How to Build a Vacuum Spring-transport Package for Spinning Rotor Gauges

Podsumowanie

Here we describe how to build a robust spring-transport mechanism for a spinning rotor gauge. This device securely immobilizes the rotor and keeps it under vacuum during transportation. We also describe packaging that minimizes the risk of damage during transport. Tests show our design works for typical shocks during transport.

Streszczenie

The spinning rotor gauge (SRG) is a high-vacuum gauge often used as a secondary or transfer standard for vacuum pressures in the range of 1.0 x 10^-4 Pa to 1.0 Pa. In this application, the SRGs are frequently transported to laboratories for calibration. Events can occur during transportation that change the rotor surface conditions, thus changing the calibration factor. To assure calibration stability, a spring-transport mechanism is often used to immobilize the rotor and keep it under vacuum during transport. It is also important to transport the spring-transport mechanism using packaging designed to minimize the risk of damage during shipping. In this manuscript, a detailed description is given on how to build a robust spring-transport mechanism and shipping container. Together these form a spring-transport package. The spring-transport package design was tested using drop-tests and the performance was found to be excellent. The present spring-transport mechanism design keeps the rotor immobilized when experiencing shocks of several hundred g (g = 9.8 m/sec² and is the acceleration due to gravity), while the shipping container assures that the mechanism will not experience shocks greater than about 100 g during common shipping mishaps (as defined by industry standards).

Wprowadzenie

The spinning rotor gauge (SRG) is a high-vacuum gauge used to determine vacuum pressures in the range of 1.0 x 10^-4 Pa to 1.0 Pa. It is fundamentally a rotating steel ball that is suspended between two permanent magnets. Electro-magnets are used to rotate, or "spin-up", the ball to some frequency (typically 410 Hz); the ball is then allowed to freely rotate, but the rotation rate will decrease over time because of collisions of gas molecules in the vacuum system with the ball surface. Vacuum pressure is thus related to the deceleration rate of the steel ball or rotor. Figure 1 shows the essential elements of the SRG: the rotor, thimble, head with connecting cable, and electronic controller. The rotor, or ball, is contained within the thimble during operation and is normally not handled by nor is visible to the SRG user. The thimble is connected to the vacuum system. To operate the SRG, the head is slipped over the thimble. The head contains two permanent magnets and several sets of wire coils used for vertical and horizontal stabilization, driving the rotor, and sensing the rotation. The electronic controller interprets the signal from the sensing coil so that a pressure measurement can be made. For a rotor with ideal surface conditions, the deceleration rate is related to the vacuum pressure by fundamental physics. To make absolute pressure measurements using an SRG, a calibration factor, known as the effective accommodation coefficient, must be determined. The effective accommodation coefficient depends on the real surface conditions of the rotor, such as the roughness, adsorbed gases, and scratches. These factors tends to be stable over the course of its use. Additional details of SRGs can be found in other references.^1-3

The SRG is used in applications where absolute vacuum measurements are required. For example, calibration laboratories often use SRGs as an absolute vacuum standard. In this case, high-vacuum gauges are calibrated by comparing their reading to that of the SRG. In turn, the SRG standard must be periodically calibrated by shipping the SRG to a primary calibration laboratory to have its accommodation coefficient re-determined. Primary calibration labs are usually National Metrology Institutes such as the National Institute of Standards and Technology (NIST). The primary lab determines the SRG accommodation coefficient by comparing its reading to a primary vacuum standard, and then returns the SRG to the "secondary" calibration lab. The SRG is also used as a transfer standard for the comparison of standards between calibration laboratories or National Metrology Institutes. In this application, the SRG is transported domestically or internationally between the various laboratories.^4-8 During shipment, events can occur that change the accommodation coefficient. Prior to shipment, the rotor must be de-suspended and the head is removed; the rotor then rests on the interior wall of the thimble. During transport, the rotor surface is subject to change from the mechanical action between the rotor and thimble due to vibrations and shocks, or the surface may change due to the exposure of the rotor to atmospheric gas and humidity. These changes affect the long-term stability of the accommodation coefficient. Ideally, the rotor should remain in vacuum and immobilized during transport.

Historically, SRGs have been used as transfer standards in key comparisons of vacuum standards among national metrology institutes, where SRGs are internationally transported many times among the various institutes.⁹ During an early key comparison, it was found that the long-term stability of the SRG accommodation coefficient could be improved by utilizing a spring-transport mechanism which both immobilized the rotor and kept it under vacuum during transportation.^1,10 Since then, the spring-transport mechanism has been used many times in international key comparisons. A recent study of the historical data showed that 90% of these comparisons had stabilities better than 0.75%, and 70% had stabilities of 0.5%.⁹ Therefore, using a spring-transport mechanism will, in most cases, yield a stability that is more than sufficient for most applications.

Until now, there has been little guidance in the literature on how to build a spring-transport mechanism. Early versions of these devices have been known to fail to fully immobilize the rotor, due to a combination of being insufficiently designed for robustness, and being mishandled during shipment. These early lessons show that it is important both to build a robust spring-transport mechanism, and to properly package it in a way that minimizes shock during transport. This later point is critical but often ignored. Here we will describe the construction of a robust spring-transport mechanism in addition to a properly constructed transport package. Our design is based on a few simple, tested, engineering principles that enable the construction of a durable spring-transport package that minimizes the possibility of failure during transport. We also describe our tests of the robustness of our design. Additional details of the test methods can be found in Fedchak et al. (2015).¹¹

Protokół

1. Procure Non-custom Parts for the Spring Transport Mechanism

1. Procure the springs, threaded rod, standoffs, nuts, and washers. These items are listed in the List of Specific Materials/Equipment. Purchase the springs and standoffs before manufacturing the ball holder. Use 18-8 stainless steel (except 303), or preferably 316 stainless steel, for all materials.
2. Procure rotor. The rotor is a ball-bearing 4.5 mm in diameter made of 440C stainless steel or E52100 alloy steel.
3. Procure the right-angle valve listed in the List of Specific Materials/Equipment.

2. Procure Materials for the Shipping Container

1. Procure the shipping container. Use rotationally-molded, polyethylene hard-shell cases with protected recesses since these were the type of cases that were successfully tested. The case in the List of Specific Materials/Equipment meets the minimum interior space requirements.
2. Procure the foam packing.
   1. Procure 2# (32 kg/m³) polyurethane (ester) foam. Purchase enough ester foam to fill the top and bottom of the shipping container. Purchase a piece of 5 cm egg-carton ester foam.
   2. Procure 2# (PE) polyethylene foam that is 7.6 cm thick and has a large enough area to cover the width and depth of the shipping container.

3. Procurement and Fabrication of Custom Parts for the Spring-transport Mechanism 

Note: Example drawings of the custom parts described in this section are given in Figures 2-4. 

1. Produce and submit drawings to custom vendor or in-house shop for manufacturing the spinning rotor gauge (SRG) thimble/flange. Critical dimensions are given in Figure 2. The custom manufacturer must be familiar with ultra-high vacuum (UHV) manufacturing techniques. The thimble is relatively simple to manufacture and is well within the ability of many vacuum component companies.
2. Acquire the tines that hold the SRG head to the flange (see Figure 1). These may be removed from the commercial SRG thimble/flange assembly that comes with the SRG electronic control unit. Each tine is held in place by a single bolt (typically a metric hex socket head) with a lock washer, and may be removed by unbolting using the appropriate wrench (such as a metric hex key).
   1. Alternatively, fabricate these by the same vendor providing the thimble/flange as in the previous step, but ultra-high vacuum manufacturing techniques need not be followed. Make exact copies of the commercial SRG tines.
3. Produce and submit drawings for the simple adapter to connect the M6 stud on the right-angle valve to an 8-32 all-thread stud (American standard hardware). See Figure 3.
4. Produce and submit drawings for the fabrication of the ball holder. Critical dimensions are given in Figure 4. Fabricate the ball holder of 316L stainless steel in accordance with UHV manufacturing techniques. Tack weld the ball holder to one end of a spring. Tack weld the other end of the spring to the standoff. Clean all parts in accordance to the cleaning procedure given in section 5.
5. Cut the 8-32 all-thread stud to a length of 18 mm and clean as described in section 5.

4. Fabrication of Custom Foam Cut-out

1. Make a cut-out for the spring-transport mechanism in the PE foam. Follow the contours of the valve assembly as closely as possible. Do this by hand using a sharp utility knife; alternatively, the contour may be professionally cut by a packaging supplier.
2. Use the dimensions of the valve given by the valve manufacturer and the thimble/flange dimensions given in Figure 2. Cut the space for the thimble large enough to accommodate the tines (1.5 cm x 3.8 cm).

5. Cleaning of the Vacuum Components 

1. Clean all vacuum components for ultra-high vacuum (UHV) before assembly. Our recommended cleaning procedure is as follows.
   1. Handle vacuum parts using Nitrile, Latex, or vinyl gloves. Do not touch with bare hands.
   2. Clean parts using a mild detergent (such as listed in the materials/equipment list) dissolved in distilled or de-ionized water and a lint-free cloth.
   3. Place parts in a bath of mild detergent dissolved in distilled or de-ionized water and place in an ultra-sonic cleaner for 20 min.
   4. Rinse parts thoroughly with distilled or de-ionized water.
   5. Cover parts with acetone and place in an ultra-sonic cleaner for 20 min.
   6. Remove parts from acetone. Cover parts with ethanol and place in an ultra-sonic cleaner for 20 min.
   7. Remove parts from ethanol. Rinse thoroughly with distilled or de-ionized water.
   8. Blow the parts dry with dry nitrogen or clean dry air.
   9. Let parts air dry on a clean-room quality lint-free cloth for 24 hr.

6. Assemble the Spring-transport Mechanism

1. During assembly, wear nitrile, vinyl, or latex gloves. Do not touch vacuum parts with bare hands.
2. Gather the necessary tools: needle nose pliers, socket head driver for 8-32 nut, wrench for adapter, ruler or caliper. Wipe clean the ruler/micrometer with ethanol; clean all other tools using the procedure in step 5.
3. Gather the necessary parts: the valve, thimble, ball-bearing, ball-holder/spring assembly (see step 3.5), 18 mm long 8-32 stud, thread adapter, nuts, and lock-washers, 3 mm Allen wrench and masking tape. See Figure 5.
4. Spring-Transport Mechanism Assembly:
   1. Fully close the right-angle valve by turning it clockwise until it stops.
   2. Looking through the valve ports, identify the M6 stud centered on the valve seat.
   3. Screw the adapter snugly onto the M6 stud. Insert an UHV clean wrench or pliers through the port to get the adapter as snug as possible.
   4. Insert 8-32 stud into the other end of the adapter. Tighten as snugly as possible. The 8-32 stud will extend through the adapter and push against the M6 stud.
   5. Place lock-washer on 8-32 stud and then a nut. Tighten the nut using a clean socket driver or pliers. The valve may be closed during this step to make tightening easier.
   6. Place a nut on the 8-32 stud. Turn it until nearly touching the nut on the other end. Place lock washer on 8-32 stud.
   7. Attach spring/ball-holder to the 8-32 stud by the standoff. Turn the standoff until it is touching the lock-washer.
      Note: The following procedure describes how to check the length adjustment of the spring assembly, see Figure 6.
   8. Place the rotor in the custom thimble and secure it with a magnet (from a commercial SRG) by placing it on the thimble end and fixing it with masking tape. The rotor is now at the end of the thimble.
   9. Slide thimble over spring/ball-holder, stop when the ball-holder touches the ball. Measure the gap between the valve flange and thimble flange, as in Figure 6.
      1. If the gap is in the range of 2 mm to 6 mm, skip to step 6.4.10.2). A nominal gap of 3 mm is ideal, but a gap in the range is of 2 to 6 mm sufficient. A gap smaller than 2 mm is not acceptable.
      2. Remove thimble/flange assembly and set aside. If the gap was smaller than 2 mm, rotate the standoff counterclockwise to make the gap larger. If the gap was larger than 6 mm, rotate the standoff clockwise to make the gap smaller. Go back to step 6.4.10.
   10. Remove thimble/flange assembly and set aside. If the gap was smaller than 2 mm, rotate the standoff counterclockwise to make the gap larger. If the gap was larger than 6 mm, rotate the standoff clockwise to make the gap smaller. Go back to step 6.4.10.
   11. Tighten the nut against the standoff.
   12. Open the valve by turning counter-clockwise.
5. Assemble the Flange:
   1. Remove rotor by removing masking tape and magnet and carefully allowing the rotor to roll out of the thimble.
   2. Attach the two tines to the flange using a lock-washer and bolt inserted through the back-side of the custom flange/thimble. The lock-washer and bolt are provided by the commercial SRG. The lock-washer and bolt do not need to be cleaned for ultra-high vacuum.
   3. Rotate the tines so that they are square with one another, as in Figure 1 and Figure 9.
   4. Check tines for straightness by slipping the SRG head over the thimble. The head should slide on freely.
   5. Give the two bolts a final tightening and re-check for alignment as in step 6.5.3.
   6. Place rotor back into the thimble, and secure with the magnet and masking tape.
6. Complete Spring Transport Assembly:
   1. Place copper or silver-plated copper gasket on the valve port.
   2. Place the rotor into the thimble (if not already in thimble from step 6.5.6).
   3. Slide the flange/thimble assembly over the spring/ball-holder. Orient the flange such that the set-screw in the tines will be pointing downward when the valve is attached to the chamber.
   4. Using ¼-28 bolts and nuts, secure the flange to the valve.
   5. Close the valve.
   6. Remove magnet and tape holding the ball.

7. Assemble the Shipping Container

1. Cut the ester foam to the size of the shipping container. The thickness of the foam will depend on the height of the container. Place a minimum thickness of 7.6 cm of foam in the bottom. Figure 7 shows the foam assembly.
2. Place the PE foam cutout on top of the ester foam.
3. Place a layer of ester foam in the lid. The minimum thickness should be 7.6 cm. Figure 8 shows the final placement of the spring-transport mechanism. Use clean aluminum foil and a plastic endcap (that came with the valve) to protect the open end of the valve port during shipment.

8. Using the Spring-transport Mechanism

1. Mounting and suspending the rotor:
   Note: Figure 9 shows the mounted spring-transport mechanism with the head attached. The first step is remove the spring-transport mechanism from the shipping container. In the following, it is assumed that the reader is familiar with the operation of the spinning-rotor gauge. Details of operating the controller can be found in the controller user manual. It is also assumed the reader is familiar with high-vacuum technology.
   1. Remove the endcap and foil from the open port of the spring transport mechanism. Attach the open port to a DN 40 (CF 2.75") port on a vacuum chamber using a new copper or silver-plated copper gasket and a ¼-28 bolt set. The orientation of the valve will depend on the orientation of the tines. The proper orientation is shown in Figure 9. The tine with the set screw points downward. Slip the head over the thimble, the orientation of the thimble should be vertical to within 2°.  Check orientation with a level.
   2. Evacuate the vacuum chamber to less than 10^-3 Pa. Slowly open the spring-transport mechanism valve.
   3. Attach head to the controller. Turn on controller and suspend the ball.
2. De-mounting the Spring-Transport Mechanism
   1. De-suspend the rotor using the electronic controller. Turn off controller.
   2. Close the spring-transport mechanism valve.
   3. Remove head.
   4. Vent vacuum chamber.
   5. Remove the spring-transport mechanism by un-bolting the valve port from the vacuum chamber.
   6. Place clean foil and a plastic endcap over the open port of the spring-transport mechanism. Place spring-transport mechanism in cut-out in shipping container.

Wyniki

All of the components of commercial SRG are shown in Figure 1. This includes the rotor, thimble, head containing the permanent magnets and wire coils used for suspension and pickup, and the electronic controller. The small spring shown (Figure 1c) is used to retain the ball in the thimble; this retainer spring is not used in the spring-transport mechanism. The commercial controller and head are used in the spring-transport mechanism. The tines from the co...

Dyskusje

The objective was to design a spring-transport mechanism with a sufficient holding force such that the rotor would remain immobilized during transport. Designing a robust spring-transport mechanism is not enough to insure the rotor will remain immobilized because, for example, dropping the mechanism from tall height onto a hard surface can produce an enormous shock. The force on the rotor can be greatly reduced by packaging the spring-transport mechanism such that it gently decelerates over a distance within the package,...

Materiały

Name	Company	Catalog Number	Comments
Spring, 3 N/m	Lee Spring (www.leespring.com)	LC 042C 18 S316	Outside diameter 0.240 in, Wire Diameter 0.042 in, Rate 17.1 lb⁠/⁠in, Free Length 2.25 in, Number of Coils 29.3
8-32 threaded rod, 316 stainless steel	McMaster-Carr (www.mcmaster.com)	90575A260	Type 316 Stainless Steel Fully Threaded Stud 8-32 Thread, 3" Length.  Cut to length specified in protocol
standoffs, 8-32 Screw Size	McMaster-Carr (www.mcmaster.com)	91125A140	18-8 Stainless Steel Female Threaded Round Standoff, 1/4" OD, 1/4" Length, 8-32 Screw Size
nuts, 8-32	McMaster-Carr (www.mcmaster.com)	90205A309	316 SS Undersized Machine Screw Hex Nut 8-32 Thread Size, 1/4" Width, 3/32" Height
Split Lock-Washers, 316 Stainless Steel	McMaster-Carr (www.mcmaster.com)	92147A425	Type 316 Stainless Steel Split Lock Washer NO. 8 Screw Size, .3" OD, .04" min Thick
Steel Rotor	McMaster-Carr (www.mcmaster.com)	9292K38	Bearing-Quality E52100 Alloy Steel, Hardened Ball, 4.5 mm Diameter
Right-Angle Valve	VAT Valve (www.vatvalve.com)	54132-GE02-0001	Easy-close all-metal angle valve, DN 40 (1.5")
Shipping Container	Allcases, Reekstin & Associates (www.allcases.com)	REAL1616-1205	Zinc Hardware w/Zinc Handles, Rotationally Molded, light-weight, high-impact, Polyethylene Case with protected recessed hardware.  15.75" x 15.88" x 16.45"
Ester Foam	Carry Cases Plus (www.carrycasesplus.com)	ES-PAD 3" Thick	3" Thick, 2 lb Charcoal Ester Foam Pad, 24" x 27".
Ester Foam	Carry Cases Plus (www.carrycasesplus.com)	ES-PAD 1" Thick	1" Thick, 2 lb Charcoal Ester Foam Pad, 24" x 27".
Egg-carton ester foam	Carry Cases Plus (www.carrycasesplus.com)	ES-CONV	ES-CONV, 2 lb, 24" x 27" x 1 1/2".  "egg-crate" ester foam.
Foam Cutout, PE foam	Willard Packaging Co. (www.willardpackaging.com)		Custom Foam Cutout.
Spinning Rotor Gauge	MKS Instruments (www.mks.com)	SRG-3	Controller, head, and thimble.  Custom thimble must be used for the spring-transport mechanism
Custom thimble	MDC vacuum Inc. (www.mdcvacuum.com)		drawing must be submitted for custom part
Detergent	Fisher Scientific Co (www.fischersci.com)	04-320-4	Sparkleen 1 Detergent
Acetone	Fisher Scientific Co (www.fischersci.com)	A18-S4	Acetone (Certified ACS)
Ethanol	Warner-Graham Company (www.warnergraham.com)	190 proof USP	190 Proof USP ethyl alcohol
Bolt set for valve	Kurt J. Lesker (www.lesker.com)	TBS25028125P	B,N&W set, 12 point, (25)1/4-28 x 1.25", for 2.75" thru, silver plat
Silver-plated copper gaskets	Kurt J. Lesker (www.lesker.com)	GA-0275LBNSP
Spring Assembly (welding)	Omley Industries, Inc. (www.omley.com)	N/A	The machine work and welding were done in NIST's shop. However, Omley industries was used as an alternative for welding the spring assembly.