This study received support from the Research Initiation Grant (RIG) of the Vice President for Research and Economic Development at the University of North Texas (UNT). The authors also thank KCIS Co. Ltd for partially supporting this study. The support from PACCAR Technology Institute at UNT to the success of this publication is greatly appreciated.

1. Planning of Experiment
<ol>
	<li>Draw a sacrificial pattern (an octet truss structure with a sprue system) using computer aided design (CAD) software as shown in Figure 1 and save the CAD model as an STL file format. 
	Note: The sacrificial pattern is an integrated pattern of the octet truss structure with a sprue system that will be eventually melted for casting. Because the sacrificial pattern includes both the octet truss structure and the sprue system, it does not exactly represent the octe...

<ol>
	<li>Gibson, L. J., Ashby, M. F. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=.">.</a> Cellular Solids-Structure and properties. , (1997).</li><li>Schaedler, T. A., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Ultralight+Metallic+Microlattices.">Ultralight Metallic Microlattices.</a> J. Science. 334 (6058), 962-965 (2011).</li><li>Zheng, X., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Ultrastiff+Mechanical+Metamaterials.">Ultrastiff Mechanical Metamaterials.</a> J. Science. 334 (6190), 1373-1377 (2014).</li><li>Ju, J., Summers, J. D., Ziegert, J., Fadel, G. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Design+of+Honeycombs+for+Modulus+and+Yield+Strain+in+Shear.">Design of Honeycombs for Modulus and Yield Strain in Shear.</a> J. Eng. Mater. &amp; Technol. 134 (1), 11-22 (2012).</li><li>Lee, J., Kim, K., Ju, J., Kim, D. M. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Compliant+Cellular+Materials+with+Elliptical+Holes:+Materials+Design+with+Mechanisms.">Compliant Cellular Materials with Elliptical Holes: Materials Design with Mechanisms.</a> Transactions of the ASME: Eng. Maters. &amp; Technol. 131 (1), 1-14 (2015).</li><li>Tan, H., Qu, S. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Chap+6:+Impact+of+Cellular+Materials.">Chap 6: Impact of Cellular Materials.</a> Cellular and Porous Materials in Structures and Processes. , (2010).</li><li>Phani, A. S., Woodhouse, J., Fleck, N. A. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Wave+Propagation+in+Two-Dimensional+Periodic+Lattices.">Wave Propagation in Two-Dimensional Periodic Lattices.</a> Acoust. Soc. A. 119 (4), 1995-2005 (2006).</li><li>Kumar, R. S., McDowell, D. L. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Rapid+Preliminary+Design+of+Rectangular+Linear+Cellular+Alloys+for+Maximum+Heat+Transfer.">Rapid Preliminary Design of Rectangular Linear Cellular Alloys for Maximum Heat Transfer.</a> AIAA. 42 (8), 1652-1661 (2004).</li><li>Banhart, J., Weaire, D. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=On+the+Road+Again:+Metal+Foams+Find+Favor.">On the Road Again: Metal Foams Find Favor.</a> Physics Today. 55 (7), 37-42 (2002).</li><li>Wadley, H. N. G., Fleck, N. A., Evans, A. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Fabrication+and+Structural+Performance+of+Periodic+Cellular+Metal+Sandwich+Structures.">Fabrication and Structural Performance of Periodic Cellular Metal Sandwich Structures.</a> Comp. Sci. and Technol. 63, 2331-2343 (2003).</li><li>Mori, L. F., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Deformation+and+Fracture+Modes+of+Sandwich+Structures+Subjected+to+Underwater+Impulsive+Loads.">Deformation and Fracture Modes of Sandwich Structures Subjected to Underwater Impulsive Loads.</a> Mech. of Mater. &amp; Struct. 2 (10), 1981-2006 (2007).</li><li>Queheillalt, D. T., Murty, Y., Wadley, H. N. G. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Mechanical+Properties+of+an+Extruded+Pyramidal+Lattice+Truss+Sandwich+Structure.">Mechanical Properties of an Extruded Pyramidal Lattice Truss Sandwich Structure.</a> Scripta Materialia. 58 (1), 76-79 (2008).</li><li>Queheillalt, D. T., Desphande, V. S., Wadley, H. N. G. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Truss+Waviness+Effects+in+Cellular+Lattice+Structures.">Truss Waviness Effects in Cellular Lattice Structures.</a> Mech. of Mater. &amp; Struct. 2 (9), 1657-1675 (2007).</li><li>Mullen, L., Stamp, R. C., Brooks, W. K., Jones, E., Sutcliffe, C. 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A. 368, 1999-2032 (2011).</li><li>Murali, K., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Direct+Selective+Laser+Sintering+of+Iron-Graphite+Powder+Mixture.">Direct Selective Laser Sintering of Iron-Graphite Powder Mixture.</a> Mater. Proc. Technol. 136, 179-185 (2003).</li><li>Lott, P., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Design+of+an+Optical+System+for+the+In-Situ+Process+Monitoring+of+Selective+Laser+Melting+(SLM).">Design of an Optical System for the In-Situ Process Monitoring of Selective Laser Melting (SLM).</a> Ph. P. 12, 683-690 (2011).</li><li>Song, B., Dong, S., Liu, Q., Liao, H., Coddet, C. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Vacuum+Heat+Treatment+of+Iron+Parts+Produced+by+Selective+Laser+Melting:+Microstructure,+Residual+Stress,+and+Tensile+Behavior.">Vacuum Heat Treatment of Iron Parts Produced by Selective Laser Melting: Microstructure, Residual Stress, and Tensile Behavior.</a> Mater. Design. 54, 727-733 (2014).</li><li>Yadroitsev, I., Smurov, I. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Surface+Morphology+in+Selective+Laser+Melting+of+Metal+Powders.">Surface Morphology in Selective Laser Melting of Metal Powders.</a> Ph. P. 12, 264-270 (2011).</li><li>Antonysamy, A. A., Meyer, J., Prangnell, P. B. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Effect+of+Build+Geometry+on+the+&#946;-grain+Structure+and+Texture+in+Additive+Manufacture+of+Ti-6Al-4V+by+Selective+Election+Beam+Melting.">Effect of Build Geometry on the &#946;-grain Structure and Texture in Additive Manufacture of Ti-6Al-4V by Selective Election Beam Melting.</a> J. of Mat. Charact. 84, 153-168 (2013).</li><li>Ladani, L. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Local+and+Global+Mechanical+Behavior+and+Microstructure+of+Ti6Al4V+Parts+Built+Using+Electron+Beam+Melting+Technology.">Local and Global Mechanical Behavior and Microstructure of Ti6Al4V Parts Built Using Electron Beam Melting Technology.</a> J. of Metalllur. &amp; Mater. Trans. 46, (2015).</li><li>Chiras, S., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=The+Structural+Performance+of+Near-Optimized+Truss+Core+Panels.">The Structural Performance of Near-Optimized Truss Core Panels.</a> Solids Struct. 39, 4093-4115 (2002).</li><li>Meisel, N. A., Williams, C. B., Druschitz, A. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Lightweight+Metal+Celluar+Structures+via+in+Direct+3D+Printing+and+Casting.">Lightweight Metal Celluar Structures via in Direct 3D Printing and Casting.</a> Proceedings of the 24th Solid Freeform Fabrication Symposium. , (2013).</li><li>Mun, J., Ju, J., Yun, B. -. G., Chang, B. -. M., Kim, D. -. M. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=A+Numerical+Study+of+Molten+Aluminum+for+Investment+Casting+of+3D+Cellular+Metals.">A Numerical Study of Molten Aluminum for Investment Casting of 3D Cellular Metals.</a> Proceedings of the ASME International Mechanical Engineering Congress and Exposition. , (2013).</li><li>Mun, J., Yun, B. -. G., Ju, J., Chang, B. -. M. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Indirect+Additive+Manufacturing+Based+Casting+of+a+Periodic+3D+Cellular+Metal+-+Flow+Simulation+of+Molten+Aluminum+Alloy.">Indirect Additive Manufacturing Based Casting of a Periodic 3D Cellular Metal - Flow Simulation of Molten Aluminum Alloy.</a> Manufact. Process. 17, 28-40 (2015).</li><li>Challapalli, A., Ju, J. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Continuum+Model+for+Effective+Properties+of+Orthotropic+Octet-Truss+Lattice+Materials.">Continuum Model for Effective Properties of Orthotropic Octet-Truss Lattice Materials.</a> Proceedings of the ASME International Mechanical Engineering Congress and Exposition. , (2014).</li><li>Taylor, H. F., Flemings, M. C., Wulff, J. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=.">.</a> Foundry Engineering. , (1959).</li><li>Mun, J., Ju, J., Thurman, J. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Indirect+Additive+Manufacturing+Based+Casting+(I+AM+Casting)+of+a+Lattice+Structure.">Indirect Additive Manufacturing Based Casting (I AM Casting) of a Lattice Structure.</a> Proceedings of the ASME International Mechanical Engineering Congress and Exposition. , (2014).</li><li>Mun, J., Ju, J., Thurman, J. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Indirect+Additive+Manufacturing+of+a+Copper+Alloy+Cubic+Lattice+Structure.">Indirect Additive Manufacturing of a Copper Alloy Cubic Lattice Structure.</a> Proceedings of the 25th Annual International Solid Freeform Fabrication Symposium. , (2014).</li><li>. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Volume+2+Properties+and+Selection:+Nonferrous+Alloys+and+Pure+Metals.">Volume 2 Properties and Selection: Nonferrous Alloys and Pure Metals.</a> Metals Handbook Ninth Edition. , (1979).</li><li>Romano, J., Ladani, L., Razmi, J., Sadowski, M. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed&cmd=Search&doptcmdl=Citation&defaultField=Title+Word&term=Temperature+Distribution+and+Melt+Geometry+in+Laser+and+Electron-beam+Melting+Processes+-+A+Comparison+Among+Common+Materials.">Temperature Distribution and Melt Geometry in Laser and Electron-beam Melting Processes - A Comparison Among Common Materials.</a> J. of Additive Manuf. 8, 1-11 (2015).</li></ol>

For conventional metal casting, it is important to keep the molten metal&#39;s flow smooth and streamlined in &#39;laminar&#39; in the mold cavity and rather avoid irregular and agitated flow generally observed in turbulent flow27. Accordingly, it is important to properly design the inlet of the sprue system associated with the rotating speed of a centrifugal arm to maintain the flow of molten metal inside the lattice mold cavity &#39;laminar&#39;.
In this study, the critical steps ...

Cellular metals are the metals made up of an interconnected network of solid struts or plates and have complex micro-architectures with voids1. Examples include both i) randomly structured stochastic foams and ii) periodically ordered two-dimensional (2D) honeycombs and three-dimensional (3D) lattice truss structures. They have received attention due to their high specific stiffness and strength1-3and high specific resilience4-5, excellent energy absorption for impact loading6, acoustic insulation7, possible design of heat dissipaters and heat exchangers8. Especially, periodically ordered lattice structures have the potential to engineer the properties superior with a capability to control the internal porous network geometry.
Due to their complex internal porous network geometry, it is difficult to manufacture cellular metals using the conventional subtractive machining. As such, researchers have started looking for alternative methods to fabricate cellular metals: forming gas in liquid metal or mixing metal powder with blowing agents were explored for manufacturing stochastic metal forms9. Due to the lack of control over cell topology, it is hard to tailor mechanical properties. Alternatively, manufacturing methods for periodically ordered cellular metals were explored: stamping thin sheets of metal into a corrugated shape followed by joining them to create periodic structures10, bonding slotted metal sheets11, extrusion12, weaving and blazing metal filaments to fabricate textiles13. Even though these manufacturing methods offer repeatable patterns, the patterns are still limited in the planar direction. In an effort to generate 3D pattern repetition, researchers started using additive manufacturing (AM); e.g., Selective Laser Melting (SLM)14, Electron Beam Melting (EBM)15, and Direct-Metal Laser Sintering (DMLS)16. Despite their capability to fabricate 3D ordered complex lattice geometries, there still exist some limitations: difficulty using metals with high thermal conductivity and high optical reflectivity17, high thermal residual stress18, poor surface finish with the &#39;balling&#39; phenomenon during laser or electron melting 19, anisotropic properties20-21 of parts caused by a combined effect of the layered manufacturing, anisotropic formation of grains, powder size, power and scanning speed of laser or electron beam15, high energy consumption, etc.
Combining polymer based AM with metal casting may provide an alternative method to manufacture lattice metals. One may call this &#34;indirect AM&#34;. Indirect AM may provide a solution to overcome the technical problems of direct AM of metals mentioned above. Several efforts have been made to manufacture lattice metals using indirect AM combining 3D printing of polymers with gravity based casting22-25; e.g., an investment casting combined with fused deposition modeling (FDM) to fabricate a lattice alloy22-25 or sand casting combined with a sand powder based AM23. The gravity based casting appears to remain a technical challenge to overcome - misrun and porosity caused by sudden solidification of molten metals when they meet network structures with sharp corners of lattice structural molds25-26. Relatively large surface area of lattice structural molds also appears to contribute to sudden cooling, resulting in premature solidification25-26.
In this study, we propose an alternative indirect AM that may overcome the misrun during manufacturing of lattice metals - centrifugal casting to a lattice mold cavity made by a 3D printed lattice sacrificial polymer pattern. We use a digital light processing (DLP) based 3D printing method to build a lattice structural sacrificial pattern followed by centrifugal casting of Al and Cu alloys. The objective of this study is to provide a detailed protocol on fabrication of 3D lattice metals having a complex shape and a thin wall thickness. The main contribution of this process is to provide an opportunity to extend the selection of materials with low manufacturing cost for manufacturing lattice metals.

<table>
	<tbody>
		<tr>
			<td>Motorized centrifugal casting machine</td>
			<td>Rey Motorized Centrifugal Casting Machine, Rey Industries Inc.</td>
			<td></td>
			<td>Made in U.S.A. by Rey industries, Inc. Dallas, TX 75220</td>
		</tr>
		<tr>
			<td>Gypsum powder</td>
			<td>Satin Cast 20, FindingKing Kerr</td>
			<td>7960</td>
			<td>Gypsum powder is used to make the investment mixture</td>
		</tr>
		<tr>
			<td>Ployjet 3D printer</td>
			<td>Projet HD3500 Plus, 3D Systems</td>
			<td></td>
			<td>This polymer based 3D printer to print out sacrificial pattern for casting.</td>
		</tr>
		<tr>
			<td>Cartridge materials - UV curable and castable acrylic plastic</td>
			<td>VisiJet Procast, 3D Systems</td>
			<td></td>
			<td>This is castable material that is going to be burn out before casting</td>
		</tr>
		<tr>
			<td>Cartridge materials- support material</td>
			<td>VijiJet S300, 3D Systems</td>
			<td></td>
			<td>This is support material that is going to be removed before pattern assemble</td>
		</tr>
		<tr>
			<td>Ancient Bronze Casting Grain</td>
			<td>Rio Grande</td>
			<td>706051</td>
			<td>This true bronze grain contains no zinc. Highly fluid, it melts quickly, casts cleanly and provides a good balance between strength and durability. The warm, deep-bronze color has rich red undertones, and the alloy takes a good patina. 
			Composition is 90% copper with an amount of tin; fits into the CDA#90700 category. This grain is sold in 1-lb. packages.</td>
		</tr>
		<tr>
			<td>Aluminum Round Wire, 1/8&#34;, 1-Lb. Spool, Dead Soft</td>
			<td>Rio Grande</td>
			<td>134700</td>
			<td>Lightweight and strong, aluminum wire is an economical and versatile choice. Not as bright-white as silver, aluminum offers a warmer tone much like that of platinum. Solder ONLY with low-temp solders such as Stay-Brite; suitable for both pulse-arc and laser welding. This quality aluminum wire is packaged on 1-lb. spools.</td>
		</tr>
		<tr>
			<td>Computer aided design software (Pro-e)</td>
			<td></td>
			<td></td>
			<td>This software can be replaced with the others such as Auto CAD, Catia, and so on.</td>
		</tr>
		<tr>
			<td>ProJet Finisher 1-A</td>
			<td>3D Systems</td>
			<td></td>
			<td>This machine is used to melt the support material.</td>
		</tr>
		<tr>
			<td>160 Watt 2.5 Liters Digital Ultrasonic Cleaner with Timer Heater Rings Tools</td>
			<td>Chicago, Electric, Power Tools</td>
			<td></td>
			<td>85 oz. capacity, Five cleaning cycles: 90, 180, 280, 380 and 480 seconds, Clean with or without heat, Easy-to-read LED digital timer, Clear-view window</td>
		</tr>
		<tr>
			<td>Fan&#160;</td>
			<td>Honeywell Inc.&#160;</td>
			<td>HT-800</td>
			<td>120V A.C., 60Hz., 0.85A. TP</td>
		</tr>
		<tr>
			<td>Paraffin wax for wax sheet - Modeler&#39;s Pink Wax Sheet, 3&#34; by 6&#34;, 24-Ga.</td>
			<td>Rio Grande</td>
			<td>700075</td>
			<td>Sheet wax is flexible and can be cut or formed into any shape. It&#8217;s ideal for designing since you can draw or trace directly onto the sheet; choose green or pink depending on which will best show your designs. High manufacturing standards ensure exceptional consistency and significant price savings. Value is enhanced by larger package quantities at the same price as the smaller packages available elsewhere. Each 8-oz. package contains approximately 30 sheets.</td>
		</tr>
		<tr>
			<td>Paraffin wax for wax stick - Modeler&#39;s Medium Red Sprue Wax, 8-Ga</td>
			<td>Rio Grande</td>
			<td>700741</td>
			<td>A pliable, softer sprue wax than the firm blue. Good for forming gates and sprues and burns out cleanly with no residue.</td>
		</tr>
		<tr>
			<td>Alcohol Lamp</td>
			<td>Rio Grande</td>
			<td>700008</td>
			<td>Use this lamp to heat wax-working tools or as a flame polisher. The heavy glass reservoir has faceted sides to allow it to be tipped for angling the flame. A screw adjustment for the 7&#34; x 3/16&#34; wick controls the height of the flame. A safety cap snuffs the flame and prevents fuel evaporation. For the best flame, use methyl alcohol fuel. Replacement wicks available. Reservoir holds 5 oz. (150ml) of fuel.</td>
		</tr>
		<tr>
			<td>Wax carving tool set - Soft Grip Wax Carvers, Set of 10</td>
			<td>Rio Grande</td>
			<td>700329</td>
			<td>This boxed set offers the best in cutting and shaping technology. Each of these ten high-quality steel wax-carving tools features a 5/16&#34; PVC covered handle that ensures a sure, comfortable grip through hours of work and all have sharp edges for shaping and fine detailing. Sharpen or custom-shape each tool to fit your needs. These tools provide exceptional tool strength and deliver excellent results. This set comes in a hinged, foam-lined wood box.</td>
		</tr>
		<tr>
			<td>Rubber Mixing Bowl, 1-1/2 Qt.</td>
			<td>Rio Grande</td>
			<td>702131</td>
			<td>This highly-flexible vulcanized rubber bowl is easy to grip, will not be marred by a spatula and cleans with ease.</td>
		</tr>
		<tr>
			<td>Pyrex Beaker, 1,000ml</td>
			<td>Rio Grande</td>
			<td>335040</td>
			<td>Ideal for holding and heating bath plating solutions, this genuine Pyrex glass beaker is sturdy and durable.</td>
		</tr>
		<tr>
			<td>Rio Premium Stainless Steel Flask, 2-1/2&#34; dia.</td>
			<td>Rio Grande</td>
			<td>70201514</td>
			<td>This solid, #304-quality stainless steel flask is corrosion-resistant, durable for a long service life and performs under extreme temperature without distortion.</td>
		</tr>
		<tr>
			<td>CAST/T Ceramic Casting Crucible, 450g</td>
			<td>Rio Grande</td>
			<td>705047</td>
			<td>Made exclusively for the CAST/T centrifugal casting machine, this crucible is designed with an angled base that slides into the hinged bracket on top of the casting machine. This brings the crucible into perfect alignment with the center of the flask ring to ensure an error-free pour.</td>
		</tr>
		<tr>
			<td>MyWeigh iBalance 300 Digital Scale</td>
			<td>Rio Grande</td>
			<td>116850</td>
			<td>This scale is used to measure the weight of the sacrificial and sprue system for metal which is going to be used for centrifugal casting.</td>
		</tr>
		<tr>
			<td>Rubber bottom - CAST/T Flask Ring Base</td>
			<td>Rio Grande</td>
			<td>705025</td>
			<td>Specially made for the CAST/T centrifugal casting machine, this rubber base accommodates all Table King flask ring styles, creating a secure, airtight seal throughout the investment process. The center post fits either of the wax disc styles for complete versatility.</td>
		</tr>
		<tr>
			<td>Scotch&#174; Colored Duct Tape, 1 7/8&#34; x 20 Yd., Blue</td>
			<td>OfficeMax&#160;</td>
			<td>22353766</td>
			<td>This scotch tape is used to make sure that the gypsum-water mixture fully covers the assembled sacrificial pattern inside the flask by allowing for extra material above the flask height</td>
		</tr>
		<tr>
			<td>Vacuum casting machine - V.I.C. 12 Tabletop Solid- and Perforated-Flask Casting Machine with The Rio Assistant, 110-Volt</td>
			<td>Rio Grande</td>
			<td>70511814</td>
			<td>The V.I.C. 12 casting machine offers all the latest technical innovations for efficient, productive vacuum investing and casting. Designed to meet the demands of medium-sized casting operations, this machine includes a powerful 1/2hp, 5cfm vacuum pump for effective vacuuming and outstanding casting results. The V.I.C. 12 casts small or large flasks. Includes an adapter table that accepts standard solid flasks up to 5&#34; x 7&#34; high and is mounted on rubber feet for stability.</td>
		</tr>
		<tr>
			<td>Furnace for burn out sacrificial pattern -Rio Model 1000 Enameling Kiln with Nine Program Controller</td>
			<td>Rio Grande</td>
			<td>703121</td>
			<td>The Rio enameling kiln features three pre-set firing temperatures for enamels and six that you can define. Use the exclusive Rio controller to set and maintain firing temperatures. Perfect for all types of enameling, including tall pieces. Includes ample space for firing and an easy-latch door that will not jar your enamels when opening and closing. Also suitable for metal clay, glass and ceramics. Galvanized steel case with high-temperature insulating firebrick keeps them cool. Element protected in recessed groove. Includes user instructions.</td>
		</tr>
		<tr>
			<td>Smith Complete Little Torch Acetylene and Oxygen System</td>
			<td>Rio Grande</td>
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			<td>Get everything you need to equip your shop for soldering and brazing. Use Little Torch systems for gold 
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		</tr>
		<tr>
			<td>Heat-Resistant Safety Apron</td>
			<td>Rio Grande</td>
			<td>750160</td>
			<td>The specially designed apron has an 800&#176;F (427&#176;C) temperature resistance. Its reflective finish repels hot metal splashes and helps insulate the wearer from heat.</td>
		</tr>
		<tr>
			<td>Radnor Heat-Resistant Gloves</td>
			<td>Rio Grande</td>
			<td>350050</td>
			<td>These flexible, heat-resistant gloves are ideal for enameling projects, allowing you to grip even small tongs securely. Blue, shoulder-split leather gloves are made of tough cowhide and lined with cotton and foam, and have reinforced thumb wings.</td>
		</tr>
		<tr>
			<td>Platinum Soldering Glasses, #7</td>
			<td>Rio Grande</td>
			<td>113914</td>
			<td>Protect yourself and your employees when soldering platinum. Comfortable glasses feature adjustable earpieces and 52mm IR green polycarbonate #7 lenses. The #7 lens is approved by The Platinum Guild.</td>
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			<td>Economy Light-Duty Flask Tongs</td>
			<td>Rio Grande</td>
			<td>704026</td>
			<td>Constructed of bent steel, these tongs are designed to handle flasks 3-1/2&#34; or less in diameter. The small-angle notches grip smaller flask sizes and the larger, rounded contour area securely holds larger flasks.</td>
		</tr>
		<tr>
			<td>Separating Screen Bucket</td>
			<td>Rio Grande</td>
			<td>201360</td>
			<td>15&#34;-diameter, 11-1/2&#34;-deep</td>
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			<td>Sand blaster - Econoline - 101701CB-A - Free-Standing Cabinets Workspace Width (Inch): 60 Workspace Depth (Inch): 48</td>
			<td>MSC industrial supply Co.&#160;</td>
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			<td>Ree-Standing Cabinets; Workspace Width (Inch): 60; Workspace Depth (Inch): 48; Workspace Height (Inch): 40; Air Requirement: 12 CFM @ 80 psi; Overall Cabinet Width (Inch): 65; Maximum Cabinet Depth (Inch): 86</td>
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			<td>Johnson&#39;s Baby Oil Shea &#38; Cocoa Butter&#160;</td>
			<td>Wal-Mart</td>
			<td>260074132</td>
			<td>This baby&#160; oil is used for removing the residue of the support material for the castable sacrificial pattern using Digital Ultrasonic Cleaner.</td>
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			<td>German 4&#34; Saw Frame and Saw Blade Kit</td>
			<td>Rio Grande</td>
			<td>110112</td>
			<td>Quality, German-made frames are our most popular saw frames, and this frame includes a sampler pack of Rio German saw blades! The adjustable saw frame allows you to achieve the blade tension you want. Throat depth is 102mm (4&#34;). Saw blades have rounded backs that make cutting curves and corners easy and are made from hardened, tempered steel.</td>
		</tr>
	</tbody>
</table>

indirect fabrication of lattice metals with thin sections using centrifugal casting

One of the typical methods to manufacture 3D lattice metals is the direct-metal additive manufacturing (AM) process such as Selective Laser Melting (SLM) and Electron Beam Melting (EBM). In spite of its potential processing capability, the direct AM method has several disadvantages such as high cost, poor surface finish of final products, limitation in material selection, high thermal stress, and anisotropic properties of parts. We propose a cost-effective method to manufacture 3D lattice metals. The objective of this study is to provide a detailed protocol on fabrication of 3D lattice metals having a complex shape and a thin wall thickness; e.g., octet truss made of Al and Cu alloys having a unit cell length of 5 mm and a cell wall thickness of 0.5 mm. An overall experimental procedure is divided into eight sections: (a) 3D printing of sacrificial patterns (b) melt-out of support materials (c) removal of residue of support materials (d) pattern assembly (e) investment (f) burn-out of sacrificial patterns (g) centrifugal casting (h) post-processing for final products. The suggested indirect AM technique provides the potential to manufacture ultra-lightweight lattice metals; e.g., lattice structures with Al alloys. It appears that the process parameters should be properly controlled depending on materials and lattice geometry, observing the final products of octet truss metals by the indirect AM technique.

Using the indirect additive manufacturing described in the protocol section, Al and Cu alloys were used for manufacturing octet truss metals, as shown in Figure 1. The whole casting procedure is summarized in Figure 2. The procedure consists of eight sections: (a) sacrificial pattern printing (b) melting-out of support material (c) removal of residue of support material (d) pattern assembly (e) investment (f) burn-out of sacrificial patterns (g) centrifug...

Watch this Scientific Journal Video about Indirect Fabrication of Lattice Metals with Thin Sections Using Centrifugal Casting at JoVE.com

Indirect Fabrication of Lattice Metals with Thin Sections Using Centrifugal Casting

An indirect additive manufacturing method combining a 3D printing of polymers with a centrifugal casting is outlined for manufacturing 3D octet truss metals (Al and Cu alloys) having a unit cell length of 5 mm with a wall thickness of 0.5 mm.

One of the typical methods to manufacture 3D lattice metals is the direct-metal additive manufacturing (AM) process such as Selective Laser Melting (SLM) ...

The overall goal of this video is to demonstrate the process of filling a cellular microcavity with molten metal for the fabrication of lattice metals by centrifugal casting. This message can help answer key questions such as, how the process parameters, material properties of molten metal, and geometry of lattice mold cavity are correlated with the flow and solidification in rapid microcasting. This technique supplements direct 3D printing massive of metals, in manufacturing lattice metals, and expands the material selection in the design space of lattice metals.Today, I will be demonstrating the procedure with doctoral student Jiwon Mun. In preparation, draw a sacrificial pattern of an octet truss structure with a sprue system using computer-aided design software. This integrated pattern of an octet truss structure with a sprue system gets melted during casting.Using the CAD software, record the volume of the sacrificial pattern to calculate the required metal mass. After printing the acrylic model, proceed with the casting process, which is detailed in the text protocol. The next step is the melting out of the support material.Following this, the residue of support material is further removed. Then, the pattern is assembled. Following its assembly, an investment mixing process is performed.Be sure to remove all lumps in the investment water mixture. Next, is the burnout process. To begin, set the time on the furnace according to the heating and cooling schedule.For a flask of this size, the burnout will take six hours. Now, turn on the furnace and start the burnout schedule. During the burnout, the sacrificial pattern melts and dissociates into a gas.Now, continue with the casting process described in the next two sections. Before beginning, ensure that the centrifugal casting machine's arm spins with an angular velocity of 425 RPM. Find the setting needed for this speed using a tachometer.Select a ceramic crucible to melt each alloy. Using a metal cutter, chop the alloys into 10 millimeter to 20 millimeter pieces. Chop up around 150 grams of each alloy, which in this case are aluminum and copper.Now, weigh out the precise mass of each alloy needed for the lattice design. The pattern cavity must be filled precisely to capacity with molten alloy. Now, get a bucket of water at room temperature ready.30 liters is sufficient. Next, put on flame retardant clothes and put on gloves and goggles. Now, take the plaster mold temporarily out from the furnace.Place it into the flask cradle of the centrifugal casting machine, and balance the arm of the centrifuge. Then, return the plaster mold back into the furnace, and start heating the machine to 482 degrees Celsius. Meanwhile, place the crucible in the crucible holder, and load the chopped alloy into the crucible.Next, set up the acetylene torch. Open the valve of the connected oxygen tank, and maintain the gas pressure near 96.5 kilopascals or 14 PSI. Then, carefully ignite the torch and control the intensity of the flame with the gas pressure.Be very careful. The flame gets up to 1, 200 degrees Celsius. Now, carefully melt the chopped alloy in the crucible until it is completely liquified.Use a carbon rod to stir the alloy and melt it with the neutral part of the torch's flame. The proper melting of the metal is critical, because if the metal is too cool, it will not fill the entire form. But, if it's too hot, the increasing porosity will cause structural issues.Now, take the preheated plaster mold from the furnace, and load it into the flask cradle holding arm next to the crucible with the molten alloy. Close the cover of the machine and let the arm spin for at least three minutes. The machine starts spinning automatically when the cover is closed.About 420 RPM's creates an inlet velocity at the mold cavity of 8.03 meters per second, as calculated by the macroscopic particle dynamics and the angular velocity. After three minutes, cut the power to the centrifugal casting machine. Then, open the cover, and using tongs, remove the plaster mold from the flask cradle.Let the mold cool at room temperature for 15 to 20 minutes, until the color of the alloy returns to that of its solid phase. Then, using tongs, quench the plaster mold in the water bucket for about five minutes. When the mold is near room temperature, it is completely quenched.Now, to obtain the lattice metal inside the mold, just dissolve the mold in water. The Jibsen mold will easily dissolve within two minutes. Post-processing is now possible, such as cleaning by sandblasting, which is described in the text protocol.Be sure to use the described sandblasting pressure as the molds are somewhat fragile, especially the aluminum octet truss which has thin walls. Using the indirect additive manufacturing described in the protocol section, aluminum and copper alloys were used to manufacture octet truss metals. The burnout process was carried out for six hours to melt out the sacrificial pattern.After the centrifugal casting process, the final products were octet truss metals made with aluminum and copper alloys. The molten aluminum alloy fully filled the entire lattice mold cavity without a misrun. On the other hand, the molten copper alloy appeared to have a casting defect caused by premature solidification at the early stage of injection of molten metal at the inlet.After watching this video, you should have a good understanding of the effect of process parameters on filling of molten metal into cellular microcavity, doing indirect fabrication of lattice metals using centrifugal casting. After its development, this technique paved the way for researchers in the field of lattice metals to explore indirect fabrication, by combining 3D printing of polymers with centrifugal casting.

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12.4K vues.  University of North Texas. The overall goal of this video is to demonstrate the process of filling a cellular microcavity with molten metal for the fabrication of lattice metals by centrifugal casting. This message can help answer key questions such as, how the process parameters, material properties of molten metal, and geometry of lattice mold cavity are correlated with the flow and solidification in rapid microcasting. This technique supplements direct 3D printing massive of metals, in manufacturing lattice metals, ...

Vidéo: Indirect Fabrication of Lattice Metals with Thin Sections Using Centrifugal Casting

An indirect additive manufacturing method combining a 3D printing of polymers with a centrifugal casting is outlined for manufacturing 3D octet truss metals (Al and Cu alloys) having a unit cell length of 5 mm with a wall thickness of 0.5...

fabrication of ultra-thin color films with highly absorbing media using oblique angle deposition

Fabrication of Ultra-thin Color Films with Highly Absorbing Media Using Oblique Angle Deposition

We present a detailed method for fabricating ultra-thin color films with improved characteristics for optical coatings. The oblique angle deposition technique using an electron beam evaporator allows improved color tunability and purity. Fabricated films of Ge and Au on Si substrates were analyzed by reflectance measurements and color information...

indirect immunofluorescence on frozen sections of mouse mammary gland

Indirect Immunofluorescence on Frozen Sections of Mouse Mammary Gland

The indirect immunofluorescence protocol described in this article allows the detection and the localization of proteins in the mouse mammary gland. A complete method is given to prepare mammary gland samples, to perform immunohistochemistry, to image the tissue sections by fluorescence microscopy, and to reconstruct...

fabrication of thin film silver/silver chloride electrodes with finely controlled single layer silver chloride

Fabrication of Thin Film Silver/Silver Chloride Electrodes with Finely Controlled Single Layer Silver Chloride

This paper aims to present a method to form smooth and well-controlled films of silver chloride (AgCl) with designated coverage on top of thin film silver...

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Author Spotlight: Advancements in High-Performance Thermoelectric Thin Films Through Radio Frequency Magnetron Sputtering

The manuscript describes a protocol for radio frequency magnetron sputtering of Bi2Te3 and Sb2Te3 thermoelectric thin films on glass substrates, which represents a reliable deposition method that provides a wide range of applications with the potential for further...

Fabrication of Bi2Te3 and Sb2Te3 Thermoelectric Thin Films using Radio Frequency Magnetron Sputtering Technique

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Multi-Scale Modification of Metallic Implants With Pore Gradients, Polyelectrolytes and Their Indirect Monitoring In vivo

In this video, we will demonstrate modification techniques for porous metallic implants to improve their functionality and to control cell migration. Techniques include development of pore gradients to control cell movement in 3D and production of basement membrane mimics to control cell movement in 2-D. Also, a HPLC-based method for monitoring implant integration in-vivo via analysis of blood proteins is...

Multi-Scale Modification of Metallic Implants With Pore Gradients, Polyelectrolytes and Their Indirect Monitoring In vivo

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Determining the Mechanical Strength of Ultra-Fine-Grained Metals

The protocol presented here describes the high-pressure radial diamond-anvil-cell experiments and analyzing the related data, which are essential for obtaining the mechanical strength of the nanomaterials with a significant breakthrough to the traditional...

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Trapping of Micro Particles in Nanoplasmonic Optical Lattice

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vibratome sectioning of whole murine kidney: a technique to generate thin sections of murine kidney

In this video, we demonstrate the vibratome sectioning of a whole mouse kidney to obtain thin slices. These sliced tissue sections can be stored at low temperatures until further downstream...

Vibratome Sectioning of Whole Murine Kidney: A Technique to Generate Thin Sections of Murine Kidney

immunohistochemical staining: a method for obtaining spatial information from thin tissue sections

This video describes the immunohistochemical staining technique to identify dendritic cells from endobronchial...

Immunohistochemical Staining: A Method for Obtaining Spatial Information from Thin Tissue Sections

Immediately apply a thin layer of cyanoacrylate glue to the base of the vibratome specimen plate and use blunt-ended forceps to place the kidney, ureter side down, on the area covered in glue. Gently apply downward pressure to the top of the kidney with the flat edge of the forceps for approximately 10 to 20 seconds to dry the...

detection and recovery of palladium, gold and cobalt metals from the urban mine using novel sensors/adsorbents designated with nanoscale wagon-wheel-shaped pores

Detection and Recovery of Palladium, Gold and Cobalt Metals from the Urban Mine Using Novel Sensors/Adsorbents Designated with Nanoscale Wagon-wheel-shaped Pores

Because of the importance and extensive use of palladium, gold and cobalt metals in high-technology equipment, their recovery and recycling constitute an important industrial challenge. The metal recovery system described herein is a simple, low-cost means for the effective detection, removal, and recovery of these metals from the urban...

preparation of semi-thin leaf sections to understand photosynthesis efficiency based on anatomical differences

Preparation of Semi-Thin Leaf Sections to Understand Photosynthesis Efficiency Based on Anatomical Differences

fabrication of soft pneumatic network actuators with oblique chambers

Fabrication of Soft Pneumatic Network Actuators with Oblique Chambers

Here we present a fabrication method of soft pneumatic network actuators with oblique chambers. The actuators are capable of generating coupled bending and twisting motions, which broadens their application in soft...

chondrogenic differentiation induction of adipose-derived stem cells by centrifugal gravity

Chondrogenic Differentiation Induction of Adipose-derived Stem Cells by Centrifugal Gravity

Mechanical stress can induce the chondrogenic differentiation of stem cells, providing a potential therapeutic approach for the repair of impaired cartilage. We present a protocol to induce the chondrogenic differentiation of adipose-derived stem cells (ASCs) using centrifugal gravity (CG). CG-induced upregulation of SOX9 results in the development of chondrogenic...

immobilization of live caenorhabditis elegans individuals using an ultra-thin polydimethylsiloxane microfluidic chip with water retention

Immobilization of Live Caenorhabditis elegans Individuals Using an Ultra-thin Polydimethylsiloxane Microfluidic Chip with Water Retention

A series of immobilization methods has been established to allow the targeted irradiation of live Caenorhabditis elegans individuals using a recently developed ultra-thin polydimethylsiloxane microfluidic chip with water retention. This novel on-chip immobilization is also adequate for imaging observations. The detailed treatment and application examples of the chip are...

Immobilization of Live Caenorhabditis elegans Individuals Using an Ultra-thin Polydimethylsiloxane Microfluidic Chip with Water Retention

assessing structural traits in triticum aestivum and zea mays for c3 and c4 photosynthetic differentiation using free-hand and semi-thin sections

Author Spotlight: Innovative Approaches to Understanding Plant Structure-Function Relationships for Climate-Resilient Crops

Assessing the anatomical differences between C3 and C4 leaf cross sections helps understand photosynthesis efficiency. This paper describes free-hand and semi-thin leaf cross sections preparation and examination, along with the caveats in the preparation for the crop species Triticum aestivum and Zea...

Assessing Structural Traits in Triticum aestivum and Zea mays for C3 and C4 Photosynthetic Differentiation Using Free-hand and Semi-thin Sections

visualizing surface t-cell receptor dynamics four-dimensionally using lattice light-sheet microscopy

Visualizing Surface T-Cell Receptor Dynamics Four-Dimensionally Using Lattice Light-Sheet Microscopy

The goal of this protocol is to show how to use Lattice Light-Sheet Microscopy to four-dimensionally visualize surface receptor dynamics in live cells. Here T cell receptors on CD4+ primary T cells are...

capillary-based centrifugal microfluidic device for size-controllable formation of monodisperse microdroplets

Capillary-based Centrifugal Microfluidic Device for Size-controllable Formation of Monodisperse Microdroplets

Here, we demonstrate a simple production method for size-controllable, monodisperse, water-in-oil (W/O) microdroplets using a capillary-based centrifugal microfluidic device. This method requires only a small sample volume and enables high-yield production. We expect this method will be useful for rapid biochemical and cellular...

Polycrystalline Silicon Thin-film Solar cells with Plasmonic-enhanced Light-trapping

One of major approaches to cheaper solar cells is reducing the amount of semiconductor material used for their fabrication and making cells thinner. To compensate for lower light absorption such physically thin devices have to incorporate light-trapping which increases their optical thickness. Light scattering by textured surfaces is a common technique but it cannot be universally applied to all solar cell technologies. Some cells, for example those made of evaporated silicon, are planar as produced and they require an alternative light-trapping means suitable for planar devices. Metal nanoparticles formed on planar silicon cell surface and capable of light scattering due to surface plasmon resonance is an effective approach.
The paper presents a fabrication procedure of evaporated polycrystalline silicon solar cells with plasmonic light-trapping and demonstrates how the cell quantum efficiency improves due to presence of metal nanoparticles.
To fabricate the cells a film consisting of alternative boron and phosphorous doped silicon layers is deposited on glass substrate by electron beam evaporation. An Initially amorphous film is crystallised and electronic defects are mitigated by annealing and hydrogen passivation. Metal grid contacts are applied to the layers of opposite polarity to extract electricity generated by the cell. Typically, such a ~2 &mu;m thick cell has a short-circuit current density (Jsc) of 14-16 mA/cm2, which can be increased up to 17-18 mA/cm2 (~25% higher) after application of a simple diffuse back reflector made of a white paint.
To implement plasmonic light-trapping a silver nanoparticle array is formed on the metallised cell silicon surface. A precursor silver film is deposited on the cell by thermal evaporation and annealed at 23&deg;C to form silver nanoparticles. Nanoparticle size and coverage, which affect plasmonic light-scattering, can be tuned for enhanced cell performance by varying the precursor film thickness and its annealing conditions. An optimised nanoparticle array alone results in cell Jsc enhancement of about 28%, similar to the effect of the diffuse reflector. The photocurrent can be further increased by coating the nanoparticles by a low refractive index dielectric, like MgF2, and applying the diffused reflector. The complete plasmonic cell structure comprises the polycrystalline silicon film, a silver nanoparticle array, a layer of MgF2, and a diffuse reflector. The Jsc for such cell is 21-23 mA/cm2, up to 45% higher than Jsc of the original cell without light-trapping or ~25% higher than Jsc for the cell with the diffuse reflector only.
Introduction
Light-trapping in silicon solar cells is commonly achieved via light scattering at textured interfaces. Scattered light travels through a cell at oblique angles for a longer distance and when such angles exceed the critical angle at the cell interfaces the light is permanently trapped in the cell by total internal reflection (Animation 1: Light-trapping). Although this scheme works well for most solar cells, there are developing technologies where ultra-thin Si layers are produced planar (e.g. layer-transfer technologies and epitaxial c-Si layers) 1 and or when such layers are not compatible with textures substrates (e.g. evaporated silicon) 2. For such originally planar Si layer alternative light trapping approaches, such as diffuse white paint reflector 3, silicon plasma texturing 4 or high refractive index nanoparticle reflector 5 have been suggested.
Metal nanoparticles can effectively scatter incident light into a higher refractive index material, like silicon, due to the surface plasmon resonance effect 6. They also can be easily formed on the planar silicon cell surface thus offering a light-trapping approach alternative to texturing. For a nanoparticle located at the air-silicon interface the scattered light fraction coupled into silicon exceeds 95% and a large faction of that light is scattered at angles above critical providing nearly ideal light-trapping condition (Animation 2: Plasmons on NP). The resonance can be tuned to the wavelength region, which is most important for a particular cell material and design, by varying the nanoparticle average size, surface coverage and local dielectric environment 6,7. Theoretical design principles of plasmonic nanoparticle solar cells have been suggested 8. In practice, Ag nanoparticle array is an ideal light-trapping partner for poly-Si thin-film solar cells because most of these design principle are naturally met. The simplest way of forming nanoparticles by thermal annealing of a thin precursor Ag film results in a random array with a relatively wide size and shape distribution, which is particularly suitable for light-trapping because such an array has a wide resonance peak, covering the wavelength range of 700-900 nm, important for poly-Si solar cell performance. The nanoparticle array can only be located on the rear poly-Si cell surface thus avoiding destructive interference between incident and scattered light which occurs for front-located nanoparticles 9. Moreover, poly-Si thin-film cells do not requires a passivating layer and the flat base-shaped nanoparticles (that naturally result from thermal annealing of a metal film) can be directly placed on silicon further increases plasmonic scattering efficiency due to surface plasmon-polariton resonance 10.
The cell with the plasmonic nanoparticle array as described above can have a photocurrent about 28% higher than the original cell. However, the array still transmits a significant amount of light which escapes through the rear of the cell and does not contribute into the current. This loss can be mitigated by adding a rear reflector to allow catching transmitted light and re-directing it back to the cell. Providing sufficient distance between the reflector and the nanoparticles (a few hundred nanometers) the reflected light will then experience one more plasmonic scattering event while passing through the nanoparticle array on re-entering the cell and the reflector itself can be made diffuse - both effects further facilitating light scattering and hence light-trapping. Importantly, the Ag nanoparticles have to be encapsulated with an inert and low refractive index dielectric, like MgF2 or SiO2, from the rear reflector to avoid mechanical and chemical damage 7. Low refractive index for this cladding layer is required to maintain a high coupling fraction into silicon and larger scattering angles, which are ensured by the high optical contrast between the media on both sides of the nanoparticle, silicon and dielectric 6. The photocurrent of the plasmonic cell with the diffuse rear reflector can be up to 45% higher than the current of the original cell or up to 25% higher than the current of an equivalent cell with the diffuse reflector only.

Polycrystalline silicon thin-film solar cells on glass are fabricated by deposition of boron and phosphorous doped silicon layers followed by crystallisation, defect passivation and metallisation. Plasmonic light-trapping is introduced by forming Ag nanoparticles on the silicon cell surface capped with a diffused reflector resulting in ~45% photocurrent enhancement.

One of major approaches to cheaper solar cells is reducing the amount of semiconductor material used for their fabrication and making cells thinner. To ...

Developing low-cost, efficient processes for recovering and recycling palladium, gold and cobalt metals from urban mine remains a significant challenge in industrialized countries. Here, the development of optical mesosensors/adsorbents (MSAs) for efficient recognition and selective recovery of Pd(II), Au(III), and Co(II) from urban mine was achieved. A simple, general method for preparing MSAs based on using high-order mesoporous monolithic scaffolds was described. Hierarchical cubic Ia3d wagon-wheel-shaped MSAs were fabricated by anchoring chelating agents (colorants) into three-dimensional pores and micrometric particle surfaces of the mesoporous monolithic scaffolds. Findings show, for the first time, evidence of controlled optical recognition of Pd(II), Au(III), and Co(II) ions and a highly selective system for recovery of Pd(II) ions (up to ~95%) in ores and industrial wastes. Furthermore, the controlled assessment processes described herein involve evaluation of intrinsic properties (e.g., visual signal change, long-term stability, adsorption efficiency, extraordinary sensitivity, selectivity, and reusability); thus, expensive, sophisticated instruments are not required. Results show evidence that MSAs will attract worldwide attention as a promising technological means of recovering and recycling palladium, gold and cobalt metals.

Because of the importance and extensive use of palladium, gold and cobalt metals in high-technology equipment, their recovery and recycling constitute an important industrial challenge. The metal recovery system described herein is a simple, low-cost means for the effective detection, removal, and recovery of these metals from the urban mine.

Developing low-cost, efficient processes for recovering and recycling palladium, gold and cobalt metals from urban mine remains a significant challenge in ...

Speciation and Bioavailability Measurements of Environmental Plutonium Using Diffusion in Thin Films

The biological uptake of plutonium (Pu) in aquatic ecosystems is of particular concern since it is an alpha-particle emitter with long half-life which can potentially contribute to the exposure of biota and humans. The diffusive gradients in thin films technique is introduced here for in-situ measurements of Pu bioavailability and speciation. A diffusion cell constructed for laboratory experiments with Pu and the newly developed protocol make it possible to simulate the environmental behavior of Pu in model solutions of various chemical compositions. Adjustment of the oxidation states to Pu(IV) and Pu(V) described in this protocol is essential in order to investigate the complex redox chemistry of plutonium in the environment. The calibration of this technique and the results obtained in the laboratory experiments enable to develop a specific DGT device for in-situ Pu measurements in freshwaters. Accelerator-based mass-spectrometry measurements of Pu accumulated by DGTs in a karst spring allowed determining the bioavailability of Pu in a mineral freshwater environment. Application of this protocol for Pu measurements using DGT devices has a large potential to improve our understanding of the speciation and the biological transfer of Pu in aquatic ecosystems.

The technique of diffusive gradients in thin films (DGT) is proposed for speciation studies of plutonium. This protocol describes diffusion experiments probing the behavior of Pu(IV) and Pu(V) in presence of organic matter. DGTs deployed in a karstic spring allow assessment of the bioavailability of Pu.

The biological uptake of plutonium (Pu) in aquatic ecosystems is of particular concern since it is an alpha-particle emitter with long half-life which can ...

A Fabrication Method for Highly Stretchable Conductors with Silver Nanowires

Stretchable electronics are identified as a key technology for electronic applications in the next generation. One of the challenges in fabrication of stretchable electronic devices is the preparation of stretchable conductors with great mechanical stability. In this study, we developed a simple fabrication method to chemically solder the contact points between silver nanowire (AgNW) networks. AgNW nanomesh was first deposited on a glass slide via spray coating method. A reactive ink composed of silver nanoparticle (AgNPs) precursors was applied over the spray coated AgNW thin films. After heating for 40 min, AgNPs were preferentially generated over the nanowire junctions to solder the AgNW nanomesh, and reinforced the conducting network. The chemically modified AgNW thin film was then transferred to polyurethane (PU) substrates by casting method. The soldered AgNW thin films on PU exhibited no obvious change in electrical conductivity under stretching or rolling process with elongation strains up to 120%.

A simple synthesis method is used to chemically solder silver nanowire thin film to fabricate highly stretchable and conductive metal conductors.

Stretchable electronics are identified as a key technology for electronic applications in the next generation. One of the challenges in fabrication of ...

Here, we demonstrate a simple method for the rapid production of size-controllable, monodisperse, W/O microdroplets using a capillary-based centrifugal microfluidic device. W/O microdroplets have recently been used in powerful methods that enable miniaturized chemical experiments. Therefore, developing a versatile method to yield monodisperse W/O microdroplets is needed. We have developed a method for generating monodisperse W/O microdroplets based on a capillary-based centrifugal axisymmetric co-flowing microfluidic device. We succeeded in controlling the size of microdroplets by adjusting the capillary orifice. Our method requires equipment that is easier-to-use than with other microfluidic techniques, requires only a small volume (0.1-1 &#181;l) of sample solution for encapsulation, and enables the production of hundreds of thousands number of W/O microdroplets per second. We expect this method will assist biological studies that require precious biological samples by conserving the volume of the samples for rapid quantitative analysis biochemical and biological studies.

Here, we demonstrate a simple production method for size-controllable, monodisperse, water-in-oil (W/O) microdroplets using a capillary-based centrifugal microfluidic device. This method requires only a small sample volume and enables high-yield production. We expect this method will be useful for rapid biochemical and cellular analyses.

Here, we demonstrate a simple method for the rapid production of size-controllable, monodisperse, W/O microdroplets using a capillary-based centrifugal ...

Fabrication of Periodic Gold Nanocup Arrays Using Colloidal Lithography

Within recent years, the field of plasmonics has exploded as researchers have demonstrated exciting applications related to chemical and optical sensing in combination with new nanofabrication techniques. A plasmon is a quantum of charge density oscillation that lends nanoscale metals such as gold and silver unique optical properties. In particular, gold and silver nanoparticles exhibit localized surface plasmon resonances-collective charge density oscillations on the surface of the nanoparticle-in the visible spectrum. Here, we focus on the fabrication of periodic arrays of anisotropic plasmonic nanostructures. These half-shell (or nanocup) structures can exhibit additional unique light-bending and polarization-dependent optical properties that simple isotropic nanostructures cannot. Researchers are interested in the fabrication of periodic arrays of nanocups for a wide variety of applications such as low-cost optical devices, surface-enhanced Raman scattering, and tamper indication. We present a scalable technique based on colloidal lithography in which it is possible to easily fabricate large periodic arrays of nanocups using spin-coating and self-assembled commercially available polymeric nanospheres. Electron microscopy and optical spectroscopy from the visible to near-infrared (near-IR) was performed to confirm successful nanocup fabrication. We conclude with a demonstration of the transfer of nanocups to a flexible, conformal adhesive film.

We demonstrate the fabrication of periodic gold nanocup arrays using colloidal lithographic techniques and discuss the importance of nanoplasmonic films.

Within recent years, the field of plasmonics has exploded as researchers have demonstrated exciting applications related to chemical and optical sensing ...

Ultra-thin film structures have been studied extensively for use as optical coatings, but performance and fabrication challenges remain.&#160; We present an advanced method for fabricating ultra-thin color films with improved characteristics. The proposed process addresses several fabrication issues, including large area processing. Specifically, the protocol describes a process for fabricating ultra-thin color films using an electron beam evaporator for oblique angle deposition of germanium (Ge) and gold (Au) on silicon (Si) substrates.&#160; Film porosity produced by the oblique angle deposition induces color changes in the ultra-thin film. The degree of color change depends on factors such as deposition angle and film thickness. Fabricated samples of the ultra-thin color films showed improved color tunability and color purity. In addition, the measured reflectance of the fabricated samples was converted into chromatic values and analyzed in terms of color. Our ultra-thin film fabricating method is expected to be used for various ultra-thin film applications such as flexible color electrodes, thin film solar cells, and optical filters. Also, the process developed here for analyzing the color of the fabricated samples is broadly useful for studying various color structures.

We present a detailed method for fabricating ultra-thin color films with improved characteristics for optical coatings. The oblique angle deposition technique using an electron beam evaporator allows improved color tunability and purity. Fabricated films of Ge and Au on Si substrates were analyzed by reflectance measurements and color information conversion.

Ultra-thin film structures have been studied extensively for use as optical coatings, but performance and fabrication challenges remain.&#160; We present ...

Processing of Bulk Nanocrystalline Metals at the US Army Research Laboratory

Given their potential for significant property improvements relative to their large grained counterparts, much work has been devoted to the continued development of nanocrystalline metals. Despite these efforts, the transition of these materials from the lab bench to actual applications has been blocked by the inability to produce large scale parts that retain the desired nanocrystalline microstructures. Following the development of a method proven to stabilize the nanosized grain structure to temperatures approaching that of the melting point for the given metal, the US Army Research Laboratory (ARL) has progressed to the next stage in the development of these materials - namely the production of large scale parts suitable for testing and evaluation in a range of relevant test environments. This report provides a broad overview of the ongoing efforts in the processing, characterization, and consolidation of these materials at ARL. In particular, focus is placed on the methodology used for producing the nanocrystalline metal powders, in both small and large-scale amounts, that are at the center of ongoing research efforts.

This paper provides a brief overview of the ongoing efforts at the Army Research Laboratory on the processing of bulk nanocrystalline metals with an emphasis on the methodologies used for the production of the novel metal powders.

Given their potential for significant property improvements relative to their large grained counterparts, much work has been devoted to the continued ...

Soft pneumatic network actuators have become one of the most promising actuation devices in soft robotics which benefits from their large bending deformation and low input. However, their monotonous bending motion form in two-dimensional (2-D) space keeps them away from wide applications. This paper presents a detailed fabrication method of soft pneumatic network actuators with oblique chambers, to explore their motions in three-dimensional (3-D) space. The design of oblique chambers enables actuators with tunable coupled bending and twisting capabilities, which gives them the possibility to move dexterously in flexible manipulators, to become biologically inspired robots and medical devices. The fabrication process is based on the molding method, including the silicone elastomer preparation, chamber and base parts fabrication, actuator assembly, tubing connections, checks for leaks, and actuator repair. The fabrication method guarantees the rapid manufacturing of a series of actuators with only a few modifications in the molds. The test results show the high quality of the actuators and their prominent bending and twisting capabilities. Experiments of the gripper demonstrate the advantages of the development in adapting to objects with different diameters and providing sufficient friction.

Here we present a fabrication method of soft pneumatic network actuators with oblique chambers. The actuators are capable of generating coupled bending and twisting motions, which broadens their application in soft robotics.

Soft pneumatic network actuators have become one of the most promising actuation devices in soft robotics which benefits from their large bending ...

Fabrication of Microscope Stage for Vertical Observation with Temperature Control Function

Samples are usually placed onto a horizontal microscope stage for microscopic observation. However, to observe the influence of gravity on a sample or study afloat behavior, it is necessary to make the microscope stage vertical. To accomplish this, a sideways inverted microscope tilted by 90&#176; has been devised. To observe samples with this microscope, sample containers such as Petri dishes or glass slides must be secured to the stage vertically. A device that can secure sample containers in place on a vertical microscope stage has been developed and is described here. Attachment of this device to the stage allows observation of sample dynamics in the vertical plane. The ability to regulate temperature using a silicone rubber heater also permits observation of temperature-dependent sample behaviors. Furthermore, the temperature data is transferred to an internet server. Temperature settings and log monitoring can be controlled remotely from a PC or smartphone.

Presented here is a protocol using a temperature-controlled microscope stage that allows a sample container to be mounted on a vertical microscope.

Samples are usually placed onto a horizontal microscope stage for microscopic observation. However, to observe the influence of gravity on a sample or ...