Synthesis of Aza-Michael Adduct 4: Tricarbonyl[(2-5-η)-6-((2-phenylethyl) Amino cyclohepta-2,4-dien-1-one]Iron
1:48
Synthesis of Tricarbonyl[(2-5-η)-6-(2-methylanilino)cyclohepta-2, 4-dien-1-one]Iron (3)
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Protection of Amine 4 as a Tert-butyl Carbamate
4:30
Synthesis of Tert-butyl (6-oxocyclohepta-2, 4-dien-1-yl)(2-phenylethyl) Carbamate (6)
5:41
Results: Description of NMR Spectral Data for Selected Compounds
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Conclusion
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This protocol is an efficient method for the synthesis of aminated tropone derivatives. These compounds can serve as synthetic intermediates for the synthesis of structurally complex amines. An advantage of this technique is that the aza-Micheal a
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Representative experimental procedures for the addition of amine nucleophiles to tricarbonyl(tropone)iron and subsequent demetallation of the resulting complexes are presented in detail.