Pd Nanoparticle Characterization by Ex Situ Small-Angle X-Ray Scattering (SAXS)
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Results: Kinetics of Nucleation and Growth of Pd Nanoparticles in Toluene and Pyridine
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Conclusion
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The advantage of this SAXS technique is that it can obtain the time evolution of particle size distribution and the actual concentration of particles at the same time. Extracting the kinetic rates from SAXS is crucial for understanding the effects
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The main goal of this work is to elucidate the role of capping agents in regulating the size of palladium nanoparticles by combining in situ small angle x-ray scattering (SAXS) and ligand-based kinetic modeling.