We gratefully acknowledge the financial support of Deutsche Telekom Innovation Laboratories.

1. Preparing the System (Figure 4)
<ol>
	<li>Insert the laser diodes LD1 and LD2 in the specific mount and connect it with the current (LDC) and temperature controllers (TEC). Turn the devices on and check the functionality of the laser diodes with the optical spectrum analyzer. Usually, a telecom wavelength around 1,550 nm is used.</li>
	<li>Connect the laser diode to the modulators (IM/PM and MZM1) according to the setup in Figure 4. The optical connectors need to be cleaned before use, to ensure the...

<ol>
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C., Kim, J., Chuang, S. L. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Variable+optical+buffer+using+slow+light+in+semiconductor+nanostructures.">Variable optical buffer using slow light in semiconductor nanostructures.</a> Proc. IEEE. 91 (11), 1897-1810 (2003).</li><li>Gersen, H., Karle, T. J., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Real-space+observation+of+ultraslow+light+in+Photonic+Crystal+Waveguides.">Real-space observation of ultraslow light in Photonic Crystal Waveguides.</a> Phys. Rev. Lett. 94 (7), 073903-073907 (2005).</li><li>Th&#233;venaz, L. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Slow+and+fast+light+in+optical+fibres.">Slow and fast light in optical fibres.</a> Nature Photon. 2, 472-481 (2008).</li><li>Uskov, A. V., Sedgwick, F. G., Chang-Hasnian, C. J. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Delay+Limit+of+Slow+Light+in+Semiconductor+Optical+Amplifiers.">Delay Limit of Slow Light in Semiconductor Optical Amplifiers.</a> IEEE Photon. Technol. Lett. 18 (6), 731-733 (2006).</li><li>Schneider, T. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Time+Delay+Limits+of+stimulated-Brillouin-scattering-based+slow+light+systems.">Time Delay Limits of stimulated-Brillouin-scattering-based slow light systems.</a> Opt. Lett. 33 (13), 1398-1400 (2008).</li><li>Sharping, J., Okawachi, Y., van Howe, J., Xu, C., Wang, Y., Willner, A., Gaeta, A. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=All-optical,+wavelength+and+bandwidth+preserving,+pulse+delay+based+on+parametric+wavelength+conversion+and+dispersion.">All-optical, wavelength and bandwidth preserving, pulse delay based on parametric wavelength conversion and dispersion.</a> Opt. Express. 13 (20), 7872-7877 (2005).</li><li>Okawachi, Y., Foster, M., Chen, X., Turner-Foster, A., Salem, R., Lipson, M., Xu, C., Gaeta, A. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Large+tunable+delays+using+parametric+mixing+and+phase+conjugation+in+Si+nanowaveguides.">Large tunable delays using parametric mixing and phase conjugation in Si nanowaveguides.</a> Opt. Express. 16 (14), 10349-10357 (2008).</li><li>Kash, M. M., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Ultraslow+group+velocity+and+enhanced+nonlinear+optical+effects+in+a+coherently+driven+hot+atomic+gas.">Ultraslow group velocity and enhanced nonlinear optical effects in a coherently driven hot atomic gas.</a> Phys. Rev. Lett. 82 (26), 5229-5232 (1999).</li><li>Turukhin, A. V., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Observation+of+ultraslow+and+stored+light+pulses+in+a+solid.">Observation of ultraslow and stored light pulses in a solid.</a> Phys. Rev. Lett. 88 (2), 023602-023605 (2001).</li><li>Fleischhauer, M., Yelin, S. F., Lukin, M. D. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=How+to+trap+photons?+Storing+single-photon+quantum+states+in+collective+atomic+excitations.">How to trap photons? Storing single-photon quantum states in collective atomic excitations.</a> Opt. Commun. 179 (1-6), 395-410 (2000).</li><li>Zhu, Z., Gauthier, D. J., Boyd, R. W. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Stored+Light+in+an+Optical+Fiber+via+Stimulated+Brillouin+Scattering.">Stored Light in an Optical Fiber via Stimulated Brillouin Scattering.</a> Science. 318 (5857), 1748-1750 (2007).</li><li>Preu&#223;ler, S., Jamshidi, K., Wiatrek, A., Henker, R., Bunge, C. A., Schneider, T. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Quasi-Light-Storage+based+on+time-frequency+coherence.">Quasi-Light-Storage based on time-frequency coherence.</a> Opt. Express. 17 (18), 15790-15798 (2009).</li><li>Jamshidi, K., Preu&#223;ler, S., Wiatrek, A., Schneider, T. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=A+review+to+the+all+optical+Quasi+Light+Storage.">A review to the all optical Quasi Light Storage.</a> IEEE J. Sel. Top. Quantum Electron. Special Issue: Nonlinear Optical Signal Processing. 18 (2), 884-890 (2012).</li><li>Preu&#223;ler, S., Jamshidi, K., Schneider, T. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Quasi-Light-Storage+Enhancement+by+Reducing+the+Brillouin+Gain+Bandwidth.">Quasi-Light-Storage Enhancement by Reducing the Brillouin Gain Bandwidth.</a> Appl. Opt. 50 (22), 4252-4256 (2011).</li><li>Schneider, T., Jamshidi, K., Preu&#223;ler, S. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Quasi-Light+Storage:+A+Method+for+the+Tunable+Storage+of+Optical+Packets+With+a+Potential+Delay-Bandwidth+Product+of+Several+Thousand.">Quasi-Light Storage: A Method for the Tunable Storage of Optical Packets With a Potential Delay-Bandwidth Product of Several Thousand.</a> Bits, J. 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The most critical step during the experiment is the adjustment of the frequency comb, i.e. the bandwidth, flatness and position in respect to the data signal in the frequency domain. According to the sampling theorem in frequency domain, signal distortions are avoided if the whole bandwidth of the optical packet is sampled with an ideally flat comb. Thus, the bandwidth of the optical packet defines the minimum bandwidth of the frequency comb and in this bandwidth the comb has to be as flat as possible. A nonidea...

The data transport in the telecommunications networks is optically, since only optical fibers offer the capacity required for today's data traffic transmitted around the world. However, in every node of the network the optical signal has to be transferred into the electrical domain in order to process it. After processing the signal is converted back to the optical domain for further transmission. This double-transfer between the domains is both time and power consuming. In order to use an all-optical processing of the data, the problem of the intermediate storage has to be solved. Thus, lots of methods for the storage or buffering of the optical signals have been suggested. The simplest way is to send the signals into a matrix of waveguides with different lengths2. However, these matrices are bulky and the storage time cannot be tuned since it is predefined by the waveguide length.
The "Slow-Light" method relies on a tunable change of the group refractive index of a medium to slow down the propagation speed of optical signal pulses2. Several physical effects and material systems can be used for this purpose3-6. However, with these methods the signal can be slowed down by just a few bit-lengths, which is by far not sufficient for optical network nodes7,8.
Another approach uses wavelength conversion and dispersion for the generation of tunable delays. Thereby, the center wavelength of the input signal is shifted via nonlinear optical conversion. Afterwards, the signal is fed into a highly dispersive fiber. The difference in the group velocity in the dispersive fiber leads to a delay that is proportional to the product of the wavelength shift and the group-velocity dispersion (GVD) in the fiber. With a second conversion the wavelength is shifted back to the original value. For the wavelength shift techniques like four-wave mixing or self phase modulation can be used. With the conversion and dispersion method storage times up to 243 nsec of tunable delay, which correspond to 2,400 bit, were reported10. However, wavelength conversion and dispersion methods in general need special components and setups for producing a large wavelength shift and/or large GVD. Additionally, they are among the most complex and power-hungry delay methods2.
Other methods store the optical signal into an excitation of a material system. A probe beam is then used to read out the information. Usually these systems cannot be used in the area of telecommunications since they require ultrahigh or -low temperatures11, will not work with telecommunications bandwidths, or require rather complicated setups and high power12-14.
Here we show how a basic property of signals (the time-frequency coherence) can be exploited for the storage of optical data packets. Since no excitation of a material system is used, we have called the method Quasi-light Storage (QLS)15-17. The QLS is independent of the modulation, data format and data rate of the packets and can store optical packets for several thousand bit lengths18.
The basic idea can be seen in Figure 1, here rectangular shaped pulses are shown. However, the method works for every pulse shape and for packets of pulses. The only restriction is that the signals have to be time-limited.
<img alt="Figure 1" fo:content-width="5in" fo:src="/files/ftp_upload/50468/50468fig1highres.jpg" src="/files/ftp_upload/50468/50468fig1.jpg" /> 
Figure 1. Time-frequency coherence for an intensity modulated signal23. A single rectangular signal in the time domain (a) is represented by a sinc-function in the frequency-domain (b). Here the normalized intensity is shown, since it is not possible to measure the fields with optical equipment. The time domain representation for a sequence of rectangular signals is shown in (c). This sequence has still the same spectral shape. But, it consists of equidistant single frequencies under the sinc-envelope (d). The time axis are normalized to half the duration of a single signal and the frequency axis to the first zero crossings, respectively. <a href="https://www.jove.com/files/ftp_upload/50468/50468fig1highres.jpg" target="_blank">Click here to view larger image.</a>
A rectangular pulse in the time domain (Figure 1a) has a "sinus cardinalis" or sinc function sin(px) / px shaped spectrum (Figure 1b), where all frequencies under the envelope are present. A train of rectangular pulses in the time domain (Figure 1c) has still a sinc function shaped spectrum (Figure 1d) with the bandwidth &#916;f. But due to the periodicity, not all frequencies are present anymore. Instead, the spectrum consists of equidistant frequencies and the inverse of the frequency spacing defines the time separation between the pulses &#916;T = 1/&#916;v.
The basic idea of the QLS is now simply to extract equidistant frequencies out of the spectrum of the input packet. Due to time-frequency coherence this results in a copying of the packet in the time domain. The copy with the desired delay can be extracted by a time domain switch.
The principle of our experiment is shown in Figure 2. A time-limited input signal is multiplied with a frequency comb in the frequency-domain. For the multiplication the nonlinear effect of stimulated Brillouin scattering (SBS) is used. The results are equidistant copies of the input signal in the time-domain. One of the signals is extracted with a switch driven by a rectangular function. Thus, at the output of the memory in principle a distortion-free copy of the input pulse can be expected.
<img alt="Figure 2" fo:content-width="5in" fo:src="/files/ftp_upload/50468/50468fig2highres.jpg" src="/files/ftp_upload/50468/50468fig2.jpg" /> 
Figure 2. Basic idea of the Quasi-light Storage15. A time limited input signal (a) is multiplied with a frequency comb (b) in the frequency-domain, which is denoted with a X. This leads to various copies of the signal in the time domain (c). From the generated pulse train one of the copies (d) is extracted with a time-domain switch by a rectangular read signal (e). The switch can be a modulator. The result is a storage of the optical signal. The storage time is defined by the frequency spacing between the comb lines and the read signal. <a href="https://www.jove.com/files/ftp_upload/50468/50468fig2highres.jpg" target="_blank">Click here to view larger image.</a>
SBS itself is a nonlinear effect that can occur in standard single mode fibers (SSMF) at low powers. Thereby, the signal interacts with an optical density change which is generated by a counter propagating pump wave. If the signal wave is downshifted in frequency, a gain region is formed in which the signal will be amplified. If it is up-shifted the signal will be attenuated in the corresponding loss region. The frequency shift between pump and signal is defined by the acoustic wave, which depends on the material properties. The biggest advantage of SBS for the presented application is the narrow bandwidth &#916;fSBS of the gain region. Thus, practically SBS forms a narrow linewidth optical filter. The narrow bandwidth of the gain region depends on the effective length and area of the fiber as well as on the used pump power19. The natural full-width at half-maximum (FWHM) bandwidth of the SBS gain in a SSMF is around 30 MHz. In special waveguides, such as AllWave fibers, and with high pump powers, the bandwidth can be reduced down to 10 MHz20. Due to the filter bandwidth the different copies are covered with an envelope. Therefore, the maximum storage time of the QLS inversely depends on the SBS bandwidth. A bandwidth of 10 MHz would result in a maximum storage time of 100 nsec. <a href="https://www.jove.com/files/ftp_upload/50468/50468fig3highres.jpg" target="_blank">Click here to view larger image.</a>
For very high bit-rate transmission the information has to be encoded into the phase of the carrier instead of its amplitude, since this offers a lot of advantages. Thus, contrary to pulses, the signals in these optical networks have constant amplitude. Figure 3 shows such a phase modulated signal in the time (left) and frequency domain (right). This spectrum can be sampled in the same way as that of the amplitude modulated signal21. In fact the spectrum of the rectangular function for intensity- and phase-modulated signals is filtered due to the transmission, which limits the spectrum.
<img alt="Figure 3" fo:content-width="5in" fo:src="/files/ftp_upload/50468/50468fig3highres.jpg" src="/files/ftp_upload/50468/50468fig3.jpg" /> 
Figure 3. Time-frequency coherence for a phase modulation21. In a phase modulated signal the phase of the carrier is changed by the signal which has to be transmitted. If each symbol consists of 1 bit, the phase is changed between 0 and &#960;, for instance. The left side of the figure shows the resulting time-domain representation for such a binary phase shift keyed (BPSK) signal. The resulting frequency-domain signal is shown on the right side. By comparison with Figure 1 it can be seen that the spectrum of the phase modulated signal is qualitatively the same as that of the intensity modulated signal. Thus, the QLS can be applied in the same way.

<table border="0" cellpadding="0" cellspacing="0" width="603">
	<tbody>
		<tr height="22">
			<td height="22" style="height:22px;width:111px;">Laser diode</td>
			<td style="width:147px;">3S Photonics</td>
			<td style="width:185px;">A1905LMI</td>
			<td style="width:160px;">2x</td>
		</tr>
		<tr height="22">
			<td height="22" style="height:22px;width:111px;">Laser Mount</td>
			<td style="width:147px;">Tektronix</td>
			<td style="width:185px;">LDH BFY-B2</td>
			<td style="width:160px;">2x</td>
		</tr>
		<tr height="43">
			<td height="43" style="height:43px;width:111px;">Temperature Controller</td>
			<td style="width:147px;">LightWave</td>
			<td style="width:185px;">LDT-5948</td>
			<td style="width:160px;">2x</td>
		</tr>
		<tr height="43">
			<td height="43" style="height:43px;width:111px;">Current Controller</td>
			<td style="width:147px;">LightWave</td>
			<td style="width:185px;">LDX-3220</td>
			<td style="width:160px;">2x</td>
		</tr>
		<tr height="43">
			<td height="43" style="height:43px;width:111px;">Optical amplifier</td>
			<td style="width:147px;">High-Wave</td>
			<td style="width:185px;">HWT-EDFA-B-30-1-FC/PC</td>
			<td style="width:160px;"></td>
		</tr>
		<tr height="22">
			<td height="22" style="height:22px;width:111px;">Circulator</td>
			<td style="width:147px;">OFR</td>
			<td style="width:185px;">OCT-3-IR2</td>
			<td style="width:160px;"></td>
		</tr>
		<tr height="43">
			<td height="43" style="height:43px;width:111px;">Waveform Generator</td>
			<td style="width:147px;">Tektronix</td>
			<td style="width:185px;">AWG7102</td>
			<td style="width:160px;"></td>
		</tr>
		<tr height="22">
			<td height="22" style="height:22px;width:111px;">Fiber 20km</td>
			<td style="width:147px;">OFS</td>
			<td style="width:185px;">AllWave-ZWP G652C-D</td>
			<td style="width:160px;"></td>
		</tr>
		<tr height="43">
			<td height="43" style="height:43px;width:111px;">Polarization Controller</td>
			<td style="width:147px;">Thorlabs</td>
			<td style="width:185px;">Fiber Pol. Contr. IPC030</td>
			<td style="width:160px;">2x</td>
		</tr>
		<tr height="22">
			<td height="22" style="height:22px;width:111px;">Modulator</td>
			<td style="width:147px;">Avanex</td>
			<td style="width:185px;">IM-10-P</td>
			<td style="width:160px;">Phase</td>
		</tr>
		<tr height="22">
			<td height="22" style="height:22px;width:111px;">Modulator</td>
			<td style="width:147px;">Avanex</td>
			<td style="width:185px;">SD20</td>
			<td style="width:160px;">Amplitude, extract</td>
		</tr>
		<tr height="22">
			<td height="22" style="height:22px;width:111px;">Modulator</td>
			<td style="width:147px;">Avanex</td>
			<td style="width:185px;">PowerBit F-10</td>
			<td style="width:160px;">Amplitude, data</td>
		</tr>
		<tr height="22">
			<td height="22" style="height:22px;width:111px;">Modulator</td>
			<td style="width:147px;">Covega</td>
			<td style="width:185px;">Mach10</td>
			<td style="width:160px;">Amplitude, comb</td>
		</tr>
		<tr height="64">
			<td height="64" style="height:64px;width:111px;">Optical Spectrum Analyzer</td>
			<td style="width:147px;">Yokogawa</td>
			<td style="width:185px;">AQ6370C</td>
			<td style="width:160px;"></td>
		</tr>
		<tr height="22">
			<td height="22" style="height:22px;width:111px;">Oscilloscope</td>
			<td style="width:147px;">Agilent</td>
			<td style="width:185px;">DCA-J 86100C</td>
			<td style="width:160px;"></td>
		</tr>
		<tr height="43">
			<td height="43" style="height:43px;width:111px;">Measurement Modul</td>
			<td style="width:147px;">Agilent</td>
			<td style="width:185px;">86106B</td>
			<td style="width:160px;"></td>
		</tr>
		<tr height="22">
			<td height="22" style="height:22px;width:111px;">Fiber Laser</td>
			<td style="width:147px;">Koheras</td>
			<td style="width:185px;">Adjustik</td>
			<td style="width:160px;"></td>
		</tr>
		<tr height="22">
			<td height="22" style="height:22px;width:111px;">Coupler</td>
			<td style="width:147px;">Newport</td>
			<td style="width:185px;">F-CPL-L22151-P</td>
			<td style="width:160px;">Ratio: 90/10</td>
		</tr>
		<tr height="22">
			<td height="22" style="height:22px;width:111px;">Coupler</td>
			<td style="width:147px;">Newport</td>
			<td style="width:185px;">F-CPL-L12155-P</td>
			<td style="width:160px;">Ratio: 50/50</td>
		</tr>
		<tr height="22">
			<td height="22" style="height:22px;width:111px;">Power supply</td>
			<td style="width:147px;">Zentro-elektrik</td>
			<td style="width:185px;">LD 2x15/1 GB</td>
			<td style="width:160px;"></td>
		</tr>
		<tr height="43">
			<td height="43" style="height:43px;width:111px;">Electrical amplifier</td>
			<td style="width:147px;">SHF</td>
			<td style="width:185px;">826H</td>
			<td style="width:160px;"></td>
		</tr>
		<tr height="22">
			<td height="22" style="height:22px;width:111px;">Supply port</td>
			<td style="width:147px;">SHF</td>
			<td style="width:185px;">B826</td>
			<td style="width:160px;"></td>
		</tr>
		<tr height="43">
			<td height="43" style="height:43px;width:111px;">Electrical amplifier</td>
			<td style="width:147px;">Amplifier Research</td>
			<td style="width:185px;">10W1000</td>
			<td style="width:160px;"></td>
		</tr>
		<tr height="22">
			<td height="22" style="height:22px;width:111px;">Photo diode</td>
			<td style="width:147px;">Newport</td>
			<td style="width:185px;">D-8ir</td>
			<td style="width:160px;"></td>
		</tr>
		<tr height="64">
			<td height="64" style="height:64px;width:111px;">Electrical spectrum analyzer</td>
			<td style="width:147px;">HP</td>
			<td style="width:185px;">8563E</td>
			<td style="width:160px;"></td>
		</tr>
	</tbody>
</table>

quasi-light storage for optical data packets

Today's telecommunication is based on optical packets which transmit the information in optical fiber networks around the world. Currently, the processing of the signals is done in the electrical domain. Direct storage in the optical domain would avoid the transfer of the packets to the electrical and back to the optical domain in every network node and, therefore, increase the speed and possibly reduce the energy consumption of telecommunications. However, light consists of photons which propagate with the speed of light in vacuum. Thus, the storage of light is a big challenge. There exist some methods to slow down the speed of the light, or to store it in excitations of a medium. However, these methods cannot be used for the storage of optical data packets used in telecommunications networks. Here we show how the time-frequency-coherence, which holds for every signal and therefore for optical packets as well, can be exploited to build an optical memory. We will review the background and show in detail and through examples, how a frequency comb can be used for the copying of an optical packet which enters the memory. One of these time domain copies is then extracted from the memory by a time domain switch. We will show this method for intensity as well as for phase modulated signals.

For the measurement a 10110101 intensity modulated data pattern with a data rate of 1 Gbps was used. The black line in Figure&#160;6 represents the original signal and the colored lines represent the different storage times achieved with the QLS.&#160; The reference is measured without the QLS and the deactivated switch at the output. Under ideal conditions storage times up to 100&#8239;nsec are achievable. The results for the stored 11001101 data pattern of a phase modulated signal, again with a data ra...

Watch this Scientific Journal Video about Quasi-light Storage for Optical Data Packets at JoVE.com

Quasi-light Storage for Optical Data Packets

The article describes a procedure to store optical data packets with an arbitrary modulation, wavelength, and data rate. These packets are the basis of modern telecommunications.

Today's telecommunication is based on optical packets which transmit the information in optical fiber networks around the world. Currently, the processing ...

quasi-light-storage-for-optical-data-packets

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10.6K vues.  Hochschule für Telekommunikation, Leipzig.  L'article décrit une procédure pour stocker les paquets de données optiques avec une modulation arbitraire, longueur d'onde, et le taux de données. Ces paquets sont à la base des télécommunications modernes. 

Vidéo: Quasi-light Storage for Optical Data Packets

The article describes a procedure to store optical data packets with an arbitrary modulation, wavelength, and data rate. These packets are the basis of modern...

graphene-assisted quasi-van der waals epitaxy of aln film on nano-patterned sapphire substrate for ultraviolet light emitting diodes

Graphene-Assisted Quasi-van der Waals Epitaxy of AlN Film on Nano-Patterned Sapphire Substrate for Ultraviolet Light Emitting Diodes

A protocol for graphene-assisted growth of high-quality AlN films on nano-patterned sapphire substrate is...

measuring light-switching behavior using an occupancy and light data logger

Measuring Light-Switching Behavior Using an Occupancy and Light Data Logger

This article describes a procedure for using and deploying an occupancy and light data logger which allows collecting data about light-switching behavior of participants in field...

fabrication and characterization of disordered polymer optical fibers for transverse anderson localization of light

Fabrication and Characterization of Disordered Polymer Optical Fibers for Transverse Anderson Localization of Light

We develop and characterize a disordered polymer optical fiber that uses transverse Anderson localization as a novel waveguiding mechanism. This microstructured fiber can transport a small localized beam with a radius that is comparable to the beam radius of conventional optical...

quantum state engineering of light with continuous-wave optical parametric oscillators

Quantum State Engineering of Light with Continuous-wave Optical Parametric Oscillators

We describe the reliable generation of non-Gaussian states of traveling optical fields, including single-photon states and coherent state superpositions, using a conditional preparation method operated on the non-classical light emitted by optical parametric oscillators. Type-I and type-II phase-matched oscillators are considered and common procedures, such as the required frequency filtering or the high-efficiency quantum state characterization by homodyning, are...

optical clearing and labeling for light-sheet fluorescence microscopy in large-scale human brain imaging

Author Spotlight: Advancing 3D Cytoarchitecture Analysis - Rapid Volumetric Reconstruction of the Human Brain 

The present protocol provides a step-by-step procedure for rapid and simultaneous optical clearing, muti-round labeling, and 3D volumetric reconstruction of tens of postmortem human brain sections by combining the (SWITCH - H2O2 - Antigen Retrieval - 2,2'-thiodiethanol [TDE]) SHORT tissue transformation technique with light-sheet fluorescence microscopy imaging in a routinely high-throughput...

Optical Clearing and Labeling for Light-sheet Fluorescence Microscopy in Large-scale Human Brain Imaging

high-throughput analysis of optical mapping data using electromap

High-Throughput Analysis of Optical Mapping Data Using ElectroMap

This protocol describes the setup and use of ElectroMap, a MATLAB-based open-source software platform for analysis of cardiac optical mapping data. ElectroMap provides a versatile high-throughput tool for analysis of optical mapping voltage and calcium datasets across a wide range of cardiac experimental...

fixed target serial data collection at diamond light source

Fixed Target Serial Data Collection at Diamond Light Source

We present a comprehensive guide to fixed target sample preparation, data collection, and data processing for serial synchrotron crystallography at Diamond beamline I24.

quasi-metagenomic analysis of salmonella from food and environmental samples

Quasi-metagenomic Analysis of Salmonella from Food and Environmental Samples

Here, we present a protocol to prepare DNA samples from food and environmental microbiomes for concerted detection and subtyping of Salmonella through quasimetagenomic sequencing. The combined use of culture enrichment, immunomagnetic separation (IMS), and multiple displacement amplification (MDA) allows effective concentration of Salmonella genomic DNA from food and environmental...

Quasi-metagenomic Analysis of Salmonella from Food and Environmental Samples

in vivo visible light optical coherence tomography (oct) mouse retinal imaging

In Vivo Visible Light Optical Coherence Tomography (OCT) Mouse Retinal Imaging  

high resolution phonon-assisted quasi-resonance fluorescence spectroscopy

High Resolution Phonon-assisted Quasi-resonance Fluorescence Spectroscopy

The manuscript describes a method of phonon-assisted quasi-resonant fluorescence spectroscopy that incorporates both laser-limited resolution and photoluminescence (PL) spectroscopy. This method utilizes optical phonons to provide linewidth-limited resolution spectra of atom-like semiconductor structures in the energy domain. The method is also easily realized with a single spectrometer optical spectroscopy setup.

micron-scale resolution optical tomography of entire mouse brains with confocal light sheet microscopy

Micron-scale Resolution Optical Tomography of Entire Mouse Brains with Confocal Light Sheet Microscopy

In this article we describe the full experimental procedure to reconstruct, with high resolution, the fine brain anatomy of fluorescently labeled mouse brains. The described protocol includes sample preparation and clearing, specimen mounting for imaging, data post-processing and multi-scale...

collection, processing, and storage consideration for urinary biomarker research

Collection, Processing, and Storage Consideration for Urinary Biomarker Research

This protocol aims to provide considerations for urine sample collection, processing, and storage for urine tract infection biomarker...

an introduction to processing, fitting, and interpreting transient absorption data

Author Spotlight: Exploring Light-Driven Chemical Reactions and Energy-Harnessing Devices in Photochemical Research

This protocol is a beginner's entryway into processing, fitting, and interpreting transient absorption spectra. The focus of this protocol is the preparation of datasets, and fitting using both single wavelength kinetics and global lifetime analysis. Challenges associated with transient absorption data and its fitting are discussed.

Decoding Transient Absorption - Processing, Fitting, and Interpreting Data

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alignment of visible-light optical coherence tomography fibergrams with confocal images of the same mouse retina

Author Spotlight: Advancements in In Vivo and Ex Vivo Retinal Imaging for Improved Glaucoma Diagnosis and Treatment 

The present protocol outlines the steps for aligning in vivo visible-light optical coherence tomography fibergraphy (vis-OCTF) images with ex vivo confocal images of the same mouse retina for the purpose of verifying the observed retinal ganglion cell axon bundle morphology in the in vivo images.

Alignment of Visible-Light Optical Coherence Tomography Fibergrams with Confocal Images of the Same Mouse Retina

finite element modeling for the simulation of the quasi-static compression of corrugated tapered tubes

Finite Element Modeling for the Simulation of the Quasi-Static Compression of Corrugated Tapered Tubes

This protocol describes the study of the quasi-static compression performance of corrugated tapered tubes using finite element simulations. The influence of the thickness gradient on the compression performance was investigated. The results show that proper thickness gradient design can change the deformation mode and significantly improve the energy absorption performance of the...

digitizing the core surfaces for analysis and storage of cores

Digitizing the Core Surfaces for Analysis and Storage of Cores

fixation of ovarian cancer organoids for long-term storage

Fixation of Ovarian Cancer Organoids for Long-Term Storage

in situ x-ray crystallographic data collection using the beamline at diamond light source

In Situ X-ray Crystallographic Data Collection Using the Beamline at Diamond Light Source  

low-cost cryo-light microscopy stage fabrication for correlated light/electron microscopy

Low-Cost Cryo-Light Microscopy Stage Fabrication for Correlated Light/Electron Microscopy

We demonstrate the fabrication of a low-cost cryogenic stage designed to fit most reflected light microscopes. This lab-built cryogenic stage enables efficient and reliable correlative imaging between cryo-light and cryo-electron...

Construction and Testing of Coin Cells of Lithium Ion Batteries

Rechargeable lithium ion batteries have wide applications in electronics, where customers always demand more capacity and longer lifetime. Lithium ion batteries have also been considered to be used in electric and hybrid vehicles1 or even electrical grid stabilization systems2. All these applications simulate a dramatic increase in the research and development of battery materials3-7, including new materials3,8, doping9, nanostructuring10-13, coatings or surface modifications14-17 and novel binders18. Consequently, an increasing number of physicists, chemists and materials scientists have recently ventured into this area. Coin cells are widely used in research laboratories to test new battery materials; even for the research and development that target large-scale and high-power applications, small coin cells are often used to test the capacities and rate capabilities of new materials in the initial stage. 
 In 2010, we started a National Science Foundation (NSF) sponsored research project to investigate the surface adsorption and disordering in battery materials (grant no. DMR-1006515). In the initial stage of this project, we have struggled to learn the techniques of assembling and testing coin cells, which cannot be achieved without numerous help of other researchers in other universities (through frequent calls, email exchanges and two site visits). Thus, we feel that it is beneficial to document, by both text and video, a protocol of assembling and testing a coin cell, which will help other new researchers in this field. This effort represents the "Broader Impact" activities of our NSF project, and it will also help to educate and inspire students.
In this video article, we document a protocol to assemble a CR2032 coin cell with a LiCoO2 working electrode, a Li counter electrode, and (the mostly commonly used) polyvinylidene fluoride (PVDF) binder. To ensure new learners to readily repeat the protocol, we keep the protocol as specific and explicit as we can. However, it is important to note that in specific research and development work, many parameters adopted here can be varied. First, one can make coin cells of different sizes and test the working electrode against a counter electrode other than Li. Second, the amounts of C black and binder added into the working electrodes are often varied to suit the particular purpose of research; for example, large amounts of C black or even inert powder were added to the working electrode to test the "intrinsic" performance of cathode materials14. Third, better binders (other than PVDF) have also developed and used18. Finally, other types of electrolytes (instead of LiPF6) can also be used; in fact, certain high-voltage electrode materials will require the uses of special electrolytes7.

A protocol to construct and test coin cells of lithium ion batteries is described. The specific procedures of making a working electrode, preparing a counter electrode, assembling a cell inside a glovebox and testing the cell are presented.

Rechargeable lithium ion batteries have wide applications in electronics, where customers always demand more capacity and longer lifetime.  Lithium ion ...

Fabricating Metamaterials Using the Fiber Drawing Method

Metamaterials are man-made composite materials, fabricated by assembling components much smaller than the wavelength at which they operate 1. They owe their electromagnetic properties to the structure of their constituents, instead of the atoms that compose them. For example, sub-wavelength metal wires can be arranged to possess an effective electric permittivity that is either positive or negative at a given frequency, in contrast to the metals themselves 2. This unprecedented control over the behaviour of light can potentially lead to a number of novel devices, such as invisibility cloaks 3, negative refractive index materials 4, and lenses that resolve objects below the diffraction limit 5. However, metamaterials operating at optical, mid-infrared and terahertz frequencies are conventionally made using nano- and micro-fabrication techniques that are expensive and produce samples that are at most a few centimetres in size 6-7. Here we present a fabrication method to produce hundreds of meters of metal wire metamaterials in fiber form, which exhibit a terahertz plasmonic response 8. We combine the stack-and-draw technique used to produce microstructured polymer optical fiber 9 with the Taylor-wire process 10, using indium wires inside polymethylmethacrylate (PMMA) tubes. PMMA is chosen because it is an easy to handle, drawable dielectric with suitable optical properties in the terahertz region; indium because it has a melting temperature of 156.6 &deg;C which is appropriate for codrawing with PMMA. We include an indium wire of 1 mm diameter and 99.99% purity in a PMMA tube with 1 mm inner diameter (ID) and 12 mm outside diameter (OD) which is sealed at one end. The tube is evacuated and drawn down to an outer diameter of 1.2 mm. The resulting fiber is then cut into smaller pieces, and stacked into a larger PMMA tube. This stack is sealed at one end and fed into a furnace while being rapidly drawn, reducing the diameter of the structure by a factor of 10, and increasing the length by a factor of 100. Such fibers possess features on the micro- and nano- scale, are inherently flexible, mass-producible, and can be woven to exhibit electromagnetic properties that are not found in nature. They represent a promising platform for a number of novel devices from terahertz to optical frequencies, such as invisible fibers, woven negative refractive index cloths, and super-resolving lenses.

Metamaterials at terahertz frequencies offer unique opportunities, but are challenging to fabricate in bulk. We adapt the fabrication procedure for microstructured polymer optical fibers to inexpensively fabricate metamaterials potentially on an industrial scale. We produce polymethylmethacrylate fibers containing ~10 &mu;m diameter indium wires separated by ~100 &mu;m, which exhibit a terahertz plasmonic response.

Metamaterials are man-made composite materials, fabricated by assembling components much smaller than the wavelength at which they operate 1. They owe ...

Optical Trapping of Nanoparticles

Optical trapping is a technique for immobilizing and manipulating small objects in a gentle way using light, and it has been widely applied in trapping and manipulating small biological particles. Ashkin and co-workers first demonstrated optical tweezers using a single focused beam1. The single beam trap can be described accurately using the perturbative gradient force formulation in the case of small Rayleigh regime particles1. In the perturbative regime, the optical power required for trapping a particle scales as the inverse fourth power of the particle size. High optical powers can damage dielectric particles and cause heating. For instance, trapped latex spheres of 109 nm in diameter were destroyed by a 15 mW beam in 25 sec1, which has serious implications for biological matter2,3.
A self-induced back-action (SIBA) optical trapping was proposed to trap 50 nm polystyrene spheres in the non-perturbative regime4. In a non-perturbative regime, even a small particle with little permittivity contrast to the background can influence significantly the ambient electromagnetic field and induce a large optical force. As a particle enters an illuminated aperture, light transmission increases dramatically because of dielectric loading. If the particle attempts to leave the aperture, decreased transmission causes a change in momentum outwards from the hole and, by Newton's Third Law, results in a force on the particle inwards into the hole, trapping the particle. The light transmission can be monitored; hence, the trap can become a sensor. The SIBA trapping technique can be further improved by using a double-nanohole structure.
The double-nanohole structure has been shown to give a strong local field enhancement5,6. Between the two sharp tips of the double-nanohole, a small particle can cause a large change in optical transmission, thereby inducing a large optical force. As a result, smaller nanoparticles can be trapped, such as 12 nm silicate spheres7 and 3.4 nm hydrodynamic radius bovine serum albumin proteins8. In this work, the experimental configuration used for nanoparticle trapping is outlined. First, we detail the assembly of the trapping setup which is based on a Thorlabs Optical Tweezer Kit. Next, we explain the nanofabrication procedure of the double-nanohole in a metal film, the fabrication of the microfluidic chamber and the sample preparation. Finally, we detail the data acquisition procedure and provide typical results for trapping 20 nm polystyrene nanospheres.

The following setup approach details low power optical trapping of dielectric nanoparticles using a double-nanohole in metal film.

Optical trapping is a technique for immobilizing and manipulating small objects in a gentle way using light, and it has been widely applied in trapping ...

The Generation of Higher-order Laguerre-Gauss Optical Beams for High-precision Interferometry

Thermal noise in high-reflectivity mirrors is a major impediment for several types of high-precision interferometric experiments that aim to reach the standard quantum limit or to cool mechanical systems to their quantum ground state. This is for example the case of future gravitational wave observatories, whose sensitivity to gravitational wave signals is expected to be limited in the most sensitive frequency band, by atomic vibration of their mirror masses. One promising approach being pursued to overcome this limitation is to employ higher-order Laguerre-Gauss (LG) optical beams in place of the conventionally used fundamental mode. Owing to their more homogeneous light intensity distribution these beams average more effectively over the thermally driven fluctuations of the mirror surface, which in turn reduces the uncertainty in the mirror position sensed by the laser light.
We demonstrate a promising method to generate higher-order LG beams by shaping a fundamental Gaussian beam with the help of diffractive optical elements. We show that with conventional sensing and control techniques that are known for stabilizing fundamental laser beams, higher-order LG modes can be purified and stabilized just as well at a comparably high level. A set of diagnostic tools allows us to control and tailor the properties of generated LG beams. This enabled us to produce an LG beam with the highest purity reported to date. The demonstrated compatibility of higher-order LG modes with standard interferometry techniques and with the use of standard spherical optics makes them an ideal candidate for application in a future generation of high-precision interferometry.

Large laser-interferometers are being constructed to create a new type of astronomy based on gravitational waves. Their sensitivities, as for many other high-precision experiments, are approaching fundamental noise limits such as the atomic vibration of their components. We are pioneering technologies to overcome these limits using novel laser beam shapes.

Thermal noise in high-reflectivity mirrors is a major impediment for several  types of high-precision interferometric experiments that aim to reach the  ...

Convergent Polishing: A Simple, Rapid, Full Aperture Polishing Process of High Quality Optical Flats &amp; Spheres

Convergent Polishing is a novel polishing system and method for finishing flat and spherical glass optics in which a workpiece, independent of its initial shape (i.e., surface figure), will converge to final surface figure with excellent surface quality under a fixed, unchanging set of polishing parameters in a single polishing iteration. In contrast, conventional full aperture polishing methods require multiple, often long, iterative cycles involving polishing, metrology and process changes to achieve the desired surface figure. The Convergent Polishing process is based on the concept of workpiece-lap height mismatch resulting in pressure differential that decreases with removal and results in the workpiece converging to the shape of the lap. The successful implementation of the Convergent Polishing process is a result of the combination of a number of technologies to remove all sources of non-uniform spatial material removal (except for workpiece-lap mismatch) for surface figure convergence and to reduce the number of rogue particles in the system for low scratch densities and low roughness. The Convergent Polishing process has been demonstrated for the fabrication of both flats and spheres of various shapes, sizes, and aspect ratios on various glass materials. The practical impact is that high quality optical components can be fabricated more rapidly, more repeatedly, with less metrology, and with less labor, resulting in lower unit costs. In this study, the Convergent Polishing protocol is specifically described for fabricating 26.5 cm square fused silica flats from a fine ground surface to a polished ~&#955;/2 surface figure after polishing 4 hr per surface on a 81 cm diameter polisher.

A novel optical polishing process, called &#8220;Convergent Polishing&#8221;, which enables faster, lower cost polishing, is described. Unlike conventional polishing processes, Convergent Polishing allows a glass workpiece to be polished in a single iteration and with high surface quality to its final surface figure without requiring changes to polishing parameters.

Convergent Polishing is a novel polishing system and method for finishing flat and spherical glass optics in which a workpiece, independent of its initial ...

Writing Bragg Gratings in Multicore Fibers

Fiber Bragg gratings in multicore fibers can be used as compact and robust filters in astronomical and other research and commercial applications. Strong suppression at a single wavelength requires that all cores have matching transmission profiles. These gratings cannot be inscribed using the same method as for single-core fibers because the curved surface of the cladding acts as a lens, focusing the incoming UV laser beam and causing variations in exposure between cores. Therefore we use an additional optical element to ensure that the beam shape does not change while passing through the cross-section of the multicore fiber. This consists of a glass capillary tube which has been polished flat on one side, which is then placed over the section of the fiber to be inscribed. The laser beam enters the fiber through the flat surface of the capillary tube and hence maintains its original dimensions. This paper demonstrates the improvements in core-to-core uniformity for a 7-core fiber using this method. The technique can be generalized to larger multicore fibers.

We describe a technique for inscribing identical fiber Bragg gratings into each core of a multicore fiber. This is achieved by introducing an additional surface into the optical path to mitigate lensing by the curved surface of the fiber cladding.

Fiber Bragg gratings in multicore fibers can be used as compact and robust filters in astronomical and other research and commercial applications. Strong ...

Compact Lens-less Digital Holographic Microscope for MEMS Inspection and Characterization

A micro-electro-mechanical-system (MEMS) is a widely used component in many industries, including energy, biotechnology, medical, communications, and automotive. However, effective inspection and characterization metrology systems are needed to ensure the functional reliability of MEMS. This study presents a system based on digital holography as a tool for MEMS metrology. Digital holography has gained increasing attention in the past 20 years. With the fast development and decreasing cost of sensor arrays, resolution of such systems has increased broadening potential applications. Thus, it has attracted attention from both research and industry sides as a potential reliable tool for industrial metrology. Indeed, by recording the interference pattern between an object beam (which contains sample height information) and a reference beam on a CCD camera, one can retrieve the quantitative phase information of an object. However, most of digital holographic systems are bulky and thus not easy to implement on industry production lines. The novelty of the system presented is that it is lens-less and thus very compact. In this study, it is shown that the Compact Digital Holographic Microscope (CDHM) can be used to evaluate several characteristics typically consider as criteria in MEMS inspections. The surface profiles of MEMS in both static and dynamic conditions are presented. Comparison with AFM is investigated to validate the accuracy of the CDHM.

We present a compact reflection digital holographic system (CDHM) for inspection and characterization of MEMS devices. A lens-less design using a diverging input wave providing natural geometrical magnification is demonstrated. Both static and dynamic studies are presented.

A micro-electro-mechanical-system (MEMS) is a widely used component in many industries, including energy, biotechnology, medical, communications, and ...

Data Acquisition Protocol for Determining Embedded Sensitivity Functions

The effectiveness of many structural health monitoring techniques depends on the placement of sensors and the location of input forces. Algorithms for determining optimal sensor and forcing locations typically require data, either simulated or measured, from the damaged structure. Embedded sensitivity functions provide an approach for determining the best available sensor location to detect damage with only data from the healthy structure. In this video and manuscript, the data acquisition procedure and best practices for determining the embedded sensitivity functions of a structure is presented. The frequency response functions used in the calculation of the embedded sensitivity functions are acquired using modal impact testing. Data is acquired and representative results are shown for a residential scale wind turbine blade. Strategies for evaluating the quality of the data being acquired are provided during the demonstration of the data acquisition process.

The data acquisition procedure for determining embedded sensitivity functions is described. Data is acquired and representative results are shown for a residential scale wind turbine blade.

The effectiveness of many structural health monitoring techniques depends on the placement of sensors and the location of input forces. Algorithms for ...

Two-way Valorization of Blast Furnace Slag: Synthesis of Precipitated Calcium Carbonate and Zeolitic Heavy Metal Adsorbent

The aim of this work is to present a zero-waste process for storing CO2 in a stable and benign mineral form while producing zeolitic minerals with sufficient heavy metal adsorption capacity. To this end, blast furnace slag, a residue from iron-making, is utilized as the starting material. Calcium is selectively extracted from the slag by leaching with acetic acid (2 M CH3COOH) as the extraction agent. The filtered leachate is subsequently physico-chemically purified and then carbonated to form precipitated calcium carbonate (PCC) of high purity (&lt;2 wt% non-calcium impurities, according to ICP-MS analysis). Sodium hydroxide is added to neutralize the regenerated acetate. The morphological properties of the resulting calcitic PCC are tuned for its potential application as a filler in papermaking. In parallel, the residual solids from the extraction stage are subjected to hydrothermal conversion in a caustic solution (2 M NaOH) that leads to the predominant formation of a particular zeolitic mineral phase (detected by XRD), namely analcime (NaAlSi2O6&#8729;H2O). Based on its ability to adsorb Ni2+, as reported from batch adsorption experiments and ICP-OES analysis, this product can potentially be used in wastewater treatment or for environmental remediation applications.

A protocol for the parallel production of precipitated calcium carbonate and zeolitic material from blast furnace slag via mineral carbonation and alkaline hydrothermal conversion, respectively, is presented. The performance of the zeolitic material towards nickel adsorption is tested.

The aim of this work is to present a zero-waste process for storing CO2 in a stable and benign mineral form while producing zeolitic minerals with ...

Scanning Light Scattering Profiler (SLPS) Based Methodology to Quantitatively Evaluate Forward and Backward Light Scattering from Intraocular Lenses

The scanning light scattering profiler (SLSP) methodology has been developed for the full-angle quantitative evaluation of forward and backward light scattering from intraocular lenses (IOLs) using goniophotometer principles. This protocol describes the SLSP platform and how it employs a 360&#176; rotational photodetector sensor that is scanned around an IOL sample while recording the intensity and location of scattered light as it passes through the IOL medium. The SLSP platform can be used to predict, non-clinically, the propensity for current and novel IOL designs and materials to induce light scatter. Non-clinical evaluation of light scattering properties of IOLs can significantly reduce the number of patient complaints related to unwanted glare, glistening, optical defects, poor image quality, and other phenomena associated with the unintended light scattering. Future studies should be conducted to correlate SLSP data with clinical results to help identify which measured light scatter is most problematic for patients that have undergone cataract surgery subsequent to IOL implantation.

Scanning Light Scattering Profiler SLPS Based Methodology to Quantitatively Evaluate Forward and Backward Light Scattering from Intraocular Lenses

This protocol describes the scanning light scattering profiler (SLSP) that enables the full-angle quantitative evaluation of forward and backward scattering of light from intraocular lenses (IOLs) using goniophotometer principles.

The scanning light scattering profiler (SLSP) methodology has been developed for the full-angle quantitative evaluation of forward and backward light ...