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JoVE Journal

Chemistry

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Preparation of Enantiopure Non-Activated Aziridines and Synthesis of Biemamide B, D, and epiallo-Isomuscarine

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11:04 min

June 13th, 2022

June 13th, 2022

2,770 Views

0:04

Introduction

1:31

Synthesis of the Diastereomeric Mixture of Chiral Aziridine (-)-Mentholyl Ester Derivative

6:38

Regio and Stereoselective Aziridine Ring-Opening by Azide Nucleophile for the Total Synthesis of Biemamide B and Biemamide D

8:33

Results: Synthesis of Aziridine-2-Carboxylates, Biemamide, and Epiallo-Isomuscarine

10:16

Conclusion

Transcribir

For the last 30 years, Professor Hyun-Joon Ha's group has studied the aziridine chemistry and developed the synthesis of nitrogen-containing valuable molecules in an asymmetric manner. In this visual experiment, we show here the synthesis of enant

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In this study, we prepare both enantiomers of aziridine-2-carboxylate, which are used in the asymmetric synthesis of alkaloids, including biemamide B and D, and (-)-epiallo-isomuscarine.

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