Name: pool-boiling heat-transfer enhancement on cylindrical surfaces with hybrid wettable patterns
Uploaded: 2017-04-10T14:00:00.000+00:00
Duration: 7 min 32 s
Description: Watch this Scientific Journal Video about Pool-Boiling Heat-Transfer Enhancement on Cylindrical Surfaces with Hybrid Wettable Patterns at JoVE.com

The authors gratefully acknowledge funding support from the Ministry of Science and Technology, MOST (project numbers: MOST 104-2218-E-002 -004, MOST 105-2218-E-002-019, MOST 105-2221-E-002 -107 -MY3, MOST 102-2221-E-002 -133 -MY3, and MOST 102-2221-E-002 -088 -MY3).

1. Preparazione delle superfici modificate <ol><li> Lucidare manualmente il pezzo di prova (cilindro cavo in rame con una lunghezza di 40 mm (l), un diametro esterno di 25 mm (d o), ed un diametro interno di 18 mm (d i)) per 15 minuti usando uno smeriglio N. 2.000 carta. Pulire la superficie lucidata da risciacquo con acetone mediante acqua deionizzata. </li><li> Si dispone la provetta lucidata in un forno per 2 ore a una temperatura costante di 120 ° C. </li><li> Preparare una soluzione di nanoparticelle superidrofilia SiO 2 procede come segue. <ol><li> Preparare la soluzione A miscelando 1: 4 rapporti molari di silano tetraethoxy e acqua deionizzata. Aggiungere 2 gocce di 37% HCl concentrato alla soluzione A e mescolare per 2 ore. </li><li> Preparare la soluzione B miscelando un rapporto 1: 3 moli di etanolo e acqua deionizzata. </li><li> Mescolare 1 mL di soluzione A e 80 mL di soluzione B e agitare per 2 ore. </li><li> Aggiungere 32 g di SiO 2 nanoparticelle (diametro 40 nm) per la solu preparatozione e mescolare per 1 ora. </li></ol></li><li> Immergere la provetta nella soluzione preparata utilizzando l&#39;apparecchiatura dip-coating ad una velocità di 5 mm / min. Tenere il pezzo di prova rivestito in un forno a 120 ° C per 1 ora. </li><li> Preparare 2, 4, e 8 modelli ibridi interlined con diversi orientamenti lungo la direzione assiale (come mostrato in figura 1) utilizzando la seguente procedura. <ol><li> Mascherare l&#39;area da non rivestito utilizzando il nastro isolante secondo il numero richiesto di interlining con il giusto orientamento (per la superficie 2-interlinea in un orientamento 0 °, regolare interlining al centro e la zona superidrofilia (superficie da rivestire) sulla il lato superiore. D&#39;altra parte, per l&#39;orientamento 90 °, regolare un&#39;interlinea nella parte superiore e un altro in basso e per l&#39;orientamento 180 °, regolare zona superidrofilia in basso e le interlining al centro. Analogamente, regolare la posizione dei 4, 8 superfici interlined con il differente orientation come mostrato in Figura 1). </li><li> Immergere la provetta mascherato nella soluzione preparata utilizzando un apparecchio di rivestimento a immersione, immersione ad una velocità di immersione elevato e luogo ad una lenta velocità di 5 mm / min. Tenere il pezzo di prova rivestito in un forno a 120 ° C per 1 ora. </li><li> Rimuovere il nastro isolante dalla maschera per ottenere il numero necessario di interlining con il corretto orientamento. </li></ol></li></ol><img alt="Figura 1" src="/files/ftp_upload/55387/55387fig1.jpg" /> Figura 1. selezione di vari interlined superfici. (a) Schema di varie superfici interlined con diversi orientamenti. Il rapporto di una superficie di rame piana ed una superficie superidrofilia area è 1: 1 in tutte le condizioni. criteri di selezione (b) di orientamento. (c) vista isometrica del 2 interlinea 0 ° angolo di superficie orientata. Orientamento viene selezionato come l&#39;angolo tra la linea di base e di rivestimentomezzeria del primo modello idrofilo dal lato superiore e si misura in senso orario. <a href="http://ecsource.jove.com/files/ftp_upload/55387/55387fig1large.jpg" target="_blank">Si prega di cliccare qui per vedere una versione più grande di questa figura.</a> 2. Procedura sperimentale <ol><li> Utilizzando il nastro isolante, fissare un tubo di vetro in ogni base circolare della provetta rivestita. </li><li> Orizzontalmente risolvere questo assieme alla camera 140- x 140- x 160 mm (come mostrato in figura 2) con pasta di silicone secondo la posizione richiesta di interlining. </li><li> Posizionare un 550-W, diametro 18 mm, e 40 mm lungo riscaldatore a cartuccia con una pellicola sottile di pasta termica sulla superficie circonferenziale nel foro della provetta. </li><li> Collegare il riscaldatore a cartuccia ad un&#39;unità di alimentazione a corrente continua (DC). </li><li> Posto T-termocoppie nelle 8 fori 1 mm equidistanziate, con profondità alternati su 5 e 7 mm, come mostrato in figura3 Collegarli al data logger. </li><li> Inserire e fissare termoresistenze (RTD), un condensatore a riflusso, e un riscaldatore ausiliario negli spazi previsti sul coperchio superiore. fissarli sopra la camera di ebollizione. </li><li> Riempire 1.400 ml di acqua DI nella camera piscina bollente. </li><li> Collegare il condensatore a riflusso per una camera di raffreddamento che viene mantenuta a 5 ° C. </li><li> Prima dell&#39;esperimento, l&#39;ebollizione l&#39;acqua DI nella camera piscina-bollente per 30 minuti usando il riscaldatore ausiliario. </li><li> Mantenere l&#39;acqua DI nella condizione di ebollizione satura utilizzando il riscaldatore ausiliario. Successivamente, accendere l&#39;alimentazione e fornire una corrente iniziale di 0,1 A. </li><li> Attendere per 2 minuti al fine di raggiungere uno stato stazionario. Quindi, aumentare la corrente elettrica con incrementi di 0,3 A. </li><li> Registrare la temperatura a ciascun ingresso di potenza utilizzando il datalogger. Continuare l&#39;esperimento fino al raggiungimento di una corrente massima di 4 A. Nel frattempo, registrare la dinamica bolla f<html> o ciascun ingresso di alimentazione utilizzando una telecamera CCD posta di fronte alla piscina bollente camera, che si concentra sul provino. </li></ol><img alt="figura 2" src="/files/ftp_upload/55387/55387fig2.jpg" /> Figura 2. Schema della Camera Pool-bollente. tubi di vetro sono collegati ad entrambi i lati del cilindro cavo in rame con pasta di silicone. Questo è fissato alla camera piscina ebollizione con pasta di silicone. <a href="http://ecsource.jove.com/files/ftp_upload/55387/55387fig2large.jpg" target="_blank">Si prega di cliccare qui per vedere una versione più grande di questa figura.</a> <img alt="Figura 3" src="/files/ftp_upload/55387/55387fig3.jpg" /> Figura 3. Posizionamento termocoppia. 8 termocoppie sono collocati all&#39;interno dei fori 1 mm di diametro circonferenzialmente collocati provetta ad un diametro di 20 mm. Le profondità di fori del diametro di 1 mm alternativi sono fissati a 5 mm e 7 mm./files/ftp_upload/55387/55387fig3large.jpg&quot; target = &#39;_ blank&#39;&gt; Clicca qui per vedere una versione più grande di questa figura. 3. Riduzione dei dati <ol><li> Calcolare l&#39;apporto di calore (Q) utilizzando la seguente equazione 19 Q = I V (1) NOTA: I e V sono la corrente di ingresso in ampere e la tensione in volt, rispettivamente. </li><li> Valutare la perdita di calore (perdita Q) dalle due superfici laterali utilizzando la formula 19: <img alt="equazione 2" src="/files/ftp_upload/55387/55387eq2.jpg" /> (2) NOTA: k è la conducibilità termica del rame; T 7 mm e T 5 mm non sono i valori medi della temperatura a profondità di 7 mm e 5 mm, rispettivamente; Ax (2 mm) è la differenza tra le profondità; e <img alt="equazione 2B" src="/files/ftp_upload/55387/55387eq2b.jpg" /> è l&#39;area della sezione trasversale del test p<html> IECE. </li><li> Determinare il flusso di calore (q &#39;&#39;) utilizzando la seguente formula 19: <img alt="equazione 3" src="/files/ftp_upload/55387/55387eq3.jpg" /> (3) NOTA: A = π d o l è la zona circonferenziale della provetta. </li><li> Calcolare il surriscaldamento parete (usando la seguente equazione 19: <img alt="equazione 4" src="/files/ftp_upload/55387/55387eq4.jpg" /> (4) NOTA: T m è la media di T 7 mm e T 5 mm, è la lunghezza della provetta, r o (12.5 mm) raggio esterno della provetta, r m (10 mm) raggio della provetta alla misurazione fori, e T sAT è la temperatura di saturazione di acqua dI, come illustrato nella figura 4. </li><li> Calcolare l&#39;HTC (α) utilizzando la seguente formula 19: PLOAD / 55387 / 55387eq5.jpg&quot;/&gt; (5) </li></ol><img alt="Figura 4" src="/files/ftp_upload/55387/55387fig4.jpg" /> Figura 4. Schema di Wall Analisi temperatura. temperatura di parete è calcolato utilizzando la media temperatura misurata e conosciuto cilindrica resistenza termica. <a href="http://ecsource.jove.com/files/ftp_upload/55387/55387fig4large.jpg" target="_blank">Si prega di cliccare qui per vedere una versione più grande di questa figura.</a>

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The authors declare that they have no competing financial interests.

The main goal of this investigation was to develop a pool-boiling heat sink for high heat dissipation applications, such as nuclear reactors, boilers, and heat pipes, by introducing the hybrid wettable surface, as described in the protocol section. These surfaces can produce better pool-boiling performances than homogeneous wettable surfaces (hydrophilic and hydrophobic). The improvement in the boiling heat-transfer performance is due to an increase in active nucleation sites and the easy detachment of the formed bubbles...

Un sistema di calore elevato flusso di sostentamento che fornisce raffreddamento nell&#39;intervallo 10-10 5 W / cm 2 è richiesta nei settori emergenti dell&#39;elettronica, difesa, avionica e sviluppo dispositivo nucleare. raffreddamento convenzionale con aria è sufficiente per queste applicazioni a causa del coefficiente di scambio termico basso (HTC) per entrambe le condizioni di libero e convezione forzata. Le tecniche di raffreddamento cambiamento basate fase, come piscina ebollizione e il flusso bollente, sono abbastanza buono per rimuovere elevati flussi di calore dell&#39;ordine di 10 - 1,000 W / cm 2 1. Poiché il processo di trasferimento di calore a due fasi è isotermico, la temperatura del dispositivo raffreddato è quasi costante sulla sua superficie. A causa della variazione trascurabile della temperatura lungo la superficie, lo shock termico del dispositivo può essere eliminato. Tuttavia, il principale parametro limitante in ebollizione trasferimento di calore è il flusso di calore critico (CHF), che causa un aumento anomalo della temperatura 2 </sup&gt;. Negli ultimi decenni, vasta ricerca è stata effettuata per migliorare la CHF mediante modificazione superficiale, nanofluidi, e rivestimenti di superficie 3, 4, 5, 6, 7, 8, 9, 10, 11. Tra i vari metodi, rivestimenti di superficie si trovano ad essere il metodo migliore per migliorare il CHF causa del notevole aumento della superficie. Rivestimenti superficiali generalmente aumenta il trasferimento di calore con l&#39;azione della pinna, effetti porosità e superficie bagnabilità 12. bagnabilità della superficie gioca un ruolo significativo nella bollente scambio termico. Precedenti studi mostrano che in condizioni di flusso termico inferiore, la superficie idrofoba mostra meglio HTC dovuta ai primi nucleazione. Tuttavia, aflusso di calore superiore, il distacco delle bolle formate è lento a causa della bassa affinità di acqua verso la superficie. Questo porta a bolla coalescenza e si traduce in una minore CHF 3. D&#39;altro canto, una superficie idrofila produce una maggiore CHF, a causa del distacco rapido delle bolle formate, ma dà un HTC inferiore a flussi di calore bassa, a causa del ritardo nella bolla nucleazione 13. Le strutture ibride mostrano migliora notevolmente bollente scambio termico per tutti i flussi di calore per l&#39;effetto combinato di idrofobicità e idrofilia 14, 15, 16. Hsu et al. prodotta superficie bagnabile eterogenea rivestendo superidrofilia Si nanoparticelle su una superficie di rame mascherato. Hanno raggiunto differenti rapporti bagnabilità variando il tempo di rivestimento. L&#39;insorgenza di ebollizione si è verificato in precedenza sulle superfici eterogenee rispetto alla hsuperficie omogenea, che ha ridotto sostanzialmente la parete Surriscaldamento 17. Jo et al. condotto studi termodistributori nucleata bollente su superfici bagnanti idrofile, idrofobe, ed eterogenei. La superficie bagnatura eterogenea è stata composta da punti modellati idrofobe sulla superficie idrofila. Hanno ottenuto HTCs superiore e la stessa CHF per la superficie eterogenea rispetto alla superficie idrofila. Un miglioramento bollente termovettore dipende direttamente dal numero di punti sulla superficie e dalle condizioni di ebollizione 18. In questo studio, assiali modelli bagnabili ibridi sono stati prodotti su una superficie di rame cilindrica con la tecnica dip coating. Pool-bollente studi scambio termico sono stati condotti per determinare gli effetti del numero di interlining e dell&#39;orientamento del modello bagnabile ibrido. Ebollizione flusso di calore, HTC e dinamiche bolla sono stati analizzati per i substrati tutti rivestiti e tiri rispetto al substrato di rame.

<table><tbody><tr><td>Deionized water</td><td></td><td></td><td></td></tr><tr><td>Silica nanopowder,40 nm</td><td>UniRegion Bio-Tech</td><td>60676860</td><td></td></tr><tr><td>Ethanol</td><td>ECHO Chemical co. Ltd</td><td>64175</td><td></td></tr><tr><td>Hydrochloric acid</td><td>SHOWA Chemical co. Ltd.</td><td>7647010</td><td></td></tr><tr><td>Tetraethoxysilane</td><td>SHOWA Chemical co. Ltd.</td><td>78104</td><td></td></tr><tr><td>Acetone</td><td>UNI-ONWARD CORP.</td><td>67641</td><td></td></tr><tr><td>Cartridge Heater</td><td>Chung Shun Heater &amp;amp; Instrument Co, Ltd.</td><td></td><td></td></tr><tr><td>Pyrex glass&amp;nbsp;</td><td>Automotive Glass service , Taiwan</td><td></td><td></td></tr><tr><td>Ordinary toughened glass</td><td>Automotive Glass service , Taiwan</td><td></td><td></td></tr><tr><td>Thermal paste</td><td>Electrolube</td><td>EG-30&amp;nbsp;</td><td></td></tr><tr><td>Insulation Tape</td><td>Chuan Chi Trading Co. Ltd</td><td>Kapton Tape</td><td></td></tr><tr><td>Sandpaper</td><td>Chuan Chi Trading Co. Ltd</td><td>#2000</td><td></td></tr><tr><td>Heating furnace</td><td>Chung Chuan</td><td>Hong Sen HS-101</td><td></td></tr><tr><td>Electronic scales</td><td>A&amp;amp;D co. Ltd</td><td>GX400</td><td></td></tr><tr><td>Ultrasonic cleaner</td><td>Bransonic</td><td>Bransonic 3510</td><td></td></tr><tr><td>Magnet stirrer</td><td>Yellow line</td><td>MST D S1</td><td></td></tr><tr><td>Data logger&amp;nbsp;</td><td>Yokogawa</td><td>MX-100</td><td></td></tr><tr><td>CCD camera</td><td>JVC</td><td>LY35862-001A</td><td></td></tr><tr><td>Silicon paste</td><td>Permatex</td><td>599BR</td><td></td></tr><tr><td>Power supply</td><td>Gwinstek</td><td>GPR-20H50D</td><td></td></tr><tr><td>Teflon tape&amp;nbsp;</td><td>Chuan Chi Trading Co. Ltd</td><td>CS170000</td><td></td></tr><tr><td>Contact Angle Goniometer</td><td>Sindatek</td><td>Model 100SB</td><td></td></tr><tr><td>Auxiliary Heater</td><td>Chuan Chi Trading Co. Ltd</td><td></td><td></td></tr><tr><td>T- type thermocouples</td><td>Chuan Chi Trading Co. Ltd</td><td></td><td></td></tr><tr><td>Reflux Condenser&amp;nbsp;</td><td>Chuan Chi Trading Co. Ltd</td><td></td><td></td></tr><tr><td>Fiber glass</td><td>Professional Plastics, Taiwan</td><td></td><td></td></tr></tbody></table>

pool-boiling heat-transfer enhancement on cylindrical surfaces with hybrid wettable patterns

In this study, pool-boiling heat-transfer experiments were performed to investigate the effect of the number of interlines and the orientation of the hybrid wettable pattern. Hybrid wettable patterns were produced by coating superhydrophilic SiO2 on a masked, hydrophobic, cylindrical copper surface. Using de-ionized (DI) water as the working fluid, pool-boiling heat-transfer studies were conducted on the different surface-treated copper cylinders of a 25-mm diameter and a 40-mm length. The experimental results showed that the number of interlines and the orientation of the hybrid wettable pattern influenced the wall superheat and the HTC. By increasing the number of interlines, the HTC was enhanced when compared to the plain surface. Images obtained from the charge-coupled device (CCD) camera indicated that more bubbles formed on the interlines as compared to other parts. The hybrid wettable pattern with the lowermost section being hydrophobic gave the best heat-transfer coefficient (HTC). The experimental results indicated that the bubble dynamics of the surface is an important factor that determines the nucleate boiling.

Esperimenti termodistributori piscina-bollente sono state condotte su una superficie cilindrica bagnabile ibrido usando l&#39;apparato sperimentale il cui schema è mostrato in figura 5. La procedura sperimentale piscina-bollente spiegato nel passaggio 2 della sezione protocollo è stato effettuato con successo mentre indaga l&#39;effetto del numero di interlining e dell&#39;orientamento del modello bagnabile ibrida sul rendimento piscina-bollente. Le prestazioni piscina...

Watch this Scientific Journal Video about Pool-Boiling Heat-Transfer Enhancement on Cylindrical Surfaces with Hybrid Wettable Patterns at JoVE.com

Pool-Boiling Heat-Transfer Enhancement on Cylindrical Surfaces with Hybrid Wettable Patterns

esperimenti di trasferimento di calore Pool-bollente sono state effettuate per osservare gli effetti dei modelli ibridi bagnabili sul coefficiente di scambio termico (HTC). I parametri di ricerca sono il numero di interlining e l&#39;orientamento modello della superficie bagnabile modificata.

Enhancement Pool-ebollizione di trasferimento del calore su superfici cilindriche con i modelli ibridi bagnabili

In this study, pool-boiling heat-transfer experiments were performed to investigate the effect of the number of interlines and the orientation of the ...

pool-boiling-heat-transfer-enhancement-on-cylindrical-surfaces-with

Research

JoVE Journal

Engineering

9.0K Views.  National Taiwan University.  esperimenti di trasferimento di calore Pool-bollente sono state effettuate per osservare gli effetti dei modelli ibridi bagnabili sul coefficiente di scambio termico (HTC). I parametri di ricerca sono il numero di interlining e l'orientamento modello della superficie bagnabile modificata. 

Video: Pool-Boiling Heat-Transfer Enhancement on Cylindrical Surfaces with Hybrid Wettable Patterns

Visualization of High Speed Liquid Jet Impaction on a Moving Surface

Two apparatuses for examining liquid jet impingement on a high-speed moving surface are described: an air cannon device (for examining surface speeds between 0 and 25 m/sec) and a spinning disk device (for examining surface speeds between 15 and 100 m/sec). The air cannon linear traverse is a pneumatic energy-powered system that is designed to accelerate a metal rail surface mounted on top of a wooden projectile. A pressurized cylinder fitted with a solenoid valve rapidly releases pressurized air into the barrel, forcing the projectile down the cannon barrel. The projectile travels beneath a spray nozzle, which impinges a liquid jet onto its metal upper surface, and the projectile then hits a stopping mechanism. A camera records the jet impingement, and a pressure transducer records the spray nozzle backpressure. The spinning disk set-up consists of a steel disk that reaches speeds of 500 to 3,000 rpm via a variable frequency drive (VFD) motor. A spray system similar to that of the air cannon generates a liquid jet that impinges onto the spinning disc, and cameras placed at several optical access points record the jet impingement. Video recordings of jet impingement processes are recorded and examined to determine whether the outcome of impingement is splash, splatter, or deposition. The apparatuses are the first that involve the high speed impingement of low-Reynolds-number liquid jets on high speed moving surfaces. In addition to its rail industry applications, the described technique may be used for technical and industrial purposes such as steelmaking and may be relevant to high-speed 3D printing.

Two experimental devices for examining liquid jet impingement on a high-speed moving surface are described: an air cannon device and a spinning disk device. The apparatuses are used to determine optimal approaches to the application of liquid friction modifier (LFM) onto rail tracks for top-of-rail friction control.

Visualizzazione di Liquid High Speed ​​Jet Occlusione su una superficie mobile

Two apparatuses for examining liquid jet impingement on a high-speed moving surface are described: an air cannon device (for examining surface speeds ...

Ricerca

Ingegneria

Measurements of Local Instantaneous Convective Heat Transfer in a Pipe - Single and Two-phase Flow

This manuscript provides step by step description of the manufacturing process of a test section designed to measure the local instantaneous heat transfer coefficient as a function of the liquid flow rate in a transparent pipe. With certain amendments, the approach is extended to gas-liquid flows, with a particular emphasis on the effect of a single elongated (Taylor) air bubble on heat transfer enhancement. A non-invasive thermography technique is applied to measure the instantaneous temperature of a thin metal foil heated electrically. The foil is glued to cover a narrow slot cut in the pipe. The thermal inertia of the foil is small enough to detect the variation in the instantaneous foil temperature. The test section can be moved along the pipe and is long enough to cover a considerable part of the growing thermal boundary layer.
At the beginning of each experimental run, a steady state with a constant water flow rate and heat flux to the foil is attained and serves as the reference. The Taylor bubble is then injected into the pipe. The heat transfer coefficient variations due to the passage of a Taylor bubble propagating in a vertical pipe is measured as function of the distance of the measuring point from the bottom of the moving Taylor bubble. Thus, the results represent the local heat transfer coefficients. Multiple independent runs preformed under identical conditions allow accumulating sufficient data to calculate reliable ensemble-averaged results on the transient convective heat transfer. In order to perform this in a frame of reference moving with the bubble, the location of the bubble along the pipe has to be known at all times. Detailed description of measurements of the length and of the translational velocity of the Taylor bubbles by optical probes is presented.

This manuscript describes methods aimed at measuring the local instantaneous convective heat transfer coefficients in a single or two-phase pipe flow. A simple optical method to determine the length and the propagation velocity of an elongated (Taylor) air bubble moving at a constant velocity is also presented.

Misure di scambio di calore convettivo istantanea locale in un tubo - flusso singolo e due fasi

This manuscript provides step by step description of the manufacturing process of a test section designed to measure the local instantaneous heat transfer ...

Uncoupling Coriolis Force and Rotating Buoyancy Effects on Full-Field Heat Transfer Properties of a Rotating Channel

An experimental method for exploring the heat transfer characteristics of an axially rotating channel is proposed. The governing flow parameters that characterize the transport phenomena in a rotating channel are identified via the parametric analysis of the momentum and energy equations referring to a rotating frame of reference. Based on these dimensionless flow equations, an experimental strategy that links the design of the test module, the experimental program and the data analysis is formulated with the attempt to reveal the isolated Coriolis-force and buoyancy effects on heat transfer performances. The effects of Coriolis force and rotating buoyancy are illustrated using the selective results measured from rotating channels with various geometries. While the Coriolis-force and rotating-buoyancy impacts share several common features among the various rotating channels, the unique heat transfer signatures are found in association with the flow direction, the channel shape and the arrangement of heat transfer enhancement devices. Regardless of the flow configurations of the rotating channels, the presented experimental method enables the development of physically consistent heat transfer correlations that permit the evaluation of isolated and interdependent Coriolis-force and rotating-buoyancy effects on the heat transfer properties of rotating channels.

Here, we present an experimental method for decoupling the interdependent Coriolis-force and rotating-buoyancy effects on full-field heat transfer distributions of a rotating channel.

Disgiungere forza di Coriolis e rotante galleggiabilità effetti sul calore pieno campo il trasferimento di proprietà di un canale rotante

An experimental method for exploring the heat transfer characteristics of an axially rotating channel is proposed. The governing flow parameters that ...

Analyzing Mixing Inhomogeneity in a Microfluidic Device by Microscale Schlieren Technique

In this paper, we introduce the use of microscale schlieren technique to measure mixing inhomogeneity in a microfluidic device. The microscale schlieren system is constructed from a Hoffman modulation contrast microscope, which provides easy access to the rear focal plane of the objective lens, by removing the slit plate and replacing the modulator with a knife-edge. The working principle of microscale schlieren technique relies on detecting light deflection caused by variation of refractive index1-3. The deflected light either escapes or is obstructed by the knife-edge to produce a bright or a dark band, respectively. If the refractive index of the mixture varies linearly with its composition, the local change in light intensity in the image plane is proportional to the concentration gradient normal to the optical axis. The micro-schlieren image gives a two-dimensional projection of the disturbed light produced by three-dimensional inhomogeneity.
To accomplish quantitative analysis, we describe a calibration procedure that mixes two fluids in a T-microchannel. We carry out a numerical simulation to obtain the concentration gradient in the T-microchannel that correlates closely with the corresponding micro-schlieren image. By comparison, a relationship between the grayscale readouts of the micro-schlieren image and the concentration gradients presented in a microfluidic device is established. Using this relationship, we are able to analyze the mixing inhomogeneity from associate micro-schlieren image and demonstrate the capability of microscale schlieren technique with measurements in a microfluidic oscillator4. For optically transparent fluids, microscale schlieren technique is an attractive diagnostic tool to provide instantaneous full-field information that retains the three-dimensional features of the mixing process.

Herein, we describe a procedure that employs microscale schlieren technique to measure mixing inhomogeneity in a microfluidic device. Through calibration, distribution of concentration gradient can be derived from the micro-schlieren image.

Analizzando disomogeneità Mescolando in un dispositivo a microfluidi da Tecnica microscala Schlieren

In this paper, we introduce the use of microscale schlieren technique to measure mixing inhomogeneity in a microfluidic device. The microscale schlieren ...

Bioingegneria

Scalable Stamp Printing and Fabrication of Hemiwicking Surfaces

Hemiwicking is a process where a fluid wets a patterned surface beyond its normal wetting length due to a combination of capillary action and imbibition. This wetting phenomenon is important in many technical fields ranging from physiology to aerospace engineering. Currently, several different techniques exist for fabricating hemiwicking structures. These conventional methods, however, are often time consuming and are difficult to scale-up for large areas or are difficult to customize for specific, nonhomogeneous patterning geometries. The presented protocol provides researchers with a simple, scalable, and cost-effective method for fabricating micro-patterned hemiwicking surfaces. The method fabricates wicking structures through the use of stamp printing, polydimethylsiloxane (PDMS) molding, and thin-film surface coatings. The protocol is demonstrated for hemiwicking with ethanol on PDMS micropillar arrays coated with a 70 nm thick aluminum thin-film.

A simple protocol is provided for the fabrication of hemiwicking structures of varying sizes, shapes, and materials. The protocol uses a combination of physical stamping, PDMS molding, and thin-film surface modifications via common materials deposition techniques.

Stampa timbro scalabile e fabbricazione delle superfici Hemiwicking

Hemiwicking is a process where a fluid wets a patterned surface beyond its normal wetting length due to a combination of capillary action and imbibition. ...

Rendering SiO2/Si Surfaces Omniphobic by Carving Gas-Entrapping Microtextures Comprising Reentrant and Doubly Reentrant Cavities or Pillars

We present microfabrication protocols for rendering intrinsically wetting materials repellent to liquids (omniphobic) by creating gas-entrapping microtextures (GEMs) on them comprising cavities and pillars with reentrant and doubly reentrant features. Specifically, we use SiO2/Si as the model system and share protocols for two-dimensional (2D) designing, photolithography, isotropic/anisotropic etching techniques, thermal oxide growth, piranha cleaning, and storage towards achieving those microtextures. Even though the conventional wisdom indicates that roughening intrinsically wetting surfaces (&#952;o &#60; 90&#176;) renders them even more wetting (&#952;r &#60; &#952;o &#60; 90&#176;), GEMs demonstrate liquid repellence despite the intrinsic wettability of the substrate. For instance, despite the intrinsic wettability of silica &#952;o &#8776; 40&#176; for the water/air system, and &#952;o &#8776; 20&#176; for the hexadecane/air system, GEMs comprising cavities entrap air robustly on immersion in those liquids, and the apparent contact angles for the droplets are &#952;r &#62; 90&#176;. The reentrant and doubly reentrant features in the GEMs stabilize the intruding liquid meniscus thereby trapping the liquid-solid-vapor system in metastable air-filled states (Cassie states) and delaying wetting transitions to the thermodynamically-stable fully-filled state (Wenzel state) by, for instance, hours to months. Similarly, SiO2/Si surfaces with arrays of reentrant and doubly reentrant micropillars demonstrate extremely high contact angles (&#952;r &#8776; 150&#176;&#8211;160&#176;) and low contact angle hysteresis for the probe liquids, thus characterized as superomniphobic. However, on immersion in the same liquids, those surfaces dramatically lose their superomniphobicity and get fully-filled within &#60;1 s. To address this challenge, we present protocols for hybrid designs that comprise arrays of doubly reentrant pillars surrounded by walls with doubly reentrant profiles. Indeed, hybrid microtextures entrap air on immersion in the probe liquids. To summarize, the protocols described here should enable the investigation of GEMs in the context of achieving omniphobicity without chemical coatings, such as perfluorocarbons, which might unlock the scope of inexpensive common materials for applications as omniphobic materials. Silica microtextures could also serve as templates for soft materials.

Rendering SiO2/Si Surfaces Omniphobic by Carving Gas-Entrapping Microtextures Comprising Reentrant and Doubly Reentrant Cavities or Pillars

This work presents microfabrication protocols for achieving cavities and pillars with reentrant and doubly reentrant profiles on SiO2/Si wafers using photolithography and dry etching. Resulting microtextured surfaces demonstrate remarkable liquid repellence, characterized by robust long-term entrapment of air under wetting liquids, despite the intrinsic wettability of silica.

Rendering di siO2/Si Superfici omnifobiche da intaglio Gas-Entrapping Microtextures Comprising Reentrant e Doubly Reentrant Cavities or Pillars

We present microfabrication protocols for rendering intrinsically wetting materials repellent to liquids (omniphobic) by creating gas-entrapping ...

Proof-of-Concept for Gas-Entrapping Membranes Derived from Water-Loving SiO2/Si/SiO2 Wafers for Green Desalination

Desalination through direct contact membrane distillation (DCMD) exploits water-repellent membranes to robustly separate counterflowing streams of hot and salty seawater from cold and pure water, thus allowing only pure water vapor to pass through. To achieve this feat, commercial DCMD membranes are derived from or coated with water-repellent perfluorocarbons such as polytetrafluoroethylene (PTFE) and polyvinylidene difluoride (PVDF). However, the use of perfluorocarbons is limiting due to their high cost, non-biodegradability, and vulnerability to harsh operational conditions. Unveiled here is a new class of membranes referred to as gas-entrapping membranes (GEMs) that can robustly entrap air upon immersion in water. GEMs achieve this function by their microstructure rather than their chemical make-up. This work demonstrates a proof-of-concept for GEMs using intrinsically wetting SiO2/Si/SiO2 wafers as the model system; the contact angle of water on SiO2 is &#952;o &#8776; 40&#176;. Silica-GEMs had 300 &#956;m-long cylindrical pores whose diameters at the (2 &#956;m-long) inlet and outlet regions were significantly smaller; this geometrically discontinuous structure, with 90&#176; turns at the inlets and outlets, is known as the &#34;reentrant microtexture&#34;. The microfabrication protocol for silica-GEMs entails designing, photolithography, chrome sputtering, and isotropic and anisotropic etching. Despite the water loving nature of silica, water does not intrude silica-GEMs on submersion. In fact, they robustly entrap air underwater and keep it intact even after six weeks (&#62;106 seconds). On the other hand, silica membranes with simple cylindrical pores spontaneously imbibe water (&#60; 1 s). These findings highlight the potential of the GEMs architecture for separation processes. While the choice of SiO2/Si/SiO2 wafers for GEMs is limited to demonstrating the proof-of-concept, it is expected that the protocols and concepts presented here will advance the rational design of scalable GEMs using inexpensive common materials for desalination and beyond.

Proof-of-Concept for Gas-Entrapping Membranes Derived from Water-Loving SiO2/Si/SiO2 Wafers for Green Desalination

Presented here is a stepwise protocol for realizing gas-entrapping membranes (GEMs) from SiO2/Si wafers using integrated circuit microfabrication technology. When silica-GEMs are immersed in water, the intrusion of water is prevented, despite the water-loving composition of silica.

Proof-of-Concept per le membrane che affliggiano il gas Derivate da SiO2/Si/SiO2 Wafers per la desalinizzazione verde

Desalination through direct contact membrane distillation (DCMD) exploits water-repellent membranes to robustly separate counterflowing streams of hot and ...

Preparation of Free-Surface Hyperbolic Water Vortices

Free surface vortices are present in industry in flow regulation, energy dissipation, and energy generation. Although investigated extensively, detailed experimental data regarding free surface vortices are lacking, particularly regarding the turbulence at the interface. The present paper reports on a special type of free surface vortex first proposed by Walter Schauberger in the 1960s that has an oxygen volumetric mass transfer coefficient exceeding the value of similar systems. This special type of vortex forms in a hyperbolic funnel. Different stable regimes can be stabilized with different hydraulic characteristics. Other advantages of this technology are its energy efficiency, simple design, and scalability. The flow in this hyperbolic funnel is characterized by strong turbulence and an increased surface area of the air-water interface. The local pressure strongly varies along the surface, resulting in a pronounced wavey air-water boundary layer. Due to the helical flow, these perturbations move inward, pulling the boundary layer with them. The resultant pressure gradient draws a certain air volume into the water vortex. The construction of the basic hyperbolic funnel setup and operational examples, including high-speed visualization for three different stable regimes, are presented in this work.

This paper describes how three different water vortex regimes in a hyperbolic Schauberger funnel can be created, their most important characteristics, and how associated parameters such as the oxygen transfer rates can be calculated.

Preparazione di vortici d'acqua iperbolici a superficie libera

Free surface vortices are present in industry in flow regulation, energy dissipation, and energy generation. Although investigated extensively, detailed ...

Testing the Heat Transfer Efficiency of a Finned-tube Heat Exchanger

Source: Michael G. Benton and Kerry M. Dooley, Department of Chemical Engineering, Louisiana State University, Baton Rouge, LA
Heat exchangers transfer heat from one fluid to another fluid. Multiple classes of heat exchangers exist to fill different needs. Some of the most common types are shell and tube exchangers and plate exchangers1. Shell and tube heat exchangers use a system of tubes through which fluid flows1. One set of tubes contains the liquid to be cooled or heated, while the second set contains the liquid that will either absorb heat or transmit it1. Plate heat exchangers use a similar concept, in which plates are closely joined together with a small gap between each for liquid to flow1. The fluid flowing between the plates alternates between hot and cold so that heat will move into or out of the necessary streams1. These exchangers have large surface areas, so they are usually more efficient1.
The goal for this experiment is to test the heat transfer efficiency of a finned-tube heat exchanger (Figure 1) and compare it to the theoretical efficiency of a heat exchanger without fins. The experimental data will be measured for three different flow rates of monoethylene glycol (MEG). Two different water flow rates for each MEG flow rate will be used. Using the Wilson plot method the heat transfer coefficients will be determined from the experimental data. Additionally, the Reynold&#39;s number and the amount of heat transferred will be compared for flow with and without the fins to evaluate heat transfer efficiency.
<img alt="Figure 1" src="/files/ftp_upload/10437/10437fig1.jpg" /> 
Figure 1: Finned-tube Heat Exchanger. 1) MEG outlet temperature 2) water inlet temperature 3) MEG inlet temperature 4) water outlet temperature 5) water meter 6) MEG accumulation sight glass/cylinder.

Heat Transfer Efficiency Test of a Finned-tube Heat Exchanger

Verifica dell'efficienza del trasferimento di calore di uno scambiatore di calore a tubi alettati

Source: Michael G. Benton and Kerry M. Dooley, Department of Chemical Engineering, Louisiana State University, Baton Rouge, LA
Heat exchangers transfer ...

Didattica

JoVE Science Education

Ingegneria chimica

Quenching and Boiling

Source: Alexander S Rattner, Sanjay Adhikari, and Mahdi Nabil; Department of Mechanical and Nuclear Engineering, The Pennsylvania State University, University Park, PA
Controlled heating followed by rapid cooling is an important element of many materials processing applications. This heat-treating procedure can increase material hardness, which is important for cutting tools or surfaces in high wear environments. The rapid cooling stage is called quenching, and is often performed by immersing materials in a fluid bath (often water or oil). Quenching heat transfer can occur due to forced convection - when the action of rapidly moving material through coolant drives the heat transfer process, and due to free convection - when the reduced density of hot fluid near the material surface causes buoyancy-driven circulation and heat transfer. At high material temperatures, the coolant can boil, leading to increased heat transfer effectiveness. However, when extremely hot materials are quenched, they can be blanketed in relatively low thermal conductivity coolant vapor, leading to poor heat transfer.
In this experiment, quenching heat transfer will be measured for a heated copper cylinder, which is representative of small heat-treated parts. The transient sample temperature profile will be measured during quenching and compared with theoretical results for free convection heat transfer. Boiling phenomena will also be investigated qualitatively.

Quenching, Boiling, Convection and Nusselt Number

Raffreddamento ed ebollizione

Source: Alexander S Rattner, Sanjay Adhikari, and Mahdi Nabil; Department of Mechanical and Nuclear Engineering, The Pennsylvania State University, ...

Enhancement Pool-ebollizione di trasferimento del calore su superfici cilindriche con i modelli ibridi bagnabili

Riepilogo

Esplora Altri Video

Capitoli in questo video

Visualizzazione di Liquid High Speed Jet Occlusione su una superficie mobile

Misure di scambio di calore convettivo istantanea locale in un tubo - flusso singolo e due fasi

Disgiungere forza di Coriolis e rotante galleggiabilità effetti sul calore pieno campo il trasferimento di proprietà di un canale rotante

Analizzando disomogeneità Mescolando in un dispositivo a microfluidi da Tecnica microscala Schlieren

Stampa timbro scalabile e fabbricazione delle superfici Hemiwicking

Rendering di siO₂/Si Superfici omnifobiche da intaglio Gas-Entrapping Microtextures Comprising Reentrant e Doubly Reentrant Cavities or Pillars

Proof-of-Concept per le membrane che affliggiano il gas Derivate da SiO₂/Si/SiO₂ Wafers per la desalinizzazione verde

Preparazione di vortici d'acqua iperbolici a superficie libera

Verifica dell'efficienza del trasferimento di calore di uno scambiatore di calore a tubi alettati

Raffreddamento ed ebollizione

Enhancement Pool-ebollizione di trasferimento del calore su superfici cilindriche con i modelli ibridi bagnabili

Riepilogo

Esplora Altri Video

Capitoli in questo video

Visualizzazione di Liquid High Speed ​​Jet Occlusione su una superficie mobile

Misure di scambio di calore convettivo istantanea locale in un tubo - flusso singolo e due fasi

Disgiungere forza di Coriolis e rotante galleggiabilità effetti sul calore pieno campo il trasferimento di proprietà di un canale rotante

Analizzando disomogeneità Mescolando in un dispositivo a microfluidi da Tecnica microscala Schlieren

Stampa timbro scalabile e fabbricazione delle superfici Hemiwicking

Rendering di siO2/Si Superfici omnifobiche da intaglio Gas-Entrapping Microtextures Comprising Reentrant e Doubly Reentrant Cavities or Pillars

Proof-of-Concept per le membrane che affliggiano il gas Derivate da SiO2/Si/SiO2 Wafers per la desalinizzazione verde

Preparazione di vortici d'acqua iperbolici a superficie libera

Verifica dell'efficienza del trasferimento di calore di uno scambiatore di calore a tubi alettati

Raffreddamento ed ebollizione

Visualizzazione di Liquid High Speed Jet Occlusione su una superficie mobile

Rendering di siO₂/Si Superfici omnifobiche da intaglio Gas-Entrapping Microtextures Comprising Reentrant e Doubly Reentrant Cavities or Pillars

Proof-of-Concept per le membrane che affliggiano il gas Derivate da SiO₂/Si/SiO₂ Wafers per la desalinizzazione verde