Performing In Situ Closed-Cell Gas Reactions in the Transmission Electron MicroscopeKinga A. Unocic 1, Dale K. Hensley 1, Franklin S. Walden 2, Wilbur C. Bigelow 3, Michael B. Griffin 4, Susan E. Habas 4, Raymond R. Unocic 1, Lawrence F. Allard 5
1Center for Nanophase Materials Sciences, Oak Ridge National Laboratory, 2Protochips Inc., 3Department of Materials Science & Engineering, University of Michigan, 4Catalytic Carbon Transformation & Scale-up, National Renewable Energy Laboratory, 5Materials Science & Technology Division, Oak Ridge National Laboratory
Here, we present a protocol for performing in situ TEM closed-cell gas reaction experiments while detailing several commonly used sample preparation methods.
