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Structure and Coordination Determination of Peptide-metal Complexes Using 1D and 2D 1H NMR

DOI :

10.3791/50747-v

December 16th, 2013

December 16th, 2013

9,362 Views

1Department of Chemistry, The Hebrew University of Jerusalem, 2Wolfson Centre for Applied Structural Biology, The Hebrew University of Jerusalem

The NMR-solution structure of a metallochaperone model peptide with Cu (I) was determined, and a detailed protocol from sample preparation and 1D and 2D data collection to a three-dimensional structure is described.

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Peptide metal Complexes

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