. Measured basic transmission gain along the drive route. <a href="https://www.jove.com/files/ftp_upload/62124/62124fig11large.jpg" target="_blank">Please click here to view a larger version of this figure.</a>
<img alt="Figure 12" class="xfigimg" src="/files/ftp_upload/62124/62124fig12.jpg" /> 
Figure 12:&#160;Measured and modelled basic transmission gain.&#160;Measured basic transmission gain (blue x&#39;s), Irregular-Terrain Model (ITM) basic transmission gain (BTG) (black +&#39;s), free-space transmission gain (red circles), and system noise floor (pink dots) vs. elapsed time along the drive route. Abbreviations: MBTG = Measured basic transmission gain; ITM = Irregular-Terrain Model. <a href="https://www.jove.com/files/ftp_upload/62124/62124fig12large.jpg" target="_blank">Please click here to view a larger version of this figure.</a>
<img alt="Figure 13" class="xfigimg" src="/files/ftp_upload/62124/62124fig13.jpg" /> 
Figure 13:&#160;Terrain profile and first Fresnel zone. United States Geological Survey terrain profile (black line) for elapsed time 1636.2 s. The upper (first) Fresnel zone (blue, dotted line) and lower (first) Fresnel zone (blue, dashed line) are also plotted along with the line-of-sight line (red, dashed line) between the transmitting antenna and receiving antenna. Abbreviations: USGS = United States Geological Survey; NED = national elevation database. <a href="https://www.jove.com/files/ftp_upload/62124/62124fig13large.jpg" target="_blank">Please click here to view a larger version of this figure.</a>

Watch this Scientific Journal Video about Continuous-Wave Propagation Channel-Sounding Measurement System - Testing, Verification, and Measurements at JoVE.com

Continuous-Wave Propagation Channel-Sounding Measurement System - Testing, Verification, and Measurements

This report describes the setup, validation and verification, and results from propagation measurements using a continuous-wave, radio frequency channel-sounding measurement system.

Channel sounders are used to measure channel characteristics for radio systems. There are several types of channel sounders used today: continuous-wave ...

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2.8K Views.  Institute for Telecommunication Sciences. This report describes the setup, validation and verification, and results from propagation measurements using a continuous-wave, radio frequency channel-sounding measurement system.

Video: Continuous-Wave Propagation Channel-Sounding Measurement System - Testing, Verification, and Measurements

Quantum State Engineering of Light with Continuous-wave Optical Parametric Oscillators

Engineering non-classical states of the electromagnetic field is a central quest for quantum optics1,2. Beyond their fundamental significance, such states are indeed the resources for implementing various protocols, ranging from enhanced metrology to quantum communication and computing. A variety of devices can be used to generate non-classical states, such as single emitters, light-matter interfaces or non-linear systems3. We focus here on the use of a continuous-wave optical parametric oscillator3,4. This system is based on a non-linear &#967;2 crystal inserted inside an optical cavity and it is now well-known as a very efficient source of non-classical light, such as single-mode or two-mode squeezed vacuum depending on the crystal phase matching. 
Squeezed vacuum is a Gaussian state as its quadrature distributions follow a Gaussian statistics. However, it has been shown that number of protocols require non-Gaussian states5. Generating directly such states is a difficult task and would require strong &#967;3 non-linearities. Another procedure, probabilistic but heralded, consists in using a measurement-induced non-linearity via a conditional preparation technique operated on Gaussian states. Here, we detail this generation protocol for two non-Gaussian states, the single-photon state and a superposition of coherent states, using two differently phase-matched parametric oscillators as primary resources. This technique enables achievement of a high fidelity with the targeted state and generation of the state in a well-controlled spatiotemporal mode.

We describe the reliable generation of non-Gaussian states of traveling optical fields, including single-photon states and coherent state superpositions, using a conditional preparation method operated on the non-classical light emitted by optical parametric oscillators. Type-I and type-II phase-matched oscillators are considered and common procedures, such as the required frequency filtering or the high-efficiency quantum state characterization by homodyning, are detailed.

Engineering non-classical states of the electromagnetic field is a central quest for quantum optics1,2. Beyond their fundamental significance, such states ...

Optical Trap Loading of Dielectric Microparticles In Air

We demonstrate a method to trap a selected dielectric microparticle in air using radiation pressure from a single-beam gradient optical trap. Randomly scattered dielectric microparticles adhered to a glass substrate are momentarily detached using ultrasonic vibrations generated by a piezoelectric transducer (PZT). Then, the optical beam focused on a selected particle lifts it up to the optical trap while the vibrationally excited microparticles fall back to the substrate. A particle may be trapped at the nominal focus of the trapping beam or at a position above the focus (referred to here as the levitation position) where gravity provides the restoring force. After the measurement, the trapped particle can be placed at a desired position on the substrate in a controlled manner. 
In this protocol, an experimental procedure for selective optical trap loading in air is outlined. First, the experimental setup is briefly introduced. Second, the design and fabrication of a PZT holder and a sample enclosure are illustrated in detail. The optical trap loading of a selected microparticle is then demonstrated with step-by-step instructions including sample preparation, launching into the trap, and use of electrostatic force to excite particle motion in the trap and measure charge. Finally, we present recorded particle trajectories of Brownian and ballistic motions of a trapped microparticle in air. These trajectories can be used to measure stiffness or to verify optical alignment through time domain and frequency domain analysis. Selective trap loading enables optical tweezers to track a particle and its changes over repeated trap loadings in a reversible manner, thereby enabling studies of particle-surface interaction.

A protocol for launching and stably trapping selected dielectric microparticles in air is presented.

We demonstrate a method to trap a selected dielectric microparticle in air using radiation pressure from a single-beam gradient optical trap. Randomly ...

High-speed Continuous-wave Stimulated Brillouin Scattering Spectrometer for Material Analysis

Recent years have witnessed a significant increase in the use of spontaneous Brillouin spectrometers for non-contact analysis of soft matter, such as aqueous solutions and biomaterials, with fast acquisition times. Here, we discuss the assembly and operation of a Brillouin spectrometer that uses stimulated Brillouin scattering (SBS) to measure stimulated Brillouin gain (SBG) spectra of water and lipid emulsion-based tissue-like samples in transmission mode with &lt;10 MHz spectral-resolution and &lt;35 MHz Brillouin-shift measurement precision at &lt;100 ms. The spectrometer consists of two nearly counter-propagating continuous-wave (CW) narrow-linewidth lasers at 780 nm whose frequency detuning is scanned through the material Brillouin shift. By using an ultra-narrowband hot rubidium-85 vapor notch filter and a phase-sensitive detector, the signal-to-noise-ratio of the SBG signal is significantly enhanced compared to that obtained with existing CW-SBS spectrometers. This improvement enables measurement of SBG spectra with up to 100-fold faster acquisition times, thereby facilitating high spectral-resolution and high-precision Brillouin analysis of soft materials at high speed.

We describe the construction of a rapid continuous-wave-stimulated-Brillouin-scattering (CW-SBS) spectrometer. The spectrometer employs single-frequency diode-lasers and an atomic vapor notch-filter to acquire transmission spectra of turbid/non-turbid samples with high spectral-resolution at speeds up to 100-fold faster than those of existing CW-SBS spectrometers. This improvement enables high-speed Brillouin material analysis.

Recent years have witnessed a significant increase in the use of spontaneous Brillouin spectrometers for non-contact analysis of soft matter, such as ...

Subsurface Defect Localization by Structured Heating Using Laser Projected Photothermal Thermography

The presented method is used to locate subsurface defects oriented perpendicularly to the surface. To achieve this, we create destructively interfering thermal wave fields that are disturbed by the defect. This effect is measured and used to locate the defect. We form the destructively interfering wave fields by using a modified projector. The original light engine of the projector is replaced with a fiber-coupled high-power diode laser. Its beam is shaped and aligned to the projector&#39;s spatial light modulator and optimized for optimal optical throughput and homogeneous projection by first characterizing the beam profile, and, second, correcting it mechanically and numerically. A high-performance infrared (IR) camera is set up according to the tight geometrical situation (including corrections of the geometrical image distortions) and the requirement to detect weak temperature oscillations at the sample surface. Data acquisition can be performed once a synchronization between the individual thermal wave field sources, the scanning stage, and the IR camera is established by using a dedicated experimental setup which needs to be tuned to the specific material being investigated. During data post-processing, the relevant information on the presence of a defect below the surface of the sample is extracted. It is retrieved from the oscillating part of the acquired thermal radiation coming from the so-called depletion line of the sample surface. The exact location of the defect is deduced from the analysis of the spatial-temporal shape of these oscillations in a final step. The method is reference-free and very sensitive to changes within the thermal wave field. So far, the method has been tested with steel samples but is applicable to different materials as well, in particular to temperature sensitive materials.

This method aims at locating vertical subsurface defects. Here, we couple a laser with a spatial light modulator and trigger its video input to heat a sample surface deterministically with two anti-phased modulated lines while acquiring highly resolved thermal images. The defect position is retrieved from evaluating thermal wave interference minima.

The presented method is used to locate subsurface defects oriented perpendicularly to the surface. To achieve this, we create destructively interfering ...

Cutting Procedures, Tensile Testing, and Ageing of Flexible Unidirectional Composite Laminates

Many body armor designs incorporate unidirectional (UD) laminates. UD laminates are constructed of thin (&#60;0.05 mm) layers of high-performance yarns, where the yarns in each layer are oriented parallel to each other and held in place using binder resins and thin polymer films. The armor is constructed by stacking the unidirectional layers in different orientations. To date, only very preliminary work has been performed to characterize the ageing of the binder resins used in unidirectional laminates and the effects on their performance. For example, during the development of the conditioning protocol used in the National Institute of Justice Standard-0101.06, UD laminates showed visual signs of delamination and reductions in V50, which is the velocity at which half of the projectiles are expected to perforate the armor, after ageing. A better understanding of the material property changes in UD laminates is necessary to comprehend the long-term performance of armors constructed from these materials. There are no current standards recommended for mechanically interrogating unidirectional (UD) laminate materials. This study explores methods and best practices for accurately testing the mechanical properties of these materials and proposes a new test methodology for these materials. Best practices for ageing these materials are also described.

The goal of the study was to develop protocols to prepare consistent specimens for accurate mechanical testing of high-strength aramid or ultra-high-molar-mass polyethylene-based flexible unidirectional composite laminate materials and to describe protocols for performing artificial ageing on these materials.

Many body armor designs incorporate unidirectional (UD) laminates. UD laminates are constructed of thin (&#60;0.05 mm) layers of high-performance yarns, ...

Full-field Strain Measurements for Microstructurally Small Fatigue Crack Propagation Using Digital Image Correlation Method

A novel measurement approach is used to reveal the cumulative deformation field at a sub-grain level and to study the influence of microstructure on the growth of microstructurally small fatigue cracks. The proposed strain field analysis methodology is based on the use of a unique pattering technique with a characteristic speckle size of approximately 10 &#181;m. The developed methodology is applied to study the small fatigue crack behavior in body centered cubic (bcc) Fe-Cr ferritic stainless steel with a relatively large grain size allowing a high spatial measurement accuracy at the sub-grain level. This methodology allows the measurement of small fatigue crack growth retardation events and associated intermittent shear strain localization zones ahead of the crack tip. In addition, this can be correlated with the grain orientation and size. Thus, the developed methodology can provide a deeper fundamental understanding of the small fatigue crack growth behavior, required for the development of robust theoretical models for the small fatigue crack&#160;propagation in polycrystalline materials.

Microstructurally small fatigue crack growth behavior is investigated using a novel methodological approach combining crack growth rate measurement and strain-field analysis to reveal the cumulative deformation field at sub-grain level.

A novel measurement approach is used to reveal the cumulative deformation field at a sub-grain level and to study the influence of microstructure on the ...

Method Development for Contactless Resonant Cavity Dielectric Spectroscopic Studies of Cellulosic Paper

The current analytical techniques for characterizing printing and graphic arts substrates are largely ex situ and destructive. This limits the amount of data that can be obtained from an individual sample and renders it difficult to produce statistically relevant data for unique and rare materials. Resonant cavity dielectric spectroscopy is a non-destructive, contactless technique which can simultaneously interrogate both sides of a sheeted material and provide measurements which are suitable for statistical interpretations. This offers analysts the ability to quickly discriminate between sheeted materials based on composition and storage history. In this methodology article, we demonstrate how contactless resonant cavity dielectric spectroscopy may be used to differentiate between paper analytes of varying fiber species compositions, to determine the relative age of the paper, and to detect and quantify the amount of post-consumer waste (PCW) recycled fiber content in manufactured office paper.

A protocol for the non-destructive analysis of the fiber content and relative age of paper.

The current analytical techniques for characterizing printing and graphic arts substrates are largely ex situ and destructive. This limits the amount of ...

Calibration of Vector Network Analyzer for Measurements in Radio Frequency Propagation Channels

In situ measurements of radio frequency (RF) spectrum activity provide insight into the physics of radio frequency wave propagation and validate existing and new spectrum propagation models. Both of these parameters are essential to supporting and preserving interference-free spectrum sharing, as spectrum use continues to increase. It is vital that such propagation measurements are accurate, reproducible, and free of artifacts and bias. Characterizing the gains and losses of components used in these measurements is vital to their accuracy. A vector network analyzer (VNA) is a well-established, highly accurate, and versatile piece of equipment that measures both magnitude and phase of signals, if properly calibrated. This article details the best practices for calibrating a VNA. Once calibrated, it can be used to accurately measure components of a correctly configured propagation measurement (or channel sounding) system or can be used as a measurement system itself.

This protocol describes best practices for calibrating a vector network analyzer prior to use as an accurate instrument, intended to measure components of a radio frequency propagation measurement test system.

In situ measurements of radio frequency (RF) spectrum activity provide insight into the physics of radio frequency wave propagation and validate existing ...

Measuring Sub-23 Nanometer Real Driving Particle Number Emissions Using the Portable DownToTen Sampling System

The current particle size threshold of the European Particle Number (PN) emission standards is 23 nm. This threshold could change because future combustion engine vehicle technology may emit large amounts of sub-23 nm particles. The Horizon 2020 funded project DownToTen (DTT) developed a sampling and measurement method to characterize particle emissions in this currently unregulated size range. A PN measurement system was developed based on an extensive review of the literature and laboratory experiments testing a variety of PN measurement and sampling approaches. The measurement system developed is characterized by high particle penetration and versatility, which enables the assessment of primary particles, delayed primary particles, and secondary aerosols, starting from a few nanometers in diameter. This paper provides instruction on how to install and operate this Portable Emission Measurement System (PEMS) for Real Drive Emissions (RDE) measurements and assess particle number emissions below the current legislative limit of 23 nm.

Presented here is the DownToTen (DTT) portable emission measurement system to assess real driving automotive emissions of sub-23 nm particles.

The current particle size threshold of the European Particle Number (PN) emission standards is 23 nm. This threshold could change because future ...

Solution Blow Spinning of Polymeric Nano-Composite Fibers for Personal Protective Equipment

Light-weight, protective armor systems typically consist of high modulus (&#62;109 MPa) and high-strength polymeric fibers held in place with an elastic resin material (binder) to form a non-woven, unidirectional laminate. While significant efforts have focused on improving the mechanical properties of the high-strength fibers, little work has been undertaken to improve the properties of the binder materials. To improve the performance of these elastomeric polymer binders, a relatively new and simple fabrication process, known as solution blow spinning, was used. This technique is capable of producing sheets or webs of fibers with average diameters ranging from the nanoscale to the microscale. To achieve this, a solution blow spinning (SBS) apparatus has been designed and built in the laboratory to fabricate non-woven fiber mats from polymer elastomer solutions.
In this study, a commonly used binder material, a styrene-butadiene-styrene block-co-polymer dissolved in tetrahydrofuran, was used to produce nanocomposite fiber mats by adding metallic nanoparticles (NPs), such as iron oxide NPs, that were encapsulated with silicon oil and thus incorporated in the fibers formed via the SBS process. The protocol described in this work will discuss the effects of the various critical parameters involved in the SBS process, including the polymer molar mass, the selection of the thermodynamically appropriate solvent, the polymer concentration in solution, and the carrier gas pressure to assist others in performing similar experiments, as well as provide guidance to optimize the configuration of the experimental setup. The structural integrity and morphology of the resultant non-woven fiber mats were examined using scanning electron microscopy (SEM) and elemental X-ray analysis via energy-dispersive X-ray spectroscopy (EDS). The goal of this study is to evaluate the effects of the various experimental parameters and material selections to optimize the structure and morphology of the SBS fiber mats.

The primary goal of this study is to describe a protocol to prepare polymeric fiber mats with consistent morphology via solution blow spinning (SBS). We aim to use SBS to develop novel, tunable, flexible polymeric fiber nanocomposites for various applications, including protective materials, by incorporating nanoparticles in a polymer-elastomer matrix.

Light-weight, protective armor systems typically consist of high modulus (&#62;109 MPa) and high-strength polymeric fibers held in place with an elastic ...