Methods Article

Screening of Coatings for an All-Solid-State Battery Using In Situ Transmission Electron Microscopy

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07:20 min

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January 20th, 2023

DOI :

10.3791/64316-v

January 20th, 2023

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Shibarata Basak¹^,², Junbeom Park¹, Janghyun Jo², Osmane Camara¹, Amir H. Tavabi², Hermann Tempel¹, Hans Kungl¹, Chandramohan George³, Rafal E. Dunin-Borkowski², Joachim Mayer²^,⁴, Rüdiger-A. Eichel¹^,⁵

¹Institute of Energy and Climate Research - Fundamental Electrochemistry (IEK-9), Forschungszentrum Jülich GmbH, ²Ernst Ruska-Centre for Microscopy and Spectroscopy with Electrons, Forschungszentrum Jülich GmbH, ³Dyson School of Design Engineering, Imperial College London, ⁴Central Facility for Electron Microscopy (GFE), RWTH Aachen University, ⁵Institute of Physical Chemistry, RWTH Aachen University

Podsumowanie

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All solid state Battery

Coatings

In Situ Transmission Electron Microscopy

Silicon Nanoparticles

Rozdziały w tym wideo

0:04

Introduction

1:00

Preparation of Half‐Cut TEM Grids with Coated Si Nanoparticles for Checking the Suitability of ALD‐Deposited Titanium Dioxide Coatings

1:53

Preparing the Tungsten Needle

2:37

Loading the Drop‐Casted TEM Grid and Lithium Loaded Tungsten Needle into the In Situ TEM Holder

3:15

Inserting the Assembled In Situ Holder into the TEM

4:02

Performing the In Situ Biasing Experiment in the TEM and Analyzing the TEM Images

5:37

Results: Screening Method of Potential Coatings for All‐Solid‐State Batteries Using In Situ Transmission Electron Microscopy

6:28

Conclusion

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