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SUNY Geneseo

2 ARTICLES PUBLISHED IN JoVE

Chemistry

Exfoliation and Analysis of Large-area, Air-Sensitive Two-Dimensional Materials

Josh P. Thompson¹, M. Hasan Doha¹, Peter Murphy^1,2, Jin Hu^1,3, Hugh O.H. Churchill^1,3

¹Department of Physics, University of Arkansas, ²Department of Physics, SUNY Geneseo, ³Institute for Nanoscale Science and Engineering, University of Arkansas

A method for exfoliating large thin flakes of air sensitive two-dimensional materials and safely transporting them for analysis outside of a glovebox is presented.

Biochemistry

The Automated Crystallography Pipelines at the EMBL HTX Facility in Grenoble

Irina Cornaciu^1,2, Raphael Bourgeas¹, Guillaume Hoffmann¹, Florine Dupeux^1,3, Anne-Sophie Humm¹, Vincent Mariaule¹, Andrea Pica^1,2, Damien Clavel^1,2, Gael Seroul^1,2, Peter Murphy¹, José Antonio Márquez^1,2

¹European Molecular Biology Laboratory, ²ALPX S.A.S., ³Institut de Biologie Structurale

Here, we describe how to use the automated macromolecular crystallography pipelines for protein-to-structure, rapid ligand-protein complex analysis and large-scale fragment screening based on the CrystalDirect technology at the HTX Laboratory in EMBL Grenoble.