Microwave-assisted Denitration of 2-Azido-1-nitrate Esters and Trichloroacetimide Formation
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Results: Microwave-assisted Conversion of Anomeric Nitrate Esters to Trichloroacetimidates
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Conclusion
Transcripción
The overall goal of this experiment is to use a one-pot procedure to synthesize trichloroacetimidates directly from azido nitrate-esters with minimal workup in purification. This method poses clear advantages for the synthesis of trichloroacetimid
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A 2-azido-1-nitrate-ester can be converted to the corresponding 2-azido-1-trichloroacetimidate in a one-pot procedure. The goal of the manuscript is to demonstrate utility of the microwave reactor in carbohydrate synthesis.