Reaction in a 7.5-mL Vial (Purging Conditions - Air Excluded)
3:34
Reaction in a 35-mL Pressure Tube (Air Not Excluded)
5:08
Results: Representative 1H NMR Reaction Analyses
5:46
Conclusion
Transcript
This method can help address a key challenge in the field of synthetic organic chemistry, namely how to perform reactions under carbon dioxide atmosphere quickly and easily. The main advantage of this technique is that it allows reactions to be pe
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Here we present a protocol for performing reactions in simple reaction vessels under low-to-moderate pressures of CO2. The reactions can be performed in a variety of vessels simply by administering the carbon dioxide in the form of dry ice, without the need for costly or elaborate equipment or set-ups.