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One-pot Microwave-assisted Conversion of Anomeric Nitrate-esters to Trichloroacetimidates

DOI :

10.3791/56610-v

January 15th, 2018

January 15th, 2018

7,320 Views

1Department of Chemistry, Vanderbilt University, 2Institute of Chemical-Biology, Vanderbilt University

A 2-azido-1-nitrate-ester can be converted to the corresponding 2-azido-1-trichloroacetimidate in a one-pot procedure. The goal of the manuscript is to demonstrate utility of the microwave reactor in carbohydrate synthesis.

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