Thermocouple Preparation and Alignment in the Optical Dewer
3:16
Temperature-dependent Cryogenic Spectroscopy in the Optical Dewar
4:34
Results: [Rh(4,7-Me2-1,10-phen)3]3+ and Related Compounds
5:34
Conclusion
TRANSCRIÇÃO
The overall goal of this experiment is to measure temperature dependent luminescence spectral intensities. This method can help answer key questions on the topic of excited state energy migration in metal complexes. Such as, ruthenium diamine comp
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A simple liquid nitrogen Dewar/cryostat apparatus comprised of a small fused silica optical Dewar, a thermocouple, and a charge-coupled device (CCD) spectrograph are described. The experiments for which this Dewar/cryostat is designed require fast sample loading, freezing, and alignment, accurate and stable sample temperatures, and small size/portability.