Chapter 9
Method Development and Sampling Techniques
Разработка аналитических методов
An analytical methodology can be divided into four sequential steps: technique, method, procedure, and protocol. A technique is a scientific principle ...
Контроль качества
Quality control is one of the three cyclical quality assurance activities that help keep a system under statistical control. Typical quality control ...
Гарантия качества
Quality assurance is the overarching term used to describe the activities employed to ensure the proper performance of a system. These activities can be ...
Проверка данных
Method validation is a crucial process in analytical chemistry designed to confirm that a given method consistently produces reliable and high-quality ...
Качественный анализ
Qualitative analysis is the process of identifying elements, ions, or compounds in an unknown sample. It is the first and most fundamental type of ...
Количественный анализ
Quantitative analysis is a technique for measuring the amount of specific constituents in a sample. When the sample's composition is unknown, ...
Калибровка прибора
Instrument calibration is essential for ensuring that instruments produce accurate and consistent results. It is vital in manufacturing, healthcare, ...
Калибровка стеклянной посуды
Accurate calibration of glassware, such as volumetric flasks, pipettes, and burettes, is essential to ensure accurate measurements in the analytical ...
Типовые решения
Standard solutions refer to solutions with a precisely known concentration or composition. A primary standard is a highly pure, high molar mass, stable ...
Пустые решения
A blank solution is a solution that does not contain the analyte, or the substance of interest being tested or measured. It is typically prepared using ...
Методы отбора проб: обзор
A sample refers to a smaller subset representative of a larger population. In analytical chemistry, studying or analyzing an entire population is often ...
Методы отбора проб: типы проб
Sampling materials are classified into three main types: solid, liquid, and gas.
Solid samples include a variety of substances, such as sediments from ...
Планы отбора проб
Sampling is a crucial step in analytical chemistry, allowing researchers to collect representative data from a large population. Common sampling methods ...
Подготовка образцов к анализу: обзор
Sample preparation is an essential step in the analytical process. It involves preparing a sample so that it can be analyzed accurately. The goal is to ...
Подготовка образцов к анализу: передовые методики
Accurate analysis of complex samples often requires advanced preparation techniques to achieve reliable and reproducible results. Samples containing ...
Работа с образцами
Transportation of samples from the collection point to the laboratory, as well as storage and preservation techniques, are crucial for maintaining sample ...
Загрязнения и ошибки
Effective sample preparation is crucial for accurate and reliable laboratory analysis. During this process, two significant sources of error can arise: ...
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