The cryo-SEM and FIB method can be used to study solid-liquid interfaces and biological samples while preserving the samples native structure. The main advantage of this technique is that the cryo-SEM allows the user to quickly probe the interface
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Cryogenic Focused Ion Beam (FIB) and Scanning Electron Microscopy (SEM) techniques can provide key insights into the chemistry and morphology of intact solid-liquid interfaces. Methods for preparing high quality Energy Dispersive X-ray (EDX) spectroscopic maps of such interfaces are detailed, with a focus on energy storage devices.