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JoVE Journal

Chemistry

This content is Open Access.

Microwave-assisted Functionalization of Poly(ethylene glycol) and On-resin Peptides for Use in Chain Polymerizations and Hydrogel Formation

28.4K Views

15:33 min

October 29th, 2013

October 29th, 2013

28,427 Views

0:05

Title

1:58

Microwave-assisted Synthesis of PEGDM and Characterization of Functionalization

5:07

Microwave-assisted Functionalization of On-resin Peptides

8:23

Characterization of Peptide Functionalization

9:35

Characterization of Functionalized PEGDM and Peptides, and Demonstration of Their Use in Hydrogel Formation

14:39

Conclusion

This video will illustrate a rapid, efficient method to methacrylate poly(ethylene glycol), enabling chain polymerizations and hydrogel synthesis. It will demonstrate how to similarly introduce methacrylamide functionalities into peptides, detail common analytical methods to assess functionalization efficiency, provide suggestions for troubleshooting and advanced modifications, and demonstrate typical hydrogel characterization techniques.

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